##############################################################################
###                                                                        ###
###        Electronic paper (Acta Crystallographica Section E)             ###
###                                                                        ###
##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in Acta     #
# Crystallographica Section E. It conforms to the requirements of Notes      #
# for Authors for Section E, and has been peer reviewed under the auspices   #
# of the IUCr Commission on Journals.                                        #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.1.    #
#                                                                            #
# Software is freely available for graphical display of the structure(s) in  #
# this CIF.  For information consult the CIF home page http://www.iucr.org/  #
# cif/home.html                                                              #
#                                                                            #
#            Copyright International Union of Crystallography                #
#                                                                            #
##############################################################################
                                             
data_I
_audit_creation_method     SHELXL-97
_chemical_name_systematic
;
(3,5-Dimethyl-1H-pyrazole-\kN²)(4-oxidopent-3-en-2-one
2-hydroxybenzoylhydrazonatoκ²N,O)copper(II)
;
_chemical_name_common     ?
_chemical_formula_moiety     'C17 H20 Cu N4 O3'
_chemical_formula_sum     'C17 H20 Cu N4 O3'
_chemical_formula_iupac     '[Cu (C12 H12 N2 O3) (C5 H8 N2)]'
_chemical_formula_weight     391.91
_chemical_melting_point     ?
_symmetry_cell_setting     triclinic
_symmetry_space_group_name_H-M     'P -1'
_symmetry_space_group_name_Hall     '-P 1'
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, -y, -z'
_cell_length_a     8.0713(7)
_cell_length_b     10.6660(11)
_cell_length_c     10.9429(8)
_cell_angle_alpha     110.393(4)
_cell_angle_beta     96.174(3)
_cell_angle_gamma     96.299(4)
_cell_volume     866.87(13)
_cell_formula_units_Z     2
_cell_measurement_reflns_used     3907
_cell_measurement_theta_min     2.57
_cell_measurement_theta_max     27.48
_cell_measurement_temperature     293(2)
_exptl_crystal_description     block
_exptl_crystal_colour     black
_exptl_crystal_size_max     0.62
_exptl_crystal_size_mid     0.53
_exptl_crystal_size_min     0.45
_exptl_crystal_density_diffrn     1.501
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     406
_exptl_absorpt_coefficient_mu     1.284
_exptl_absorpt_correction_type     psi-scan
_exptl_absorpt_process_details
                               '(TEXRAY; Molecular Structure Corporation, 1999)'
_exptl_absorpt_correction_T_min     0.538
_exptl_absorpt_correction_T_max     0.774
_exptl_special_details
;
 ?
;
_diffrn_ambient_temperature     293(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'fine-focus sealed tube'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type     'Rigaku Weissenberg IP area-detector'
_diffrn_measurement_method     ω
_diffrn_detector_area_resol_mean     ?
_diffrn_reflns_number     8035
_diffrn_reflns_av_R_equivalents     0.035
_diffrn_reflns_av_sigmaI/netI     0.0222
_diffrn_reflns_theta_min     2.57
_diffrn_reflns_theta_max     27.48
_diffrn_reflns_theta_full     27.48
_diffrn_measured_fraction_theta_max     0.981
_diffrn_measured_fraction_theta_full     0.981
_diffrn_reflns_limit_h_min     -10
_diffrn_reflns_limit_h_max     10
_diffrn_reflns_limit_k_min     0
_diffrn_reflns_limit_k_max     13
_diffrn_reflns_limit_l_min     -14
_diffrn_reflns_limit_l_max     13
_diffrn_standards_number     0
_diffrn_standards_interval_count     .
_diffrn_standards_interval_time     .
_diffrn_standards_decay_%     0
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
_reflns_number_total     3907
_reflns_number_gt     3549
_reflns_threshold_expression     I>2σ(I)
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.0373
_refine_ls_R_factor_gt     0.0330
_refine_ls_wR_factor_gt     0.0882
_refine_ls_wR_factor_ref     0.0908
_refine_ls_goodness_of_fit_ref     1.069
_refine_ls_restrained_S_all     1.069
_refine_ls_number_reflns     3907
_refine_ls_number_parameters     232
_refine_ls_number_restraints     0
_refine_ls_hydrogen_treatment     constr
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
           'calc w=1/[σ²(Fo²)+(0.047P)²+0.356P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.000
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.323
_refine_diff_density_min     -0.489
_refine_ls_extinction_method     none
_refine_ls_extinction_coef     ?
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0061 0.0033
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Cu' 'Cu' 0.3201 1.2651
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'TEXRAY (Molecular Structure Corporation, 1999)'
_computing_cell_refinement     'TEXRAY'
_computing_data_reduction     'TEXSAN (Molecular Structure Corporation, 1999)'
_computing_structure_solution     'SHELXS97 (Sheldrick, 1997)'
_computing_structure_refinement     'SHELXL97 (Sheldrick, 1997)'
_computing_molecular_graphics     'ORTEX (McArdle, 1995)'
_computing_publication_material     'SHELXL97/2'
loop_
    _atom_site_type_symbol
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    Cu Cu1 0.32166(3) 0.04733(2) 0.43229(2) 0.03629(9) Uani d . 1 . .
    O O1 0.7545(3) 0.50508(19) 0.60846(19) 0.0663(5) Uani d . 1 . .
    H H01 0.6879 0.4312 0.5424 0.073(9) Uiso d R 1 . .
    O O2 0.44823(19) 0.15762(15) 0.60425(14) 0.0461(3) Uani d . 1 . .
    O O3 0.21695(19) -0.05728(15) 0.25458(14) 0.0432(3) Uani d . 1 . .
    N N1 0.5481(2) 0.28407(17) 0.48744(17) 0.0391(4) Uani d . 1 . .
    N N2 0.4483(2) 0.17950(17) 0.38205(17) 0.0380(3) Uani d . 1 . .
    N N3 0.1760(2) -0.07361(16) 0.49460(16) 0.0363(3) Uani d . 1 . .
    N N4 0.0805(2) -0.18331(17) 0.39976(17) 0.0394(4) Uani d . 1 . .
    H H4B 0.0826 -0.2036 0.3167 0.047 Uiso calc R 1 . .
    C C1 0.6301(2) 0.3684(2) 0.7213(2) 0.0399(4) Uani d . 1 . .
    C C2 0.7339(3) 0.4830(2) 0.7206(2) 0.0480(5) Uani d . 1 . .
    C C3 0.8180(4) 0.5793(3) 0.8393(3) 0.0648(7) Uani d . 1 . .
    H H3A 0.8868 0.6549 0.8389 0.078 Uiso calc R 1 . .
    C C4 0.8011(4) 0.5645(3) 0.9570(3) 0.0665(7) Uani d . 1 . .
    H H4A 0.8585 0.6299 1.0355 0.080 Uiso calc R 1 . .
    C C5 0.6990(4) 0.4529(3) 0.9598(3) 0.0635(7) Uani d . 1 . .
    H H5A 0.6870 0.4433 1.0398 0.076 Uiso calc R 1 . .
    C C6 0.6154(3) 0.3561(2) 0.8430(2) 0.0516(5) Uani d . 1 . .
    H H6A 0.5475 0.2808 0.8451 0.062 Uiso calc R 1 . .
    C C7 0.5368(2) 0.2640(2) 0.5988(2) 0.0379(4) Uani d . 1 . .
    C C8 0.5657(3) 0.2929(3) 0.2440(3) 0.0570(6) Uani d . 1 . .
    H H8A 0.5385 0.3792 0.2953 0.085 Uiso calc R 1 . .
    H H8B 0.5499 0.2816 0.1523 0.085 Uiso calc R 1 . .
    H H8C 0.6811 0.2888 0.2720 0.085 Uiso calc R 1 . .
    C C9 0.4522(3) 0.1821(2) 0.2633(2) 0.0414(4) Uani d . 1 . .
    C C10 0.3518(3) 0.0794(2) 0.1511(2) 0.0465(5) Uani d . 1 . .
    H H10A 0.3589 0.0833 0.0652 0.061(8) Uiso d R 1 . .
    C C11 0.2441(3) -0.0300(2) 0.15091(19) 0.0414(4) Uani d . 1 . .
    C C12 0.1443(3) -0.1298(3) 0.0236(2) 0.0548(6) Uani d . 1 . .
    H H12A 0.1642 -0.2196 0.0141 0.082 Uiso calc R 1 . .
    H H12B 0.1786 -0.1083 -0.0490 0.082 Uiso calc R 1 . .
    H H12C 0.0263 -0.1252 0.0245 0.082 Uiso calc R 1 . .
    C C13 0.2148(3) 0.0264(3) 0.7394(2) 0.0508(5) Uani d . 1 . .
    H H13A 0.2377 0.1128 0.7305 0.076 Uiso calc R 1 . .
    H H13B 0.3183 0.0022 0.7697 0.076 Uiso calc R 1 . .
    H H13C 0.1386 0.0315 0.8019 0.076 Uiso calc R 1 . .
    C C14 0.1368(2) -0.0781(2) 0.6090(2) 0.0398(4) Uani d . 1 . .
    C C15 0.0153(3) -0.1918(2) 0.5839(2) 0.0473(5) Uani d . 1 . .
    H H15A -0.0335 -0.2182 0.6461 0.057 Uiso calc R 1 . .
    C C16 -0.0177(3) -0.2569(2) 0.4492(2) 0.0441(5) Uani d . 1 . .
    C C17 -0.1356(3) -0.3825(3) 0.3632(3) 0.0601(6) Uani d . 1 . .
    H H17A -0.2145 -0.3608 0.3043 0.090 Uiso calc R 1 . .
    H H17B -0.1957 -0.4195 0.4171 0.090 Uiso calc R 1 . .
    H H17C -0.0723 -0.4478 0.3128 0.090 Uiso calc R 1 . .
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    Cu1 O3 . 1.9153(14) yes
    Cu1 N2 . 1.9180(16) yes
    Cu1 O2 . 1.9361(14) yes
    Cu1 N3 . 1.9911(16) yes
    O1 C2 . 1.351(3) no
    O1 H01 . 0.9266 no
    O2 C7 . 1.296(2) no
    O3 C11 . 1.300(2) no
    N1 C7 . 1.319(3) no
    N1 N2 . 1.389(2) no
    N2 C9 . 1.313(3) no
    N3 C14 . 1.340(3) no
    N3 N4 . 1.351(2) no
    N4 C16 . 1.338(3) no
    N4 H4B . 0.8600 no
    C1 C6 . 1.399(3) no
    C1 C2 . 1.407(3) no
    C1 C7 . 1.471(3) no
    C2 C3 . 1.389(3) no
    C3 C4 . 1.370(4) no
    C3 H3A . 0.9300 no
    C4 C5 . 1.382(4) no
    C4 H4A . 0.9300 no
    C5 C6 . 1.377(3) no
    C5 H5A . 0.9300 no
    C6 H6A . 0.9300 no
    C8 C9 . 1.503(3) no
    C8 H8A . 0.9600 no
    C8 H8B . 0.9600 no
    C8 H8C . 0.9600 no
    C9 C10 . 1.421(3) no
    C10 C11 . 1.375(3) no
    C10 H10A . 0.9630 no
    C11 C12 . 1.503(3) no
    C12 H12A . 0.9600 no
    C12 H12B . 0.9600 no
    C12 H12C . 0.9600 no
    C13 C14 . 1.489(3) no
    C13 H13A . 0.9600 no
    C13 H13B . 0.9600 no
    C13 H13C . 0.9600 no
    C14 C15 . 1.399(3) no
    C15 C16 . 1.374(3) no
    C15 H15A . 0.9300 no
    C16 C17 . 1.495(3) no
    C17 H17A . 0.9600 no
    C17 H17B . 0.9600 no
    C17 H17C . 0.9600 no
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    O3 Cu1 N2 . . 93.22(6) yes
    O3 Cu1 O2 . . 173.97(6) yes
    N2 Cu1 O2 . . 81.76(6) yes
    O3 Cu1 N3 . . 89.24(6) yes
    N2 Cu1 N3 . . 173.60(7) yes
    O2 Cu1 N3 . . 96.10(6) yes
    C2 O1 H01 . . 104.1 no
    C7 O2 Cu1 . . 110.40(13) no
    C11 O3 Cu1 . . 125.59(13) no
    C7 N1 N2 . . 110.46(16) no
    C9 N2 N1 . . 117.64(16) no
    C9 N2 Cu1 . . 128.44(14) no
    N1 N2 Cu1 . . 113.91(12) no
    C14 N3 N4 . . 105.48(16) no
    C14 N3 Cu1 . . 138.34(14) no
    N4 N3 Cu1 . . 116.14(13) no
    C16 N4 N3 . . 112.56(17) no
    C16 N4 H4B . . 123.7 no
    N3 N4 H4B . . 123.7 no
    C6 C1 C2 . . 118.2(2) no
    C6 C1 C7 . . 119.98(19) no
    C2 C1 C7 . . 121.83(19) no
    O1 C2 C3 . . 117.9(2) no
    O1 C2 C1 . . 122.7(2) no
    C3 C2 C1 . . 119.4(2) no
    C4 C3 C2 . . 121.1(2) no
    C4 C3 H3A . . 119.5 no
    C2 C3 H3A . . 119.5 no
    C3 C4 C5 . . 120.4(2) no
    C3 C4 H4A . . 119.8 no
    C5 C4 H4A . . 119.8 no
    C6 C5 C4 . . 119.4(3) no
    C6 C5 H5A . . 120.3 no
    C4 C5 H5A . . 120.3 no
    C5 C6 C1 . . 121.6(2) no
    C5 C6 H6A . . 119.2 no
    C1 C6 H6A . . 119.2 no
    O2 C7 N1 . . 123.12(18) no
    O2 C7 C1 . . 119.40(18) no
    N1 C7 C1 . . 117.48(17) no
    C9 C8 H8A . . 109.5 no
    C9 C8 H8B . . 109.5 no
    H8A C8 H8B . . 109.5 no
    C9 C8 H8C . . 109.5 no
    H8A C8 H8C . . 109.5 no
    H8B C8 H8C . . 109.5 no
    N2 C9 C10 . . 120.72(18) no
    N2 C9 C8 . . 120.28(19) no
    C10 C9 C8 . . 118.99(19) no
    C11 C10 C9 . . 126.46(19) no
    C11 C10 H10A . . 114.8 no
    C9 C10 H10A . . 118.7 no
    O3 C11 C10 . . 125.54(19) no
    O3 C11 C12 . . 114.17(18) no
    C10 C11 C12 . . 120.29(19) no
    C11 C12 H12A . . 109.5 no
    C11 C12 H12B . . 109.5 no
    H12A C12 H12B . . 109.5 no
    C11 C12 H12C . . 109.5 no
    H12A C12 H12C . . 109.5 no
    H12B C12 H12C . . 109.5 no
    C14 C13 H13A . . 109.5 no
    C14 C13 H13B . . 109.5 no
    H13A C13 H13B . . 109.5 no
    C14 C13 H13C . . 109.5 no
    H13A C13 H13C . . 109.5 no
    H13B C13 H13C . . 109.5 no
    N3 C14 C15 . . 109.45(19) no
    N3 C14 C13 . . 122.68(18) no
    C15 C14 C13 . . 127.88(19) no
    C16 C15 C14 . . 106.51(19) no
    C16 C15 H15A . . 126.7 no
    C14 C15 H15A . . 126.7 no
    N4 C16 C15 . . 106.01(18) no
    N4 C16 C17 . . 122.3(2) no
    C15 C16 C17 . . 131.7(2) no
    C16 C17 H17A . . 109.5 no
    C16 C17 H17B . . 109.5 no
    H17A C17 H17B . . 109.5 no
    C16 C17 H17C . . 109.5 no
    H17A C17 H17C . . 109.5 no
    H17B C17 H17C . . 109.5 no
loop_
    _geom_torsion_atom_site_label_1
    _geom_torsion_atom_site_label_2
    _geom_torsion_atom_site_label_3
    _geom_torsion_atom_site_label_4
    _geom_torsion_site_symmetry_1
    _geom_torsion_site_symmetry_2
    _geom_torsion_site_symmetry_3
    _geom_torsion_site_symmetry_4
    _geom_torsion
    _geom_torsion_publ_flag
    O3 Cu1 O2 C7 . . . . 39.1(7) no
    N2 Cu1 O2 C7 . . . . 5.28(14) no
    N3 Cu1 O2 C7 . . . . -168.64(14) no
    N2 Cu1 O3 C11 . . . . 1.10(18) no
    O2 Cu1 O3 C11 . . . . -32.3(7) no
    N3 Cu1 O3 C11 . . . . 175.19(18) no
    C7 N1 N2 C9 . . . . -177.03(19) no
    C7 N1 N2 Cu1 . . . . 2.6(2) no
    O3 Cu1 N2 C9 . . . . -1.5(2) no
    O2 Cu1 N2 C9 . . . . 175.2(2) no
    N3 Cu1 N2 C9 . . . . -114.0(6) no
    O3 Cu1 N2 N1 . . . . 178.97(13) no
    O2 Cu1 N2 N1 . . . . -4.38(13) no
    N3 Cu1 N2 N1 . . . . 66.5(6) no
    O3 Cu1 N3 C14 . . . . -170.4(2) no
    N2 Cu1 N3 C14 . . . . -57.7(7) no
    O2 Cu1 N3 C14 . . . . 12.4(2) no
    O3 Cu1 N3 N4 . . . . 6.86(14) no
    N2 Cu1 N3 N4 . . . . 119.6(6) no
    O2 Cu1 N3 N4 . . . . -170.34(13) no
    C14 N3 N4 C16 . . . . 0.2(2) no
    Cu1 N3 N4 C16 . . . . -177.94(14) no
    C6 C1 C2 O1 . . . . -179.0(2) no
    C7 C1 C2 O1 . . . . 0.2(3) no
    C6 C1 C2 C3 . . . . 0.1(4) no
    C7 C1 C2 C3 . . . . 179.4(2) no
    O1 C2 C3 C4 . . . . 179.0(3) no
    C1 C2 C3 C4 . . . . -0.2(4) no
    C2 C3 C4 C5 . . . . -0.1(5) no
    C3 C4 C5 C6 . . . . 0.5(5) no
    C4 C5 C6 C1 . . . . -0.5(4) no
    C2 C1 C6 C5 . . . . 0.2(4) no
    C7 C1 C6 C5 . . . . -179.1(2) no
    Cu1 O2 C7 N1 . . . . -5.9(3) no
    Cu1 O2 C7 C1 . . . . 174.18(14) no
    N2 N1 C7 O2 . . . . 2.3(3) no
    N2 N1 C7 C1 . . . . -177.73(16) no
    C6 C1 C7 O2 . . . . -3.5(3) no
    C2 C1 C7 O2 . . . . 177.2(2) no
    C6 C1 C7 N1 . . . . 176.5(2) no
    C2 C1 C7 N1 . . . . -2.7(3) no
    N1 N2 C9 C10 . . . . -179.21(18) no
    Cu1 N2 C9 C10 . . . . 1.3(3) no
    N1 N2 C9 C8 . . . . 1.8(3) no
    Cu1 N2 C9 C8 . . . . -177.72(17) no
    N2 C9 C10 C11 . . . . -0.2(4) no
    C8 C9 C10 C11 . . . . 178.8(2) no
    Cu1 O3 C11 C10 . . . . -0.6(3) no
    Cu1 O3 C11 C12 . . . . 179.99(15) no
    C9 C10 C11 O3 . . . . -0.1(4) no
    C9 C10 C11 C12 . . . . 179.3(2) no
    N4 N3 C14 C15 . . . . -0.2(2) no
    Cu1 N3 C14 C15 . . . . 177.20(16) no
    N4 N3 C14 C13 . . . . -179.68(19) no
    Cu1 N3 C14 C13 . . . . -2.3(3) no
    N3 C14 C15 C16 . . . . 0.2(3) no
    C13 C14 C15 C16 . . . . 179.6(2) no
    N3 N4 C16 C15 . . . . 0.0(2) no
    N3 N4 C16 C17 . . . . 179.5(2) no
    C14 C15 C16 N4 . . . . -0.1(2) no
    C14 C15 C16 C17 . . . . -179.6(2) no
data_global
_journal_date_recd_electronic     2006-11-02
_journal_date_accepted     2007-01-04
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2007
_journal_volume     63
_journal_issue      2
_journal_page_first     m443
_journal_page_last     m444
_journal_paper_category     EM
_journal_coeditor_code     WK2036
_publ_contact_author_name     'Professor Liu Shixiong'
_publ_contact_author_address
;
Department of Chemistry
Fuzhou University
Fuzhou 350002
P.R.China
;
_publ_contact_author_email     shixiongliu@yahoo.com
_publ_contact_author_fax     '86 591 83729860'
_publ_contact_author_phone     '86 591 83729860'
_publ_section_title
;
(3,5-Dimethyl-1H-pyrazole-κN²)(4-oxidopent-3-en-2-one
2-hydroxybenzoylhydrazonatoκ²N,O)copper(II)
;
loop_
    _publ_author_name
    _publ_author_footnote
    _publ_author_address
    'Du, Kang-Kai' .
;
Department of Chemistry
Fuzhou University
Fuzhou, Fujian 350002
People's Republic of China
and
College of Materials
Huaqiao University
Quanzhou, Fujian 362021
People's Republic of China
;
    'Liu, Shi-Xiong' .
;
Department of Chemistry
Fuzhou University
Fuzhou, Fujian 350002
People's Republic of China
;
