##############################################################################
###                                                                        ###
###        Electronic paper (Acta Crystallographica Section E)             ###
###                                                                        ###
##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in Acta     #
# Crystallographica Section E. It conforms to the requirements of Notes      #
# for Authors for Section E, and has been peer reviewed under the auspices   #
# of the IUCr Commission on Journals.                                        #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.1.    #
#                                                                            #
# Software is freely available for graphical display of the structure(s) in  #
# this CIF.  For information consult the CIF home page http://www.iucr.org/  #
# cif/home.html                                                              #
#                                                                            #
#            Copyright International Union of Crystallography                #
#                                                                            #
##############################################################################
                                             
data_I
_audit_creation_method     SHELXL-97
_chemical_name_systematic
;
Diethyl 2-[(4-chlorophenylamino)(2,6-dichlorophenyl)methyl]malonate
;
_chemical_name_common     ?
_chemical_formula_moiety     'C20 H20 Cl3 N O4'
_chemical_formula_sum     'C20 H20 Cl3 N O4'
_chemical_formula_iupac     'C20 H20 Cl3 N O4'
_chemical_formula_weight     444.72
_chemical_melting_point     ?
_symmetry_cell_setting     triclinic
_symmetry_space_group_name_H-M     'P -1'
_symmetry_space_group_name_Hall     '-P 1'
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, -y, -z'
_cell_length_a     8.4561(9)
_cell_length_b     11.6301(12)
_cell_length_c     11.9854(12)
_cell_angle_alpha     65.401(2)
_cell_angle_beta     84.735(2)
_cell_angle_gamma     86.205(2)
_cell_volume     1066.70(19)
_cell_formula_units_Z     2
_cell_measurement_reflns_used     2471
_cell_measurement_theta_min     2.4
_cell_measurement_theta_max     26.6
_cell_measurement_temperature     293(2)
_exptl_crystal_description     plate
_exptl_crystal_colour     colorless
_exptl_crystal_size_max     0.50
_exptl_crystal_size_mid     0.33
_exptl_crystal_size_min     0.13
_exptl_crystal_density_diffrn     1.385
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     460
_exptl_absorpt_coefficient_mu     0.455
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details     '(SADABS; Sheldrick, 1996)'
_exptl_absorpt_correction_T_min     0.756
_exptl_absorpt_correction_T_max     0.942
_exptl_special_details
;
IR
(KBr,cm⁻¹): 3375, 1750, 1730, 1601, 1495, 1291, 1268, 1252; ¹H NMR (500
MHz, CDCl₃): δ 7.25--7.24 (m, 2H), 7.10--7.05 (m, 3H), 6.74
(d, J = 8.8 Hz, 2H), 6.13 (t, J = 11.1 Hz, 1H),
4.91 (d, J = 11.3 Hz, 1H), 4.71 (d, J = 11.3 Hz,
1H), 4.24--4.20 (m, 2H), 4.01--3.97 (m, 2H), 1.23 (t,
J = 7.1 Hz, 3H), 1.04 (t, J = 7.1 Hz, 3H); ¹³C NMR (125
MHz, CDCl₃): δ 167.3, 166.3, 144.8, 137.8, 134.0, 129.7, 129.2, 123.8,
116.0, 62.2, 61.9, 56.1, 54.5, 14.2, 13.8; m.p. 356--357 K; MS (ESI):
m/z 466 ([M + Na]⁺).
;
_diffrn_ambient_temperature     293(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'fine-focus sealed tube'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type     'Bruker SMART CCD area-detector'
_diffrn_measurement_method     'φ and ω'
_diffrn_detector_area_resol_mean     10
_diffrn_reflns_number     6304
_diffrn_reflns_av_R_equivalents     0.063
_diffrn_reflns_av_sigmaI/netI     0.058
_diffrn_reflns_theta_min     1.9
_diffrn_reflns_theta_max     27.0
_diffrn_reflns_theta_full     27.0
_diffrn_measured_fraction_theta_max     0.97
_diffrn_measured_fraction_theta_full     0.97
_diffrn_reflns_limit_h_min     -10
_diffrn_reflns_limit_h_max     10
_diffrn_reflns_limit_k_min     -14
_diffrn_reflns_limit_k_max     12
_diffrn_reflns_limit_l_min     -14
_diffrn_reflns_limit_l_max     15
_diffrn_standards_number     0
_diffrn_standards_interval_count     0
_diffrn_standards_interval_time     0
_diffrn_standards_decay_%     ?
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
_reflns_number_total     4524
_reflns_number_gt     3340
_reflns_threshold_expression     I>2σ(I)
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.059
_refine_ls_R_factor_gt     0.045
_refine_ls_wR_factor_gt     0.115
_refine_ls_wR_factor_ref     0.122
_refine_ls_goodness_of_fit_ref     0.949
_refine_ls_restrained_S_all     0.949
_refine_ls_number_reflns     4524
_refine_ls_number_parameters     267
_refine_ls_number_restraints     0
_refine_ls_hydrogen_treatment     mixed
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
                 'calc w=1/[σ²(Fo²)+(0.0659P)²] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.005
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.29
_refine_diff_density_min     -0.29
_refine_ls_extinction_method     none
_refine_ls_extinction_coef     ?
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0061 0.0033
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Cl' 'Cl' 0.1484 0.1585
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'SMART (Bruker, 1998)'
_computing_cell_refinement     'SAINT (Bruker, 1998)'
_computing_data_reduction     'SAINT'
_computing_structure_solution     'SHELXS97 (Sheldrick, 1997)'
_computing_structure_refinement     'SHELXL97 (Sheldrick, 1997)'
_computing_molecular_graphics     'SHELXTL (Sheldrick, 1998)'
_computing_publication_material     'SHELXTL'
loop_
    _atom_site_type_symbol
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    Cl Cl1 -0.09944(10) 0.21103(8) 0.73580(6) 0.0954(3) Uani d . 1 . .
    Cl Cl2 0.36398(7) -0.01447(5) 0.30798(5) 0.06124(18) Uani d . 1 . .
    Cl Cl3 0.38975(7) 0.49828(5) 0.13740(6) 0.06584(19) Uani d . 1 . .
    O O1 -0.03001(17) 0.40342(13) -0.06239(14) 0.0592(4) Uani d . 1 . .
    O O2 -0.01139(14) 0.19603(12) 0.04964(12) 0.0461(3) Uani d . 1 . .
    O O3 0.4215(2) 0.17037(18) 0.01434(15) 0.0830(5) Uani d . 1 . .
    O O4 0.31162(16) 0.30812(14) -0.15262(12) 0.0550(4) Uani d . 1 . .
    N N1 0.10043(18) 0.32406(16) 0.21838(15) 0.0417(4) Uani d . 1 . .
    C C1 0.2175(2) 0.25324(17) 0.17394(16) 0.0379(4) Uani d . 1 . .
    C C2 0.2127(2) 0.31313(17) 0.03359(16) 0.0393(4) Uani d . 1 . .
    C C3 0.0436(2) 0.31215(17) 0.00029(16) 0.0401(4) Uani d . 1 . .
    C C4 0.3277(2) 0.25340(18) -0.03292(18) 0.0462(4) Uani d . 1 . .
    C C5 0.4201(3) 0.2643(2) -0.2290(2) 0.0697(7) Uani d . 1 . .
    H H5A 0.5291 0.2729 -0.2153 0.084 Uiso calc R 1 . .
    H H5B 0.4035 0.1757 -0.2080 0.084 Uiso calc R 1 . .
    C C6 0.3907(5) 0.3392(4) -0.3565(3) 0.1195(14) Uani d . 1 . .
    H H6A 0.2804 0.3360 -0.3679 0.124 Uiso calc R 1 . .
    H H6B 0.4545 0.3060 -0.4075 0.124 Uiso calc R 1 . .
    H H6C 0.4176 0.4253 -0.3789 0.124 Uiso calc R 1 . .
    C C7 -0.1784(2) 0.1852(2) 0.03393(19) 0.0493(5) Uani d . 1 . .
    H H7A -0.2003 0.2310 -0.0519 0.059 Uiso calc R 1 . .
    H H7B -0.2463 0.2208 0.0821 0.059 Uiso calc R 1 . .
    C C8 -0.2094(3) 0.0497(2) 0.0757(3) 0.0742(7) Uani d . 1 . .
    H H8A -0.1420 0.0155 0.0272 0.111 Uiso calc R 1 . .
    H H8B -0.3186 0.0400 0.0664 0.111 Uiso calc R 1 . .
    H H8C -0.1877 0.0054 0.1607 0.111 Uiso calc R 1 . .
    C C9 0.0606(2) 0.29514(17) 0.34081(16) 0.0394(4) Uani d . 1 . .
    C C10 0.0872(2) 0.17502(18) 0.43422(17) 0.0459(4) Uani d . 1 . .
    H H10 0.1391 0.1119 0.4149 0.055 Uiso calc R 1 . .
    C C11 0.0373(2) 0.1496(2) 0.55449(19) 0.0551(5) Uani d . 1 . .
    H H11 0.0551 0.0694 0.6160 0.066 Uiso calc R 1 . .
    C C12 -0.0386(3) 0.2421(2) 0.58361(19) 0.0589(6) Uani d . 1 . .
    C C13 -0.0662(3) 0.3604(2) 0.4940(2) 0.0582(5) Uani d . 1 . .
    H H13 -0.1187 0.4225 0.5145 0.070 Uiso calc R 1 . .
    C C14 -0.0162(2) 0.38733(19) 0.37332(19) 0.0516(5) Uani d . 1 . .
    H H14 -0.0340 0.4681 0.3129 0.062 Uiso calc R 1 . .
    C C15 0.3806(2) 0.24182(16) 0.22417(15) 0.0396(4) Uani d . 1 . .
    C C16 0.4509(2) 0.12340(18) 0.29078(17) 0.0458(4) Uani d . 1 . .
    C C17 0.5906(2) 0.1094(2) 0.3476(2) 0.0611(6) Uani d . 1 . .
    H H17 0.6328 0.0290 0.3926 0.073 Uiso calc R 1 . .
    C C18 0.6660(3) 0.2131(3) 0.3376(2) 0.0712(7) Uani d . 1 . .
    H H18 0.7595 0.2036 0.3762 0.085 Uiso calc R 1 . .
    C C19 0.6041(3) 0.3324(2) 0.2704(2) 0.0650(6) Uani d . 1 . .
    H H19 0.6565 0.4039 0.2616 0.078 Uiso calc R 1 . .
    C C20 0.4633(2) 0.34431(19) 0.21656(18) 0.0489(5) Uani d . 1 . .
    H H1 0.179(2) 0.1706(18) 0.2038(16) 0.039(5) Uiso d . 1 . .
    H H2 0.2372(19) 0.3953(17) 0.0028(15) 0.034(5) Uiso d . 1 . .
    H H3 0.087(2) 0.397(2) 0.174(2) 0.053(6) Uiso d . 1 . .
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    Cl1 C12 . 1.740(2) ?
    Cl2 C16 . 1.734(2) ?
    Cl3 C20 . 1.744(2) ?
    O1 C3 . 1.189(2) y
    O2 C3 . 1.326(2) y
    O2 C7 . 1.462(2) y
    O3 C4 . 1.187(2) y
    O4 C4 . 1.321(2) y
    O4 C5 . 1.454(2) y
    N1 C9 . 1.376(2) y
    N1 C1 . 1.450(2) y
    N1 H3 . 0.80(2) ?
    C1 C15 . 1.531(2) ?
    C1 C2 . 1.533(2) ?
    C1 H1 . 0.943(18) ?
    C2 C4 . 1.514(3) ?
    C2 C3 . 1.522(2) ?
    C2 H2 . 0.900(17) ?
    C5 C6 . 1.445(4) ?
    C5 H5A . 0.9700 ?
    C5 H5B . 0.9700 ?
    C6 H6A . 0.9600 ?
    C6 H6B . 0.9600 ?
    C6 H6C . 0.9600 ?
    C7 C8 . 1.476(3) ?
    C7 H7A . 0.9700 ?
    C7 H7B . 0.9700 ?
    C8 H8A . 0.9600 ?
    C8 H8B . 0.9600 ?
    C8 H8C . 0.9600 ?
    C9 C14 . 1.390(3) ?
    C9 C10 . 1.399(3) ?
    C10 C11 . 1.376(3) ?
    C10 H10 . 0.9300 ?
    C11 C12 . 1.368(3) ?
    C11 H11 . 0.9300 ?
    C12 C13 . 1.369(3) ?
    C13 C14 . 1.377(3) ?
    C13 H13 . 0.9300 ?
    C14 H14 . 0.9300 ?
    C15 C20 . 1.388(3) ?
    C15 C16 . 1.397(3) ?
    C16 C17 . 1.384(3) ?
    C17 C18 . 1.357(3) ?
    C17 H17 . 0.9300 ?
    C18 C19 . 1.378(4) ?
    C18 H18 . 0.9300 ?
    C19 C20 . 1.378(3) ?
    C19 H19 . 0.9300 ?
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    C3 O2 C7 . . 116.06(14) ?
    C4 O4 C5 . . 116.62(16) ?
    C9 N1 C1 . . 124.16(16) ?
    C9 N1 H3 . . 114.4(16) ?
    C1 N1 H3 . . 116.1(16) ?
    N1 C1 C15 . . 113.37(14) ?
    N1 C1 C2 . . 105.71(14) ?
    C15 C1 C2 . . 116.42(14) ?
    N1 C1 H1 . . 105.9(11) ?
    C15 C1 H1 . . 106.9(10) ?
    C2 C1 H1 . . 107.9(11) ?
    C4 C2 C3 . . 110.60(15) ?
    C4 C2 C1 . . 114.79(15) ?
    C3 C2 C1 . . 109.26(14) ?
    C4 C2 H2 . . 106.0(11) ?
    C3 C2 H2 . . 105.5(11) ?
    C1 C2 H2 . . 110.3(11) ?
    O1 C3 O2 . . 124.09(17) ?
    O1 C3 C2 . . 124.59(17) ?
    O2 C3 C2 . . 111.33(15) ?
    O3 C4 O4 . . 124.03(19) ?
    O3 C4 C2 . . 125.40(19) ?
    O4 C4 C2 . . 110.56(16) ?
    C6 C5 O4 . . 108.7(2) ?
    C6 C5 H5A . . 110.0 ?
    O4 C5 H5A . . 110.0 ?
    C6 C5 H5B . . 110.0 ?
    O4 C5 H5B . . 110.0 ?
    H5A C5 H5B . . 108.3 ?
    C5 C6 H6A . . 109.5 ?
    C5 C6 H6B . . 109.5 ?
    H6A C6 H6B . . 109.5 ?
    C5 C6 H6C . . 109.5 ?
    H6A C6 H6C . . 109.5 ?
    H6B C6 H6C . . 109.5 ?
    O2 C7 C8 . . 107.82(17) ?
    O2 C7 H7A . . 110.1 ?
    C8 C7 H7A . . 110.1 ?
    O2 C7 H7B . . 110.1 ?
    C8 C7 H7B . . 110.1 ?
    H7A C7 H7B . . 108.5 ?
    C7 C8 H8A . . 109.5 ?
    C7 C8 H8B . . 109.5 ?
    H8A C8 H8B . . 109.5 ?
    C7 C8 H8C . . 109.5 ?
    H8A C8 H8C . . 109.5 ?
    H8B C8 H8C . . 109.5 ?
    N1 C9 C14 . . 118.80(17) ?
    N1 C9 C10 . . 123.00(17) ?
    C14 C9 C10 . . 118.14(17) ?
    C11 C10 C9 . . 120.48(19) ?
    C11 C10 H10 . . 119.8 ?
    C9 C10 H10 . . 119.8 ?
    C12 C11 C10 . . 120.0(2) ?
    C12 C11 H11 . . 120.0 ?
    C10 C11 H11 . . 120.0 ?
    C11 C12 C13 . . 120.66(19) ?
    C11 C12 Cl1 . . 120.21(18) ?
    C13 C12 Cl1 . . 119.14(18) ?
    C12 C13 C14 . . 119.9(2) ?
    C12 C13 H13 . . 120.1 ?
    C14 C13 H13 . . 120.1 ?
    C13 C14 C9 . . 120.8(2) ?
    C13 C14 H14 . . 119.6 ?
    C9 C14 H14 . . 119.6 ?
    C20 C15 C16 . . 115.04(16) ?
    C20 C15 C1 . . 123.89(16) ?
    C16 C15 C1 . . 120.88(16) ?
    C17 C16 C15 . . 122.36(19) ?
    C17 C16 Cl2 . . 116.67(15) ?
    C15 C16 Cl2 . . 120.96(14) ?
    C18 C17 C16 . . 120.0(2) ?
    C18 C17 H17 . . 120.0 ?
    C16 C17 H17 . . 120.0 ?
    C17 C18 C19 . . 120.1(2) ?
    C17 C18 H18 . . 119.9 ?
    C19 C18 H18 . . 119.9 ?
    C20 C19 C18 . . 119.0(2) ?
    C20 C19 H19 . . 120.5 ?
    C18 C19 H19 . . 120.5 ?
    C19 C20 C15 . . 123.44(19) ?
    C19 C20 Cl3 . . 116.13(16) ?
    C15 C20 Cl3 . . 120.42(14) ?
loop_
    _geom_torsion_atom_site_label_1
    _geom_torsion_atom_site_label_2
    _geom_torsion_atom_site_label_3
    _geom_torsion_atom_site_label_4
    _geom_torsion_site_symmetry_1
    _geom_torsion_site_symmetry_2
    _geom_torsion_site_symmetry_3
    _geom_torsion_site_symmetry_4
    _geom_torsion
    _geom_torsion_publ_flag
    C9 N1 C1 C15 . . . . -55.5(2) ?
    C9 N1 C1 C2 . . . . 175.84(16) ?
    N1 C1 C2 C4 . . . . 179.79(15) ?
    C15 C1 C2 C4 . . . . 52.9(2) ?
    N1 C1 C2 C3 . . . . -55.32(18) ?
    C15 C1 C2 C3 . . . . 177.81(14) ?
    C7 O2 C3 O1 . . . . -6.2(3) ?
    C7 O2 C3 C2 . . . . 174.14(14) ?
    C4 C2 C3 O1 . . . . -108.6(2) ?
    C1 C2 C3 O1 . . . . 124.1(2) ?
    C4 C2 C3 O2 . . . . 70.99(19) ?
    C1 C2 C3 O2 . . . . -56.30(19) ?
    C5 O4 C4 O3 . . . . -1.7(3) ?
    C5 O4 C4 C2 . . . . 177.18(17) ?
    C3 C2 C4 O3 . . . . -127.4(2) ?
    C1 C2 C4 O3 . . . . -3.2(3) ?
    C3 C2 C4 O4 . . . . 53.7(2) ?
    C1 C2 C4 O4 . . . . 177.93(15) ?
    C4 O4 C5 C6 . . . . -176.9(2) ?
    C3 O2 C7 C8 . . . . 170.57(18) ?
    C1 N1 C9 C14 . . . . 161.59(17) ?
    C1 N1 C9 C10 . . . . -21.5(3) ?
    N1 C9 C10 C11 . . . . -176.50(18) ?
    C14 C9 C10 C11 . . . . 0.5(3) ?
    C9 C10 C11 C12 . . . . -0.2(3) ?
    C10 C11 C12 C13 . . . . 0.2(3) ?
    C10 C11 C12 Cl1 . . . . -179.08(15) ?
    C11 C12 C13 C14 . . . . -0.6(3) ?
    Cl1 C12 C13 C14 . . . . 178.78(17) ?
    C12 C13 C14 C9 . . . . 0.8(3) ?
    N1 C9 C14 C13 . . . . 176.32(18) ?
    C10 C9 C14 C13 . . . . -0.8(3) ?
    N1 C1 C15 C20 . . . . -53.1(2) ?
    C2 C1 C15 C20 . . . . 69.9(2) ?
    N1 C1 C15 C16 . . . . 121.67(19) ?
    C2 C1 C15 C16 . . . . -115.36(19) ?
    C20 C15 C16 C17 . . . . 1.6(3) ?
    C1 C15 C16 C17 . . . . -173.59(17) ?
    C20 C15 C16 Cl2 . . . . -179.39(13) ?
    C1 C15 C16 Cl2 . . . . 5.4(2) ?
    C15 C16 C17 C18 . . . . -1.3(3) ?
    Cl2 C16 C17 C18 . . . . 179.62(19) ?
    C16 C17 C18 C19 . . . . -0.3(4) ?
    C17 C18 C19 C20 . . . . 1.6(4) ?
    C18 C19 C20 C15 . . . . -1.2(4) ?
    C18 C19 C20 Cl3 . . . . 178.00(19) ?
    C16 C15 C20 C19 . . . . -0.3(3) ?
    C1 C15 C20 C19 . . . . 174.72(19) ?
    C16 C15 C20 Cl3 . . . . -179.52(14) ?
    C1 C15 C20 Cl3 . . . . -4.5(3) ?
loop_
    _geom_hbond_atom_site_label_D
    _geom_hbond_atom_site_label_H
    _geom_hbond_atom_site_label_A
    _geom_hbond_site_symmetry_A
    _geom_hbond_distance_DH
    _geom_hbond_distance_HA
    _geom_hbond_distance_DA
    _geom_hbond_angle_DHA
    N1 H3 O1 2_565 0.80(2) 2.19(2) 2.986(2) 174(2)
data_global
_journal_date_recd_electronic     2006-04-18
_journal_date_accepted     2006-04-28
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2006
_journal_volume     62
_journal_issue      6
_journal_page_first     o2212
_journal_page_last     o2213
_journal_paper_category     EO
_journal_coeditor_code     XU2032
_publ_contact_author_name     'Dr. Lei, Ming'
_publ_contact_author_address
;
Department of Chemistry
Zhejiang University
P. R. China
;
_publ_contact_author_email     swgwxn@zju.edu.cn
_publ_section_title
;
Diethyl 2-[(4-chlorophenylamino)(2,6-dichlorophenyl)methyl]malonate
;
loop_
    _publ_author_name
    _publ_author_address
    'Shou, Wang-Ge'
;
Department of Chemistry
Zhejiang University
People's Republic of China
;
    'Yang, Yun-Yun'
;
Department of Chemistry
Zhejiang University
People's Republic of China
;
    'Lei, Ming'
;
Department of Chemistry
Zhejiang University
People's Republic of China
;
