##############################################################################
###                                                                        ###
###        Electronic paper (Acta Crystallographica Section E)             ###
###                                                                        ###
##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in Acta     #
# Crystallographica Section E. It conforms to the requirements of Notes      #
# for Authors for Section E, and has been peer reviewed under the auspices   #
# of the IUCr Commission on Journals.                                        #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.1.    #
#                                                                            #
# Software is freely available for graphical display of the structure(s) in  #
# this CIF.  For information consult the CIF home page http://www.iucr.org/  #
# cif/home.html                                                              #
#                                                                            #
#            Copyright International Union of Crystallography                #
#                                                                            #
##############################################################################
                                             
data_I
_audit_creation_method     SHELXL-97
_chemical_name_systematic
;
 Dichloro-bis(1,10-phenanthroline)manganese(II) salicylaldoxime
;
_chemical_name_common     ?
_chemical_formula_moiety     'C24 H16 Cl2 Mn N4, C7 H7 N O2'
_chemical_formula_sum     'C31 H23 Cl2 Mn N5 O2'
_chemical_formula_iupac     '[Mn Cl2 (C12 H8 N2)2], C7 H7 N O2'
_chemical_formula_weight     623.38
_chemical_melting_point     ?
_symmetry_cell_setting     Triclinic
_symmetry_space_group_name_H-M     'P -1'
_symmetry_space_group_name_Hall     '-P 1'
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, -y, -z'
_cell_length_a     10.7688(6)
_cell_length_b     10.8408(6)
_cell_length_c     13.3473(7)
_cell_angle_alpha     89.0320(10)
_cell_angle_beta     66.4770(10)
_cell_angle_gamma     88.2760(10)
_cell_volume     1428.04(13)
_cell_formula_units_Z     2
_cell_measurement_reflns_used     4106
_cell_measurement_theta_min     1.66
_cell_measurement_theta_max     25.05
_cell_measurement_temperature     293(2)
_exptl_crystal_description     'prism'
_exptl_crystal_colour     'brown'
_exptl_crystal_size_max     0.56
_exptl_crystal_size_mid     0.50
_exptl_crystal_size_min     0.40
_exptl_crystal_density_diffrn     1.450
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     638
_exptl_absorpt_coefficient_mu     0.688
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details     '(SADABS; Sheldrick, 1996)'
_exptl_absorpt_correction_T_min     0.8070
_exptl_absorpt_correction_T_max     1.0000
_exptl_special_details
;
 ?
;
_diffrn_ambient_temperature     293(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'fine-focus sealed tube'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type     'Siemens SMART CCD area-detector'
_diffrn_measurement_method     'φ and ω scans'
_diffrn_detector_area_resol_mean     ?
_diffrn_reflns_number     7520
_diffrn_reflns_av_R_equivalents     0.0201
_diffrn_reflns_av_sigmaI/netI     0.0364
_diffrn_reflns_theta_min     1.66
_diffrn_reflns_theta_max     25.05
_diffrn_reflns_theta_full     25.05
_diffrn_measured_fraction_theta_max     0.984
_diffrn_measured_fraction_theta_full     0.984
_diffrn_reflns_limit_h_min     -11
_diffrn_reflns_limit_h_max     12
_diffrn_reflns_limit_k_min     -12
_diffrn_reflns_limit_k_max     12
_diffrn_reflns_limit_l_min     -15
_diffrn_reflns_limit_l_max     15
_diffrn_standards_number     0
_diffrn_standards_interval_count     none
_diffrn_standards_interval_time     none
_diffrn_standards_decay_%     0
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
_reflns_number_total     4964
_reflns_number_gt     4019
_reflns_threshold_expression     'I > 2σ(I)'
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_gt     0.0473
_refine_ls_wR_factor_gt     0.1050
_refine_ls_wR_factor_ref     0.1169
_refine_ls_goodness_of_fit_ref     1.077
_refine_ls_restrained_S_all     1.077
_refine_ls_number_reflns     4964
_refine_ls_number_parameters     370
_refine_ls_number_restraints     0
_refine_ls_hydrogen_treatment     constr
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
         'calc w=1/[σ²(Fo²)+(0.0427P)²+1.3089P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     <0.001
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.288
_refine_diff_density_min     -0.385
_refine_ls_extinction_method     none
_refine_ls_extinction_coef     ?
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0061 0.0033
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Mn' 'Mn' 0.3368 0.7283
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Cl' 'Cl' 0.1484 0.1585
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'SMART (Siemens, 1994)'
_computing_cell_refinement     'SMART & SAINT (Siemens, 1994)'
_computing_data_reduction     'XPREP in SHELXTL (Siemens, 1994)'
_computing_structure_solution     'SHELXTL'
_computing_structure_refinement     'SHELXTL'
_computing_molecular_graphics     'SHELXTL'
_computing_publication_material     'SHELXTL'
loop_
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    _atom_site_type_symbol
    Mn1 0.72704(4) 0.35644(4) 0.19789(4) 0.03710(15) Uani d . 1 . . Mn
    Cl1 0.90860(9) 0.36296(10) 0.26551(8) 0.0665(3) Uani d . 1 . . Cl
    Cl2 0.73667(10) 0.57094(7) 0.14043(7) 0.0537(2) Uani d . 1 . . Cl
    O1 1.0494(4) -0.1195(3) -0.3678(2) 0.1015(11) Uani d . 1 . . O
    H1 1.0250 -0.1812 -0.3292 0.152 Uiso calc R 1 . . H
    O2 1.2553(3) -0.3039(3) -0.6379(2) 0.0797(8) Uani d . 1 . . O
    H2 1.2025 -0.2853 -0.5759 0.120 Uiso calc R 1 . . H
    N1 0.8352(3) 0.2834(2) 0.0248(2) 0.0467(6) Uani d . 1 . . N
    N2 0.7230(3) 0.1436(2) 0.2083(2) 0.0513(7) Uani d . 1 . . N
    N3 0.5208(2) 0.3535(2) 0.1820(2) 0.0412(6) Uani d . 1 . . N
    N4 0.5577(2) 0.3520(2) 0.37113(19) 0.0373(6) Uani d . 1 . . N
    N5 1.1322(4) -0.1546(3) -0.4742(3) 0.0733(9) Uani d . 1 . . N
    C1 0.8927(4) 0.3521(4) -0.0639(3) 0.0594(9) Uani d . 1 . . C
    H1A 0.8963 0.4369 -0.0565 0.071 Uiso calc R 1 . . H
    C2 0.9482(4) 0.3006(5) -0.1689(3) 0.0779(12) Uani d . 1 . . C
    H2A 0.9873 0.3506 -0.2303 0.093 Uiso calc R 1 . . H
    C3 0.9439(4) 0.1757(5) -0.1795(3) 0.0788(13) Uani d . 1 . . C
    H3 0.9793 0.1409 -0.2488 0.095 Uiso calc R 1 . . H
    C4 0.8875(4) 0.1004(4) -0.0883(3) 0.0644(10) Uani d . 1 . . C
    C5 0.8330(3) 0.1588(3) 0.0139(3) 0.0493(8) Uani d . 1 . . C
    C6 0.8855(5) -0.0331(5) -0.0916(4) 0.0824(14) Uani d . 1 . . C
    H6 0.9208 -0.0725 -0.1590 0.099 Uiso calc R 1 . . H
    C7 0.8342(5) -0.1013(4) -0.0006(4) 0.0818(13) Uani d . 1 . . C
    H7 0.8355 -0.1868 -0.0058 0.098 Uiso calc R 1 . . H
    C8 0.7780(4) -0.0453(3) 0.1039(4) 0.0639(10) Uani d . 1 . . C
    C9 0.7754(3) 0.0848(3) 0.1110(3) 0.0499(8) Uani d . 1 . . C
    C10 0.7230(5) -0.1123(4) 0.2023(4) 0.0814(13) Uani d . 1 . . C
    H10 0.7224 -0.1981 0.2010 0.098 Uiso calc R 1 . . H
    C11 0.6711(5) -0.0524(4) 0.2984(4) 0.0854(14) Uani d . 1 . . C
    H11 0.6347 -0.0961 0.3639 0.102 Uiso calc R 1 . . H
    C12 0.6729(4) 0.0756(3) 0.2983(3) 0.0703(11) Uani d . 1 . . C
    H12 0.6368 0.1159 0.3652 0.084 Uiso calc R 1 . . H
    C13 0.5031(3) 0.3579(3) 0.0894(3) 0.0495(8) Uani d . 1 . . C
    H13 0.5791 0.3515 0.0240 0.059 Uiso calc R 1 . . H
    C14 0.3767(4) 0.3717(4) 0.0850(3) 0.0575(9) Uani d . 1 . . C
    H14 0.3693 0.3753 0.0180 0.069 Uiso calc R 1 . . H
    C15 0.2644(4) 0.3798(3) 0.1793(3) 0.0558(9) Uani d . 1 . . C
    H15 0.1792 0.3877 0.1773 0.067 Uiso calc R 1 . . H
    C16 0.2772(3) 0.3761(3) 0.2803(3) 0.0461(7) Uani d . 1 . . C
    C17 0.4090(3) 0.3628(3) 0.2770(2) 0.0373(7) Uani d . 1 . . C
    C18 0.1645(3) 0.3829(4) 0.3837(3) 0.0591(9) Uani d . 1 . . C
    H18 0.0772 0.3910 0.3861 0.071 Uiso calc R 1 . . H
    C19 0.1828(3) 0.3776(3) 0.4780(3) 0.0569(9) Uani d . 1 . . C
    H19 0.1078 0.3820 0.5443 0.068 Uiso calc R 1 . . H
    C20 0.3154(3) 0.3653(3) 0.4778(2) 0.0438(7) Uani d . 1 . . C
    C21 0.4288(3) 0.3595(3) 0.3779(2) 0.0369(6) Uani d . 1 . . C
    C22 0.3394(3) 0.3603(3) 0.5743(3) 0.0487(8) Uani d . 1 . . C
    H22 0.2671 0.3642 0.6422 0.058 Uiso calc R 1 . . H
    C23 0.4684(3) 0.3498(3) 0.5676(2) 0.0475(8) Uani d . 1 . . C
    H23 0.4854 0.3445 0.6306 0.057 Uiso calc R 1 . . H
    C24 0.5751(3) 0.3471(3) 0.4649(2) 0.0441(7) Uani d . 1 . . C
    H24 0.6631 0.3416 0.4613 0.053 Uiso calc R 1 . . H
    C25 1.1731(4) -0.0634(4) -0.5397(4) 0.0743(12) Uani d . 1 . . C
    H25 1.1448 0.0163 -0.5146 0.089 Uiso calc R 1 . . H
    C26 1.2638(4) -0.0828(4) -0.6535(3) 0.0627(10) Uani d . 1 . . C
    C27 1.3176(5) 0.0188(5) -0.7206(4) 0.0877(14) Uani d . 1 . . C
    H27 1.2924 0.0979 -0.6928 0.105 Uiso calc R 1 . . H
    C28 1.4068(6) 0.0038(6) -0.8270(5) 0.1051(18) Uani d . 1 . . C
    H28 1.4412 0.0723 -0.8713 0.126 Uiso calc R 1 . . H
    C29 1.4453(5) -0.1134(6) -0.8677(4) 0.0969(16) Uani d . 1 . . C
    H29 1.5070 -0.1237 -0.9396 0.116 Uiso calc R 1 . . H
    C30 1.3944(5) -0.2142(5) -0.8043(3) 0.0798(12) Uani d . 1 . . C
    H30 1.4211 -0.2928 -0.8332 0.096 Uiso calc R 1 . . H
    C31 1.3026(4) -0.2003(4) -0.6966(3) 0.0617(10) Uani d . 1 . . C
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    Mn1 N1 . 2.275(3) yes
    Mn1 N4 . 2.304(2) yes
    Mn1 N2 . 2.310(3) yes
    Mn1 N3 . 2.315(2) yes
    Mn1 Cl2 . 2.4285(9) yes
    Mn1 Cl1 . 2.4619(9) yes
    N3 C13 . 1.323(4) no
    N3 C17 . 1.359(4) no
    N4 C24 . 1.337(4) no
    N4 C21 . 1.355(4) no
    C21 C20 . 1.404(4) no
    C21 C17 . 1.445(4) no
    N2 C12 . 1.324(5) no
    N2 C9 . 1.354(4) no
    C17 C16 . 1.405(4) no
    C20 C22 . 1.411(4) no
    C20 C19 . 1.429(5) no
    C24 C23 . 1.394(4) no
    C24 H24 . 0.93 no
    C16 C15 . 1.409(5) no
    C16 C18 . 1.430(5) no
    N1 C1 . 1.325(4) no
    N1 C5 . 1.363(4) no
    C23 C22 . 1.358(5) no
    C23 H23 . 0.93 no
    O2 C31 . 1.349(5) no
    O2 H2 . 0.82 no
    C9 C8 . 1.414(5) no
    C9 C5 . 1.435(5) no
    C22 H22 . 0.93 no
    C4 C3 . 1.388(6) no
    C4 C5 . 1.405(5) no
    C4 C6 . 1.450(6) no
    C13 C14 . 1.388(5) no
    C13 H13 . 0.93 no
    C8 C10 . 1.406(6) no
    C8 C7 . 1.418(6) no
    C31 C30 . 1.389(6) no
    C31 C26 . 1.389(5) no
    C15 C14 . 1.355(5) no
    C15 H15 . 0.93 no
    C18 C19 . 1.349(5) no
    C18 H18 . 0.93 no
    C19 H19 . 0.93 no
    C14 H14 . 0.93 no
    C11 C10 . 1.347(6) no
    C11 C12 . 1.389(5) no
    C11 H11 . 0.93 no
    N5 C25 . 1.275(5) no
    N5 O1 . 1.394(4) no
    C1 C2 . 1.404(5) no
    C1 H1A . 0.93 no
    O1 H1 . 0.82 no
    C26 C27 . 1.393(6) no
    C26 C25 . 1.455(6) no
    C12 H12 . 0.93 no
    C25 H25 . 0.93 no
    C2 C3 . 1.367(6) no
    C2 H2A . 0.93 no
    C6 C7 . 1.337(7) no
    C6 H6 . 0.93 no
    C3 H3 . 0.93 no
    C7 H7 . 0.93 no
    C30 C29 . 1.358(7) no
    C30 H30 . 0.93 no
    C27 C28 . 1.369(7) no
    C27 H27 . 0.93 no
    C29 C28 . 1.376(7) no
    C29 H29 . 0.93 no
    C28 H28 . 0.93 no
    C10 H10 . 0.93 no
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    N1 Mn1 N4 . . 152.68(9) yes
    N1 Mn1 N2 . . 72.65(10) yes
    N4 Mn1 N2 . . 85.61(9) yes
    N1 Mn1 N3 . . 90.71(9) yes
    N4 Mn1 N3 . . 71.78(8) yes
    N2 Mn1 N3 . . 88.02(10) yes
    N1 Mn1 Cl2 . . 94.17(7) yes
    N4 Mn1 Cl2 . . 105.09(6) yes
    N2 Mn1 Cl2 . . 165.58(8) yes
    N3 Mn1 Cl2 . . 86.28(7) yes
    N1 Mn1 Cl1 . . 103.48(7) yes
    N4 Mn1 Cl1 . . 93.42(6) yes
    N2 Mn1 Cl1 . . 92.02(8) yes
    N3 Mn1 Cl1 . . 165.16(7) yes
    Cl2 Mn1 Cl1 . . 96.86(4) yes
    C13 N3 C17 . . 117.8(3) no
    C13 N3 Mn1 . . 125.8(2) yes
    C17 N3 Mn1 . . 115.87(18) yes
    C24 N4 C21 . . 117.4(3) no
    C24 N4 Mn1 . . 126.1(2) yes
    C21 N4 Mn1 . . 116.45(18) yes
    N4 C21 C20 . . 123.0(3) no
    N4 C21 C17 . . 117.7(3) no
    C20 C21 C17 . . 119.3(3) no
    C12 N2 C9 . . 118.0(3) no
    C12 N2 Mn1 . . 126.8(2) yes
    C9 N2 Mn1 . . 115.2(2) yes
    N3 C17 C16 . . 122.8(3) no
    N3 C17 C21 . . 117.7(3) no
    C16 C17 C21 . . 119.5(3) no
    C21 C20 C22 . . 117.3(3) no
    C21 C20 C19 . . 119.6(3) no
    C22 C20 C19 . . 123.1(3) no
    N4 C24 C23 . . 123.5(3) no
    N4 C24 H24 . . 118.2 no
    C23 C24 H24 . . 118.2 no
    C17 C16 C15 . . 116.9(3) no
    C17 C16 C18 . . 119.4(3) no
    C15 C16 C18 . . 123.7(3) no
    C1 N1 C5 . . 119.0(3) no
    C1 N1 Mn1 . . 125.4(2) yes
    C5 N1 Mn1 . . 115.6(2) yes
    C22 C23 C24 . . 119.0(3) no
    C22 C23 H23 . . 120.5 no
    C24 C23 H23 . . 120.5 no
    C31 O2 H2 . . 109.5 no
    N2 C9 C8 . . 121.8(3) no
    N2 C9 C5 . . 117.8(3) no
    C8 C9 C5 . . 120.4(3) no
    C23 C22 C20 . . 119.7(3) no
    C23 C22 H22 . . 120.1 no
    C20 C22 H22 . . 120.1 no
    C3 C4 C5 . . 116.9(4) no
    C3 C4 C6 . . 124.5(4) no
    C5 C4 C6 . . 118.6(4) no
    N3 C13 C14 . . 123.3(3) no
    N3 C13 H13 . . 118.4 no
    C14 C13 H13 . . 118.4 no
    N1 C5 C4 . . 122.5(4) no
    N1 C5 C9 . . 118.5(3) no
    C4 C5 C9 . . 119.0(3) no
    C10 C8 C9 . . 117.4(4) no
    C10 C8 C7 . . 123.5(4) no
    C9 C8 C7 . . 119.0(4) no
    O2 C31 C30 . . 117.5(4) no
    O2 C31 C26 . . 122.7(4) no
    C30 C31 C26 . . 119.8(4) no
    C14 C15 C16 . . 119.7(3) no
    C14 C15 H15 . . 120.1 no
    C16 C15 H15 . . 120.1 no
    C19 C18 C16 . . 121.1(3) no
    C19 C18 H18 . . 119.4 no
    C16 C18 H18 . . 119.4 no
    C18 C19 C20 . . 121.1(3) no
    C18 C19 H19 . . 119.5 no
    C20 C19 H19 . . 119.5 no
    C15 C14 C13 . . 119.5(3) no
    C15 C14 H14 . . 120.3 no
    C13 C14 H14 . . 120.3 no
    C10 C11 C12 . . 119.0(4) no
    C10 C11 H11 . . 120.5 no
    C12 C11 H11 . . 120.5 no
    C25 N5 O1 . . 113.2(4) no
    N1 C1 C2 . . 121.9(4) no
    N1 C1 H1A . . 119.1 no
    C2 C1 H1A . . 119.1 no
    N5 O1 H1 . . 109.5 no
    C31 C26 C27 . . 118.6(4) no
    C31 C26 C25 . . 121.9(4) no
    C27 C26 C25 . . 119.5(4) no
    N2 C12 C11 . . 123.7(4) no
    N2 C12 H12 . . 118.1 no
    C11 C12 H12 . . 118.1 no
    N5 C25 C26 . . 120.7(4) no
    N5 C25 H25 . . 119.7 no
    C26 C25 H25 . . 119.7 no
    C3 C2 C1 . . 118.9(4) no
    C3 C2 H2A . . 120.5 no
    C1 C2 H2A . . 120.5 no
    C7 C6 C4 . . 121.8(4) no
    C7 C6 H6 . . 119.1 no
    C4 C6 H6 . . 119.1 no
    C2 C3 C4 . . 120.9(4) no
    C2 C3 H3 . . 119.6 no
    C4 C3 H3 . . 119.6 no
    C6 C7 C8 . . 121.1(4) no
    C6 C7 H7 . . 119.4 no
    C8 C7 H7 . . 119.4 no
    C29 C30 C31 . . 120.2(5) no
    C29 C30 H30 . . 119.9 no
    C31 C30 H30 . . 119.9 no
    C28 C27 C26 . . 121.1(5) no
    C28 C27 H27 . . 119.5 no
    C26 C27 H27 . . 119.5 no
    C30 C29 C28 . . 120.9(5) no
    C30 C29 H29 . . 119.5 no
    C28 C29 H29 . . 119.5 no
    C27 C28 C29 . . 119.4(5) no
    C27 C28 H28 . . 120.3 no
    C29 C28 H28 . . 120.3 no
    C11 C10 C8 . . 120.0(4) no
    C11 C10 H10 . . 120.0 no
    C8 C10 H10 . . 120.0 no
loop_
    _geom_hbond_atom_site_label_D
    _geom_hbond_atom_site_label_H
    _geom_hbond_atom_site_label_A
    _geom_hbond_site_symmetry_A
    _geom_hbond_distance_DH
    _geom_hbond_distance_HA
    _geom_hbond_distance_DA
    _geom_hbond_angle_DHA
    O2 H2 N5 . 0.82 1.90 2.613(4) 145
    O1 H1 Cl1 2_755 0.82 2.34 3.055(3) 147
data_global
_journal_date_recd_electronic     2004-02-24
_journal_date_accepted     2004-03-05
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2004
_journal_volume     60
_journal_issue      4
_journal_page_first     m390
_journal_page_last     m391
_journal_paper_category     EM
_publ_contact_author_name     'Yuan-Gen Yao'
_publ_contact_author_address
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  the Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  P. R. China
;
_publ_contact_author_email     yyg@ms.fjirsm.ac.cn
_publ_contact_author_fax     '86-591-3714946'
_publ_contact_author_phone     '86-591-3711523'
_publ_section_title
;
Dichlorobis(1,10-phenanthroline)manganese(II) salicylaldoxime solvate
;
loop_
    _publ_author_name
    _publ_author_address
    'E Yang'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Jian Zhang'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Yu-Biao Chen'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Yao Kang'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Ye-Yan Qin'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Zhaoji Li'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Jian-Kai Cheng'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Rui-Feng Hu'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Yi-Hang Wen'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
    'Yuan-Gen Yao'
;
  The State Key Laboratory of Structural Chemistry,
  Fujian Institute of Research on the Structure of Matter,
  The Chinese Academy of Sciences,
  Fuzhou, Fujian 350002,
  People's Republic of China
;
