##############################################################################
###                                                                        ###
###        Electronic paper (Acta Crystallographica Section E)             ###
###                                                                        ###
##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in Acta     #
# Crystallographica Section E. It conforms to the requirements of Notes      #
# for Authors for Section E, and has been peer reviewed under the auspices   #
# of the IUCr Commission on Journals.                                        #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.1.    #
#                                                                            #
# Software is freely available for graphical display of the structure(s) in  #
# this CIF.  For information consult the CIF home page http://www.iucr.org/  #
# cif/home.html                                                              #
#                                                                            #
#            Copyright International Union of Crystallography                #
#                                                                            #
##############################################################################
                                             
data_global
_audit_creation_method     'from SHELXL97 CIF and IUCr SHELXL97-template'
_journal_date_recd_electronic     2002-11-13
_journal_date_accepted     2002-12-13
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2003
_journal_volume     59
_journal_issue      1
_journal_page_first     m29
_journal_page_last     m32
_journal_paper_category     EM
_publ_contact_author_name     'John H. Kaldis'
_publ_contact_author_address
;
Department of Chemistry
McMaster University
1280 Main Street West
Hamilton
Ontario L8S 4M1
Canada
;
_publ_contact_author_email     kaldisjh@mcmaster.ca
_publ_contact_author_fax     '905 522 2509'
_publ_contact_author_phone     '905 525 9140 ext.27699'
_publ_section_title
;
Anhydrous tris(dibenzoylmethanido)(o-phenanthroline)europium(III),
[Eu(DBM)₃.Phen]
;
loop_
    _publ_author_name
    _publ_author_footnote
    _publ_author_address
    'Ahmed, Moawia O.' .
;
Department of Chemical Engineering
National Tsing-Hua University
Hsinchu
30013 Taiwan
Republic of China
;
    'Liao, Jin-Long' .
;
Department of Chemical Engineering
National Tsing-Hua University
Hsinchu
30013 Taiwan
Republic of China
;
    'Chen, Xiwen' .
;
Department of Chemical Engineering
National Tsing-Hua University
Hsinchu
30013 Taiwan
Republic of China
;
    'Chen, Show-An' .
;
Department of Chemical Engineering
National Tsing-Hua University
Hsinchu
30013 Taiwan
Republic of China
;
    'Kaldis, John H.' .
;
Department of Chemistry
McMaster University
1280 Main Street West
Hamilton
Ontario L8S 4M1
Canada
;
data_I
_chemical_name_systematic
;
tris(dibenzoylmethanido)(o-phenanthroline)europium(III)
;
_chemical_name_common     ?
_chemical_formula_moiety     'C57 H41 Eu N2 O6'
_chemical_formula_sum     'C57 H41 Eu N2 O6'
_chemical_formula_iupac     '[Eu (C15 H11 O2)3 (C12 H8 N2)]'
_chemical_formula_weight     1001.88
_chemical_melting_point     '459-461 K'
_symmetry_cell_setting     Triclinic
_symmetry_space_group_name_H-M     'P -1'
_symmetry_space_group_name_Hall     '-P 1'
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, -y, -z'
_cell_length_a     16.275(6)
_cell_length_b     23.504(9)
_cell_length_c     31.712(12)
_cell_angle_alpha     103.844(6)
_cell_angle_beta     91.466(6)
_cell_angle_gamma     101.585(6)
_cell_volume     11504(7)
_cell_formula_units_Z     10
_cell_measurement_reflns_used     1016
_cell_measurement_theta_min     4.379
_cell_measurement_theta_max     54.789
_cell_measurement_temperature     153(2)
_exptl_crystal_description     parallelpiped
_exptl_crystal_colour     yellow
_exptl_crystal_size_max     0.24
_exptl_crystal_size_mid     0.15
_exptl_crystal_size_min     0.10
_exptl_crystal_density_diffrn     1.446
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     5080
_exptl_absorpt_coefficient_mu     1.418
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details     '(SADABS; Sheldrick, 2000)'
_exptl_absorpt_correction_T_min     0.8946
_exptl_absorpt_correction_T_max     1.0000
_exptl_special_details
;
X-ray crystallographic data were collected from a single crystal sample of 1
mounted on a glass fibre. Data were collected using a P4 Bruker
diffractometer, equipped with a Bruker SMART 1K CCD area detecor, using the
program SMART (Bruker, 2000), and a rotating anode, using graphite-
monochromated Mo-Kα radiation. The crystal-to-detector distance was 4.987 cm,
and the data collection was carried out in 512 × 512 pixel mode,
utilizing 2 × 2 pixel binning. The initial unit cell parameters were
determined by a least-squares fit of the angular settings of the strong
reflections, collected by a 12 ° scan in 40 frames over four different
sections of reciprocal space (160 frames in total).  Almost a complete sphere
of data was collected, to better than 0.8 Å resolution at 153 K.  Upon
completion of the data collection, the first 40 frames were recollected in
order to improve the decay correction analyses, which was determined to be
negligible.
;
_diffrn_ambient_temperature     153(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'rotating anode'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type     'Bruker SMART CCD area-detector'
_diffrn_measurement_method     'φ and ω'
_diffrn_reflns_number     102650
_diffrn_reflns_av_R_equivalents     0.0611
_diffrn_reflns_av_sigmaI/netI     0.1105
_diffrn_reflns_theta_min     1.26
_diffrn_reflns_theta_max     27.00
_diffrn_reflns_theta_full     27.00
_diffrn_measured_fraction_theta_max     0.990
_diffrn_measured_fraction_theta_full     0.990
_diffrn_reflns_limit_h_min     -20
_diffrn_reflns_limit_h_max     20
_diffrn_reflns_limit_k_min     -30
_diffrn_reflns_limit_k_max     29
_diffrn_reflns_limit_l_min     -36
_diffrn_reflns_limit_l_max     40
_diffrn_standards_number     0
_diffrn_standards_interval_count     none
_diffrn_standards_interval_time     ?
_diffrn_standards_decay_%     0
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
_reflns_number_total     49686
_reflns_number_gt     32004
_reflns_threshold_expression     I>2σ(I)
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.1023
_refine_ls_R_factor_gt     0.0504
_refine_ls_wR_factor_gt     0.0791
_refine_ls_wR_factor_ref     0.0945
_refine_ls_goodness_of_fit_ref     0.987
_refine_ls_restrained_S_all     0.987
_refine_ls_number_reflns     49686
_refine_ls_number_parameters     2972
_refine_ls_number_restraints     0
_refine_ls_hydrogen_treatment     constr
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
             'calc w = 1/[σ²(Fo²)+(0.0222P)²] where P = (Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.012
_refine_ls_shift/su_mean     <0.001
_refine_diff_density_max     0.607
_refine_diff_density_min     -0.676
_refine_ls_extinction_method     SHELXTL
_refine_ls_extinction_coef     0.000029(6)
_refine_ls_extinction_expression
                                  'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^'
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0061 0.0033
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Eu' 'Eu' -0.1578 3.6682
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'SMART (Bruker, 2000)'
_computing_cell_refinement     'SAINT (Bruker, 2000)'
_computing_data_reduction     'SAINT'
_computing_structure_solution     'SHELXTL (Sheldrick, 1998)'
_computing_structure_refinement     'SHELXTL'
_computing_molecular_graphics     'SHELXTL'
_computing_publication_material     'SHELXTL'
loop_
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    _atom_site_type_symbol
    Eu1A 0.323598(14) 0.195554(10) 0.095501(8) 0.02199(6) Uani d . 1 . . Eu
    N1A 0.3598(2) 0.17570(17) 0.17200(12) 0.0259(9) Uani d . 1 . . N
    O1A 0.17575(18) 0.17515(14) 0.08978(10) 0.0331(8) Uani d . 1 . . O
    C1A 0.3958(3) 0.2204(2) 0.20543(16) 0.0296(12) Uani d . 1 . . C
    H1AA 0.4125 0.2594 0.2007 0.036 Uiso calc R 1 . . H
    N2A 0.2837(2) 0.08363(17) 0.10403(14) 0.0362(11) Uani d . 1 . . N
    O2A 0.27487(17) 0.26486(13) 0.15186(10) 0.0264(8) Uani d . 1 . . O
    C2A 0.4104(3) 0.2129(2) 0.24756(17) 0.0398(14) Uani d . 1 . . C
    H2AA 0.4369 0.2461 0.2705 0.048 Uiso calc R 1 . . H
    O3A 0.44244(18) 0.27069(13) 0.12464(10) 0.0276(8) Uani d . 1 . . O
    C3A 0.3861(3) 0.1573(3) 0.25493(18) 0.0473(16) Uani d . 1 . . C
    H3AA 0.3949 0.1515 0.2832 0.057 Uiso calc R 1 . . H
    O4A 0.44149(18) 0.15565(13) 0.08048(10) 0.0272(8) Uani d . 1 . . O
    C4A 0.3484(3) 0.1094(2) 0.22065(18) 0.0387(14) Uani d . 1 . . C
    O5A 0.27953(18) 0.13808(13) 0.02175(10) 0.0273(8) Uani d . 1 . . O
    C5A 0.3222(4) 0.0492(3) 0.2256(2) 0.0537(17) Uani d . 1 . . C
    H5AA 0.3293 0.0416 0.2534 0.064 Uiso calc R 1 . . H
    O6A 0.33315(19) 0.26244(13) 0.05030(10) 0.0301(8) Uani d . 1 . . O
    C6A 0.2880(3) 0.0036(3) 0.1917(2) 0.0531(18) Uani d . 1 . . C
    H6AA 0.2719 -0.0357 0.1959 0.064 Uiso calc R 1 . . H
    C7A 0.2752(3) 0.0129(2) 0.14955(19) 0.0411(14) Uani d . 1 . . C
    C8A 0.2405(4) -0.0330(3) 0.1139(2) 0.068(2) Uani d . 1 . . C
    H8AA 0.2257 -0.0731 0.1167 0.082 Uiso calc R 1 . . H
    C9A 0.2277(5) -0.0208(3) 0.0751(2) 0.083(2) Uani d . 1 . . C
    H9AA 0.2031 -0.0522 0.0504 0.099 Uiso calc R 1 . . H
    C10A 0.2507(4) 0.0382(3) 0.0714(2) 0.064(2) Uani d . 1 . . C
    H10A 0.2419 0.0458 0.0437 0.077 Uiso calc R 1 . . H
    C11A 0.2971(3) 0.0715(2) 0.14363(17) 0.0316(13) Uani d . 1 . . C
    C12A 0.3362(3) 0.1201(2) 0.17924(16) 0.0263(12) Uani d . 1 . . C
    C13A 0.1177(3) 0.2024(2) 0.10258(15) 0.0236(11) Uani d . 1 . . C
    C14A 0.1288(3) 0.25356(19) 0.13771(14) 0.0227(11) Uani d . 1 . . C
    H14A 0.0811 0.2700 0.1460 0.027 Uiso calc R 1 . . H
    C15A 0.2064(3) 0.28149(19) 0.16112(15) 0.0243(11) Uani d . 1 . . C
    C16A 0.0331(3) 0.1757(2) 0.07730(15) 0.0238(11) Uani d . 1 . . C
    C17A 0.0259(3) 0.1263(2) 0.04249(17) 0.0404(14) Uani d . 1 . . C
    H17A 0.0729 0.1083 0.0361 0.048 Uiso calc R 1 . . H
    C18A -0.0484(3) 0.1030(3) 0.01697(19) 0.0552(17) Uani d . 1 . . C
    H18A -0.0523 0.0696 -0.0074 0.066 Uiso calc R 1 . . H
    C19A -0.1178(3) 0.1284(3) 0.0270(2) 0.0574(18) Uani d . 1 . . C
    H19A -0.1699 0.1116 0.0101 0.069 Uiso calc R 1 . . H
    C20A -0.1113(3) 0.1776(2) 0.06129(17) 0.0394(14) Uani d . 1 . . C
    H20A -0.1584 0.1955 0.0677 0.047 Uiso calc R 1 . . H
    C21A -0.0368(3) 0.2012(2) 0.08640(16) 0.0288(12) Uani d . 1 . . C
    H21A -0.0328 0.2352 0.1102 0.035 Uiso calc R 1 . . H
    C22A 0.2113(3) 0.3337(2) 0.20004(15) 0.0245(11) Uani d . 1 . . C
    C23A 0.1501(3) 0.3673(2) 0.20797(16) 0.0317(12) Uani d . 1 . . C
    H23A 0.1007 0.3567 0.1888 0.038 Uiso calc R 1 . . H
    C24A 0.1599(3) 0.4159(2) 0.24321(18) 0.0453(15) Uani d . 1 . . C
    H24A 0.1177 0.4389 0.2480 0.054 Uiso calc R 1 . . H
    C25A 0.2313(3) 0.4316(2) 0.27192(18) 0.0477(15) Uani d . 1 . . C
    H25A 0.2383 0.4656 0.2960 0.057 Uiso calc R 1 . . H
    C26A 0.2918(3) 0.3978(2) 0.26540(17) 0.0437(14) Uani d . 1 . . C
    H26A 0.3396 0.4073 0.2856 0.052 Uiso calc R 1 . . H
    C27A 0.2825(3) 0.3501(2) 0.22927(16) 0.0334(12) Uani d . 1 . . C
    H27A 0.3256 0.3279 0.2242 0.040 Uiso calc R 1 . . H
    C28A 0.5194(3) 0.2717(2) 0.13638(15) 0.0241(11) Uani d . 1 . . C
    C29A 0.5572(3) 0.2231(2) 0.12391(15) 0.0265(11) Uani d . 1 . . C
    H29A 0.6131 0.2272 0.1355 0.032 Uiso calc R 1 . . H
    C30A 0.5181(3) 0.1682(2) 0.09526(15) 0.0238(11) Uani d . 1 . . C
    C31A 0.5656(3) 0.3296(2) 0.16606(15) 0.0268(11) Uani d . 1 . . C
    C32A 0.5191(3) 0.3700(2) 0.18843(17) 0.0364(13) Uani d . 1 . . C
    H32A 0.4594 0.3602 0.1847 0.044 Uiso calc R 1 . . H
    C33A 0.5595(3) 0.4238(2) 0.21576(18) 0.0411(14) Uani d . 1 . . C
    H33A 0.5272 0.4508 0.2306 0.049 Uiso calc R 1 . . H
    C34A 0.6455(3) 0.4390(2) 0.22185(16) 0.0410(14) Uani d . 1 . . C
    H34A 0.6727 0.4759 0.2413 0.049 Uiso calc R 1 . . H
    C35A 0.6925(3) 0.4005(2) 0.19965(16) 0.0378(13) Uani d . 1 . . C
    H35A 0.7522 0.4115 0.2029 0.045 Uiso calc R 1 . . H
    C36A 0.6527(3) 0.3458(2) 0.17268(15) 0.0310(12) Uani d . 1 . . C
    H36A 0.6855 0.3189 0.1584 0.037 Uiso calc R 1 . . H
    C37A 0.5656(3) 0.1192(2) 0.08087(15) 0.0269(12) Uani d . 1 . . C
    C38A 0.6530(3) 0.1285(2) 0.08706(17) 0.0408(14) Uani d . 1 . . C
    H38A 0.6852 0.1677 0.0995 0.049 Uiso calc R 1 . . H
    C39A 0.6928(3) 0.0812(3) 0.07518(19) 0.0498(16) Uani d . 1 . . C
    H39A 0.7522 0.0878 0.0802 0.060 Uiso calc R 1 . . H
    C40A 0.6471(3) 0.0244(2) 0.05618(19) 0.0459(16) Uani d . 1 . . C
    H40A 0.6747 -0.0082 0.0484 0.055 Uiso calc R 1 . . H
    C41A 0.5614(3) 0.0149(2) 0.04843(19) 0.0492(16) Uani d . 1 . . C
    H41A 0.5298 -0.0240 0.0344 0.059 Uiso calc R 1 . . H
    C42A 0.5213(3) 0.0621(2) 0.06115(18) 0.0430(15) Uani d . 1 . . C
    H42A 0.4619 0.0550 0.0562 0.052 Uiso calc R 1 . . H
    C43A 0.2623(3) 0.1498(2) -0.01419(15) 0.0253(11) Uani d . 1 . . C
    C44A 0.2748(3) 0.2081(2) -0.02053(15) 0.0265(12) Uani d . 1 . . C
    H44A 0.2591 0.2119 -0.0486 0.032 Uiso calc R 1 . . H
    C45A 0.3085(3) 0.2607(2) 0.01135(16) 0.0269(12) Uani d . 1 . . C
    C46A 0.2271(3) 0.0992(2) -0.05216(16) 0.0300(12) Uani d . 1 . . C
    C47A 0.1679(3) 0.0504(2) -0.04605(17) 0.0350(13) Uani d . 1 . . C
    H47A 0.1529 0.0494 -0.0174 0.042 Uiso calc R 1 . . H
    C48A 0.1309(3) 0.0039(3) -0.0807(2) 0.0517(17) Uani d . 1 . . C
    H48A 0.0893 -0.0283 -0.0761 0.062 Uiso calc R 1 . . H
    C49A 0.1545(4) 0.0041(3) -0.1228(2) 0.058(2) Uani d . 1 . . C
    H49A 0.1293 -0.0280 -0.1468 0.069 Uiso calc R 1 . . H
    C50A 0.2145(5) 0.0510(3) -0.1292(2) 0.066(2) Uani d . 1 . . C
    H50A 0.2317 0.0509 -0.1576 0.079 Uiso calc R 1 . . H
    C51A 0.2496(4) 0.0981(3) -0.09448(17) 0.0486(16) Uani d . 1 . . C
    H51A 0.2901 0.1306 -0.0994 0.058 Uiso calc R 1 . . H
    C52A 0.3171(3) 0.3197(2) 0.00003(15) 0.0268(11) Uani d . 1 . . C
    C53A 0.2600(3) 0.3296(2) -0.02983(16) 0.0340(13) Uani d . 1 . . C
    H53A 0.2144 0.2981 -0.0439 0.041 Uiso calc R 1 . . H
    C54A 0.2698(3) 0.3853(2) -0.03883(17) 0.0396(14) Uani d . 1 . . C
    H54A 0.2305 0.3918 -0.0589 0.048 Uiso calc R 1 . . H
    C55A 0.3357(4) 0.4309(2) -0.01910(18) 0.0457(15) Uani d . 1 . . C
    H55A 0.3421 0.4688 -0.0259 0.055 Uiso calc R 1 . . H
    C56A 0.3932(3) 0.4225(2) 0.01071(18) 0.0434(14) Uani d . 1 . . C
    H56A 0.4392 0.4540 0.0243 0.052 Uiso calc R 1 . . H
    C57A 0.3818(3) 0.3670(2) 0.02022(16) 0.0324(12) Uani d . 1 . . C
    H57A 0.4197 0.3612 0.0413 0.039 Uiso calc R 1 . . H
    Eu1B 0.525070(14) 0.795351(10) 0.282171(8) 0.02258(6) Uani d . 1 . . Eu
    N1B 0.5213(3) 0.7624(2) 0.35577(14) 0.0367(11) Uani d . 1 . . N
    O1B 0.38108(18) 0.74812(13) 0.27441(10) 0.0285(8) Uani d . 1 . . O
    C1B 0.5324(4) 0.8017(3) 0.39403(19) 0.0520(17) Uani d . 1 . . C
    H1BA 0.5554 0.8425 0.3950 0.062 Uiso calc R 1 . . H
    N2B 0.5067(2) 0.67969(17) 0.27876(13) 0.0281(10) Uani d . 1 . . N
    O2B 0.44972(18) 0.85790(13) 0.32791(10) 0.0271(8) Uani d . 1 . . O
    C2B 0.5121(4) 0.7868(3) 0.43374(19) 0.071(2) Uani d . 1 . . C
    H2BA 0.5214 0.8168 0.4605 0.085 Uiso calc R 1 . . H
    O3B 0.63095(18) 0.87132(14) 0.32574(11) 0.0358(9) Uani d . 1 . . O
    C3B 0.4789(4) 0.7287(3) 0.4326(2) 0.072(2) Uani d . 1 . . C
    H3BA 0.4646 0.7176 0.4588 0.086 Uiso calc R 1 . . H
    O4B 0.65464(18) 0.76858(13) 0.27075(10) 0.0284(8) Uani d . 1 . . O
    C4B 0.4654(4) 0.6844(3) 0.3927(2) 0.0512(17) Uani d . 1 . . C
    O5B 0.49656(18) 0.74577(13) 0.20769(10) 0.0272(8) Uani d . 1 . . O
    C5B 0.4338(4) 0.6227(3) 0.3896(2) 0.064(2) Uani d . 1 . . C
    H5BA 0.4173 0.6102 0.4150 0.077 Uiso calc R 1 . . H
    O6B 0.53264(19) 0.86780(13) 0.24122(11) 0.0316(8) Uani d . 1 . . O
    C6B 0.4269(4) 0.5819(3) 0.3516(2) 0.062(2) Uani d . 1 . . C
    H6BA 0.4054 0.5408 0.3505 0.074 Uiso calc R 1 . . H
    C7B 0.4513(3) 0.5990(3) 0.3128(2) 0.0417(15) Uani d . 1 . . C
    C8B 0.4502(3) 0.5579(3) 0.2722(2) 0.0525(17) Uani d . 1 . . C
    H8BA 0.4292 0.5164 0.2695 0.063 Uiso calc R 1 . . H
    C9B 0.4784(3) 0.5767(2) 0.2371(2) 0.0443(15) Uani d . 1 . . C
    H9BA 0.4792 0.5489 0.2100 0.053 Uiso calc R 1 . . H
    C10B 0.5065(3) 0.6387(2) 0.24178(17) 0.0320(12) Uani d . 1 . . C
    H10B 0.5264 0.6519 0.2171 0.038 Uiso calc R 1 . . H
    C11B 0.4819(3) 0.6601(2) 0.31453(18) 0.0311(13) Uani d . 1 . . C
    C12B 0.4890(3) 0.7033(2) 0.35491(17) 0.0341(13) Uani d . 1 . . C
    C13B 0.3157(3) 0.7543(2) 0.29410(15) 0.0236(11) Uani d . 1 . . C
    C14B 0.3104(3) 0.8039(2) 0.32798(15) 0.0279(12) Uani d . 1 . . C
    H14B 0.2585 0.8048 0.3409 0.033 Uiso calc R 1 . . H
    C15B 0.3793(3) 0.8526(2) 0.34373(15) 0.0250(11) Uani d . 1 . . C
    C16B 0.2409(3) 0.7021(2) 0.28146(15) 0.0237(11) Uani d . 1 . . C
    C17B 0.2563(3) 0.6466(2) 0.26019(16) 0.0369(13) Uani d . 1 . . C
    H17B 0.3116 0.6435 0.2525 0.044 Uiso calc R 1 . . H
    C18B 0.1913(3) 0.5954(2) 0.25005(17) 0.0385(13) Uani d . 1 . . C
    H18B 0.2026 0.5574 0.2366 0.046 Uiso calc R 1 . . H
    C19B 0.1104(3) 0.6006(2) 0.25981(16) 0.0356(13) Uani d . 1 . . C
    H19B 0.0657 0.5661 0.2526 0.043 Uiso calc R 1 . . H
    C20B 0.0947(3) 0.6558(2) 0.28011(17) 0.0347(13) Uani d . 1 . . C
    H20B 0.0391 0.6593 0.2867 0.042 Uiso calc R 1 . . H
    C21B 0.1593(3) 0.7059(2) 0.29082(16) 0.0319(12) Uani d . 1 . . C
    H21B 0.1477 0.7436 0.3049 0.038 Uiso calc R 1 . . H
    C22B 0.3708(3) 0.9005(2) 0.38368(15) 0.0286(12) Uani d . 1 . . C
    C23B 0.2954(3) 0.9105(2) 0.39934(17) 0.0379(13) Uani d . 1 . . C
    H23B 0.2441 0.8869 0.3841 0.045 Uiso calc R 1 . . H
    C24B 0.2930(4) 0.9545(3) 0.43696(19) 0.0534(17) Uani d . 1 . . C
    H24B 0.2405 0.9603 0.4476 0.064 Uiso calc R 1 . . H
    C25B 0.3674(4) 0.9899(3) 0.4591(2) 0.066(2) Uani d . 1 . . C
    H25B 0.3664 1.0202 0.4848 0.079 Uiso calc R 1 . . H
    C26B 0.4424(4) 0.9805(3) 0.44336(19) 0.0572(18) Uani d . 1 . . C
    H26B 0.4935 1.0044 0.4585 0.069 Uiso calc R 1 . . H
    C27B 0.4448(3) 0.9372(2) 0.40614(18) 0.0420(14) Uani d . 1 . . C
    H27B 0.4976 0.9320 0.3955 0.050 Uiso calc R 1 . . H
    C28B 0.7104(3) 0.8816(2) 0.33524(15) 0.0257(11) Uani d . 1 . . C
    C29B 0.7604(3) 0.8410(2) 0.31782(16) 0.0283(12) Uani d . 1 . . C
    H29B 0.8179 0.8505 0.3283 0.034 Uiso calc R 1 . . H
    C30B 0.7312(3) 0.7873(2) 0.28578(15) 0.0246(11) Uani d . 1 . . C
    C31B 0.7481(3) 0.9397(2) 0.36685(16) 0.0284(12) Uani d . 1 . . C
    C32B 0.6949(3) 0.9736(3) 0.3892(2) 0.0559(17) Uani d . 1 . . C
    H32B 0.6358 0.9593 0.3836 0.067 Uiso calc R 1 . . H
    C33B 0.7253(3) 1.0272(3) 0.4190(2) 0.070(2) Uani d . 1 . . C
    H33B 0.6873 1.0488 0.4345 0.084 Uiso calc R 1 . . H
    C34B 0.8112(3) 1.0499(2) 0.42661(17) 0.0428(14) Uani d . 1 . . C
    H34B 0.8324 1.0873 0.4469 0.051 Uiso calc R 1 . . H
    C35B 0.8649(3) 1.0179(2) 0.40456(17) 0.0385(14) Uani d . 1 . . C
    H35B 0.9239 1.0334 0.4094 0.046 Uiso calc R 1 . . H
    C36B 0.8340(3) 0.9630(2) 0.37508(16) 0.0280(11) Uani d . 1 . . C
    H36B 0.8723 0.9410 0.3603 0.034 Uiso calc R 1 . . H
    C37B 0.7903(3) 0.7480(2) 0.26704(15) 0.0253(11) Uani d . 1 . . C
    C38B 0.8775(3) 0.7679(2) 0.27225(16) 0.0310(12) Uani d . 1 . . C
    H38B 0.9015 0.8079 0.2881 0.037 Uiso calc R 1 . . H
    C39B 0.9293(3) 0.7296(2) 0.25443(17) 0.0381(14) Uani d . 1 . . C
    H39B 0.9886 0.7436 0.2579 0.046 Uiso calc R 1 . . H
    C40B 0.8954(3) 0.6717(2) 0.23188(17) 0.0424(15) Uani d . 1 . . C
    H40B 0.9312 0.6456 0.2202 0.051 Uiso calc R 1 . . H
    C41B 0.8082(3) 0.6511(2) 0.22608(16) 0.0365(13) Uani d . 1 . . C
    H41B 0.7846 0.6111 0.2103 0.044 Uiso calc R 1 . . H
    C42B 0.7563(3) 0.6893(2) 0.24347(15) 0.0300(12) Uani d . 1 . . C
    H42B 0.6969 0.6755 0.2393 0.036 Uiso calc R 1 . . H
    C43B 0.4827(3) 0.7588(2) 0.17190(15) 0.0243(11) Uani d . 1 . . C
    C44B 0.4891(3) 0.8172(2) 0.16729(15) 0.0248(11) Uani d . 1 . . C
    H44B 0.4753 0.8224 0.1394 0.030 Uiso calc R 1 . . H
    C45B 0.5149(3) 0.8685(2) 0.20174(17) 0.0280(12) Uani d . 1 . . C
    C46B 0.4563(3) 0.7069(2) 0.13299(16) 0.0264(12) Uani d . 1 . . C
    C47B 0.4083(3) 0.6533(2) 0.13840(17) 0.0286(12) Uani d . 1 . . C
    H47B 0.3920 0.6505 0.1665 0.034 Uiso calc R 1 . . H
    C48B 0.3843(3) 0.6040(2) 0.10310(17) 0.0342(13) Uani d . 1 . . C
    H48B 0.3506 0.5678 0.1070 0.041 Uiso calc R 1 . . H
    C49B 0.4092(3) 0.6072(2) 0.06204(18) 0.0408(15) Uani d . 1 . . C
    H49B 0.3936 0.5733 0.0379 0.049 Uiso calc R 1 . . H
    C50B 0.4564(4) 0.6596(3) 0.05670(18) 0.0453(15) Uani d . 1 . . C
    H50B 0.4731 0.6620 0.0286 0.054 Uiso calc R 1 . . H
    C51B 0.4803(3) 0.7094(2) 0.09157(16) 0.0354(13) Uani d . 1 . . C
    H51B 0.5133 0.7454 0.0872 0.043 Uiso calc R 1 . . H
    C52B 0.5260(3) 0.9296(2) 0.19292(16) 0.0291(12) Uani d . 1 . . C
    C53B 0.4774(3) 0.9404(2) 0.15993(17) 0.0413(14) Uani d . 1 . . C
    H53B 0.4353 0.9088 0.1427 0.050 Uiso calc R 1 . . H
    C54B 0.4905(3) 0.9971(2) 0.15236(18) 0.0444(15) Uani d . 1 . . C
    H54B 0.4564 1.0046 0.1304 0.053 Uiso calc R 1 . . H
    C55B 0.5523(4) 1.0423(3) 0.1765(2) 0.0558(17) Uani d . 1 . . C
    H55B 0.5629 1.0806 0.1703 0.067 Uiso calc R 1 . . H
    C56B 0.5992(4) 1.0324(3) 0.2098(2) 0.0628(19) Uani d . 1 . . C
    H56B 0.6407 1.0643 0.2273 0.075 Uiso calc R 1 . . H
    C57B 0.5859(3) 0.9763(2) 0.21780(18) 0.0448(15) Uani d . 1 . . C
    H57B 0.6184 0.9697 0.2408 0.054 Uiso calc R 1 . . H
    Eu1C 0.085752(14) 0.981108(10) 0.313545(8) 0.02201(6) Uani d . 1 . . Eu
    N1C 0.0878(2) 1.01419(16) 0.23978(12) 0.0234(9) Uani d . 1 . . N
    O1C -0.02441(18) 1.03143(13) 0.31958(10) 0.0262(8) Uani d . 1 . . O
    C1C 0.0583(3) 0.9754(2) 0.20201(16) 0.0311(12) Uani d . 1 . . C
    H1CA 0.0410 0.9343 0.2019 0.037 Uiso calc R 1 . . H
    N2C 0.1495(2) 1.09514(16) 0.31647(13) 0.0259(9) Uani d . 1 . . N
    O2C -0.03621(17) 0.91645(12) 0.27040(10) 0.0243(7) Uani d . 1 . . O
    C2C 0.0509(3) 0.9911(2) 0.16242(17) 0.0413(14) Uani d . 1 . . C
    H2CA 0.0268 0.9618 0.1367 0.050 Uiso calc R 1 . . H
    O3C 0.09535(19) 1.02992(13) 0.38810(10) 0.0294(8) Uani d . 1 . . O
    C3C 0.0795(3) 1.0501(2) 0.16174(18) 0.0424(14) Uani d . 1 . . C
    H3CA 0.0765 1.0620 0.1352 0.051 Uiso calc R 1 . . H
    O4C 0.0607(2) 0.90750(14) 0.35367(11) 0.0337(8) Uani d . 1 . . O
    C4C 0.1127(3) 1.0922(2) 0.20035(17) 0.0329(13) Uani d . 1 . . C
    O5C 0.13902(18) 0.90893(13) 0.26541(10) 0.0310(8) Uani d . 1 . . O
    C5C 0.1450(3) 1.1544(2) 0.20237(19) 0.0415(14) Uani d . 1 . . C
    H5CA 0.1445 1.1678 0.1764 0.050 Uiso calc R 1 . . H
    O6C 0.23458(18) 1.00211(13) 0.32776(10) 0.0295(8) Uani d . 1 . . O
    C6C 0.1757(3) 1.1935(2) 0.23987(19) 0.0448(15) Uani d . 1 . . C
    H6CA 0.1974 1.2342 0.2400 0.054 Uiso calc R 1 . . H
    C7C 0.1767(3) 1.1759(2) 0.27993(17) 0.0320(13) Uani d . 1 . . C
    C8C 0.2083(3) 1.2156(2) 0.31979(18) 0.0374(13) Uani d . 1 . . C
    H8CA 0.2285 1.2569 0.3212 0.045 Uiso calc R 1 . . H
    C9C 0.2106(3) 1.1958(2) 0.35666(18) 0.0424(14) Uani d . 1 . . C
    H9CA 0.2322 1.2228 0.3838 0.051 Uiso calc R 1 . . H
    C10C 0.1803(3) 1.1342(2) 0.35379(18) 0.0352(13) Uani d . 1 . . C
    H10C 0.1820 1.1203 0.3795 0.042 Uiso calc R 1 . . H
    C11C 0.1471(3) 1.1150(2) 0.27964(15) 0.0226(11) Uani d . 1 . . C
    C12C 0.1147(3) 1.0722(2) 0.23907(16) 0.0245(11) Uani d . 1 . . C
    C13C -0.0952(3) 1.0270(2) 0.29930(15) 0.0236(11) Uani d . 1 . . C
    C14C -0.1343(3) 0.9773(2) 0.26664(15) 0.0267(11) Uani d . 1 . . C
    H14C -0.1847 0.9794 0.2518 0.032 Uiso calc R 1 . . H
    C15C -0.1043(3) 0.9240(2) 0.25396(15) 0.0243(11) Uani d . 1 . . C
    C16C -0.1353(3) 1.0800(2) 0.31338(15) 0.0250(11) Uani d . 1 . . C
    C17C -0.0865(3) 1.1336(2) 0.33650(16) 0.0326(13) Uani d . 1 . . C
    H17C -0.0290 1.1356 0.3442 0.039 Uiso calc R 1 . . H
    C18C -0.1188(3) 1.1851(2) 0.34899(17) 0.0413(14) Uani d . 1 . . C
    H18C -0.0839 1.2218 0.3650 0.050 Uiso calc R 1 . . H
    C19C -0.2025(3) 1.1819(2) 0.33782(17) 0.0396(14) Uani d . 1 . . C
    H19C -0.2251 1.2170 0.3456 0.048 Uiso calc R 1 . . H
    C20C -0.2534(3) 1.1283(2) 0.31546(18) 0.0432(15) Uani d . 1 . . C
    H20C -0.3110 1.1263 0.3081 0.052 Uiso calc R 1 . . H
    C21C -0.2201(3) 1.0771(2) 0.30369(16) 0.0326(12) Uani d . 1 . . C
    H21C -0.2555 1.0399 0.2890 0.039 Uiso calc R 1 . . H
    C22C -0.1529(3) 0.8731(2) 0.21867(15) 0.0239(11) Uani d . 1 . . C
    C23C -0.2405(3) 0.8622(2) 0.21159(16) 0.0284(12) Uani d . 1 . . C
    H23C -0.2707 0.8885 0.2290 0.034 Uiso calc R 1 . . H
    C24C -0.2833(3) 0.8140(2) 0.17987(16) 0.0347(13) Uani d . 1 . . C
    H24C -0.3429 0.8070 0.1759 0.042 Uiso calc R 1 . . H
    C25C -0.2405(3) 0.7754(2) 0.15355(17) 0.0357(13) Uani d . 1 . . C
    H25C -0.2701 0.7425 0.1312 0.043 Uiso calc R 1 . . H
    C26C -0.1536(3) 0.7858(2) 0.16053(16) 0.0351(13) Uani d . 1 . . C
    H26C -0.1236 0.7595 0.1429 0.042 Uiso calc R 1 . . H
    C27C -0.1101(3) 0.8337(2) 0.19275(16) 0.0290(12) Uani d . 1 . . C
    H27C -0.0507 0.8399 0.1973 0.035 Uiso calc R 1 . . H
    C28C 0.0913(3) 1.0160(2) 0.42461(16) 0.0261(11) Uani d . 1 . . C
    C29C 0.0735(3) 0.9566(2) 0.42849(17) 0.0327(13) Uani d . 1 . . C
    H29C 0.0683 0.9502 0.4569 0.039 Uiso calc R 1 . . H
    C30C 0.0631(3) 0.9065(2) 0.39343(17) 0.0279(12) Uani d . 1 . . C
    C31C 0.1054(3) 1.0672(2) 0.46442(16) 0.0275(12) Uani d . 1 . . C
    C32C 0.0840(3) 1.1207(2) 0.46206(17) 0.0313(12) Uani d . 1 . . C
    H32C 0.0602 1.1241 0.4353 0.038 Uiso calc R 1 . . H
    C33C 0.0967(3) 1.1689(2) 0.49805(18) 0.0404(14) Uani d . 1 . . C
    H33C 0.0805 1.2049 0.4961 0.048 Uiso calc R 1 . . H
    C34C 0.1325(3) 1.1651(2) 0.53655(18) 0.0445(14) Uani d . 1 . . C
    H34C 0.1417 1.1985 0.5612 0.053 Uiso calc R 1 . . H
    C35C 0.1553(4) 1.1124(2) 0.53941(18) 0.0519(17) Uani d . 1 . . C
    H35C 0.1806 1.1097 0.5660 0.062 Uiso calc R 1 . . H
    C36C 0.1413(3) 1.0637(2) 0.50376(17) 0.0424(15) Uani d . 1 . . C
    H36C 0.1564 1.0275 0.5061 0.051 Uiso calc R 1 . . H
    C37C 0.0511(3) 0.8450(2) 0.40270(16) 0.0291(12) Uani d . 1 . . C
    C38C 0.0817(3) 0.8371(2) 0.44179(18) 0.0396(14) Uani d . 1 . . C
    H38C 0.1114 0.8706 0.4636 0.048 Uiso calc R 1 . . H
    C39C 0.0686(4) 0.7797(3) 0.4488(2) 0.0513(17) Uani d . 1 . . C
    H39C 0.0900 0.7742 0.4753 0.062 Uiso calc R 1 . . H
    C40C 0.0253(4) 0.7316(3) 0.4178(2) 0.0526(17) Uani d . 1 . . C
    H40C 0.0157 0.6928 0.4232 0.063 Uiso calc R 1 . . H
    C41C -0.0052(4) 0.7386(2) 0.3782(2) 0.0557(17) Uani d . 1 . . C
    H41C -0.0354 0.7051 0.3565 0.067 Uiso calc R 1 . . H
    C42C 0.0097(3) 0.7956(2) 0.37113(18) 0.0420(14) Uani d . 1 . . C
    H42C -0.0091 0.8007 0.3440 0.050 Uiso calc R 1 . . H
    C43C 0.2089(3) 0.89292(19) 0.25909(14) 0.0227(11) Uani d . 1 . . C
    C44C 0.2863(3) 0.9254(2) 0.28051(15) 0.0270(12) Uani d . 1 . . C
    H44C 0.3352 0.9102 0.2729 0.032 Uiso calc R 1 . . H
    C45C 0.2953(3) 0.9793(2) 0.31265(16) 0.0264(12) Uani d . 1 . . C
    C46C 0.2037(3) 0.83501(19) 0.22510(15) 0.0225(11) Uani d . 1 . . C
    C47C 0.1241(3) 0.7988(2) 0.21136(16) 0.0298(12) Uani d . 1 . . C
    H47C 0.0758 0.8122 0.2226 0.036 Uiso calc R 1 . . H
    C48C 0.1142(3) 0.7439(2) 0.18157(17) 0.0401(14) Uani d . 1 . . C
    H48C 0.0595 0.7195 0.1730 0.048 Uiso calc R 1 . . H
    C49C 0.1832(3) 0.7243(2) 0.16434(18) 0.0399(14) Uani d . 1 . . C
    H49C 0.1768 0.6867 0.1437 0.048 Uiso calc R 1 . . H
    C50C 0.2616(3) 0.7604(2) 0.17762(19) 0.0502(16) Uani d . 1 . . C
    H50C 0.3098 0.7474 0.1659 0.060 Uiso calc R 1 . . H
    C51C 0.2718(3) 0.8151(2) 0.20757(18) 0.0430(15) Uani d . 1 . . C
    H51C 0.3267 0.8392 0.2161 0.052 Uiso calc R 1 . . H
    C52C 0.3825(3) 1.0145(2) 0.33054(17) 0.0330(12) Uani d . 1 . . C
    C53C 0.4555(3) 0.9969(2) 0.31458(17) 0.0398(14) Uani d . 1 . . C
    H53C 0.4515 0.9618 0.2917 0.048 Uiso calc R 1 . . H
    C54C 0.5336(4) 1.0315(3) 0.3327(2) 0.0640(19) Uani d . 1 . . C
    H54C 0.5832 1.0194 0.3221 0.077 Uiso calc R 1 . . H
    C55C 0.5405(4) 1.0814(4) 0.3645(3) 0.107(3) Uani d . 1 . . C
    H55C 0.5947 1.1046 0.3759 0.128 Uiso calc R 1 . . H
    C56C 0.4700(4) 1.0994(4) 0.3810(3) 0.129(4) Uani d . 1 . . C
    H56C 0.4753 1.1348 0.4039 0.154 Uiso calc R 1 . . H
    C57C 0.3903(4) 1.0651(3) 0.3637(2) 0.077(2) Uani d . 1 . . C
    H57C 0.3412 1.0770 0.3752 0.092 Uiso calc R 1 . . H
    Eu1D 0.881803(13) 0.375269(10) 0.102572(8) 0.02022(6) Uani d . 1 . . Eu
    N1D 0.8563(2) 0.40877(16) 0.03042(12) 0.0230(9) Uani d . 1 . . N
    O1D 0.77125(17) 0.42592(13) 0.11299(10) 0.0252(8) Uani d . 1 . . O
    C1D 0.8133(3) 0.3713(2) -0.00452(15) 0.0277(12) Uani d . 1 . . C
    H1DA 0.7934 0.3308 -0.0036 0.033 Uiso calc R 1 . . H
    N2D 0.9458(2) 0.48708(16) 0.10262(12) 0.0239(9) Uani d . 1 . . N
    O2D 0.75687(17) 0.30657(13) 0.07187(10) 0.0262(8) Uani d . 1 . . O
    C2D 0.7953(3) 0.3874(2) -0.04271(15) 0.0290(12) Uani d . 1 . . C
    H2DA 0.7638 0.3586 -0.0670 0.035 Uiso calc R 1 . . H
    O3D 0.90495(18) 0.42719(13) 0.17743(10) 0.0251(8) Uani d . 1 . . O
    C3D 0.8242(3) 0.4459(2) -0.04447(16) 0.0345(13) Uani d . 1 . . C
    H3DA 0.8128 0.4580 -0.0701 0.041 Uiso calc R 1 . . H
    O4D 0.87489(19) 0.30425(13) 0.14427(10) 0.0270(8) Uani d . 1 . . O
    C4D 0.8704(3) 0.4875(2) -0.00835(16) 0.0304(12) Uani d . 1 . . C
    O5D 0.92685(18) 0.30968(13) 0.04369(10) 0.0259(8) Uani d . 1 . . O
    C5D 0.9024(3) 0.5489(2) -0.00768(18) 0.0380(14) Uani d . 1 . . C
    H5DA 0.8924 0.5628 -0.0327 0.046 Uiso calc R 1 . . H
    O6D 1.03012(18) 0.38948(13) 0.11197(10) 0.0279(8) Uani d . 1 . . O
    C6D 0.9466(3) 0.5878(2) 0.02784(18) 0.0374(14) Uani d . 1 . . C
    H6DA 0.9678 0.6283 0.0273 0.045 Uiso calc R 1 . . H
    C7D 0.9621(3) 0.5687(2) 0.06643(17) 0.0310(12) Uani d . 1 . . C
    C8D 1.0083(3) 0.6074(2) 0.10393(17) 0.0357(13) Uani d . 1 . . C
    H8DA 1.0297 0.6484 0.1048 0.043 Uiso calc R 1 . . H
    C9D 1.0227(3) 0.5858(2) 0.13946(17) 0.0331(12) Uani d . 1 . . C
    H9DA 1.0537 0.6115 0.1651 0.040 Uiso calc R 1 . . H
    C10D 0.9908(3) 0.5251(2) 0.13699(16) 0.0273(11) Uani d . 1 . . C
    H10D 1.0020 0.5103 0.1614 0.033 Uiso calc R 1 . . H
    C11D 0.9322(3) 0.5083(2) 0.06689(15) 0.0225(11) Uani d . 1 . . C
    C12D 0.8850(3) 0.4667(2) 0.02909(16) 0.0262(11) Uani d . 1 . . C
    C13D 0.6962(3) 0.4169(2) 0.09630(15) 0.0234(11) Uani d . 1 . . C
    C14D 0.6534(3) 0.3636(2) 0.06815(15) 0.0247(11) Uani d . 1 . . C
    H14D 0.5996 0.3628 0.0554 0.030 Uiso calc R 1 . . H
    C15D 0.6845(3) 0.3108(2) 0.05739(15) 0.0249(11) Uani d . 1 . . C
    C16D 0.6555(3) 0.4700(2) 0.10732(15) 0.0257(11) Uani d . 1 . . C
    C17D 0.7057(3) 0.5268(2) 0.12296(15) 0.0284(12) Uani d . 1 . . C
    H17D 0.7649 0.5312 0.1271 0.034 Uiso calc R 1 . . H
    C18D 0.6711(3) 0.5773(2) 0.13265(15) 0.0333(13) Uani d . 1 . . C
    H18D 0.7067 0.6158 0.1432 0.040 Uiso calc R 1 . . H
    C19D 0.5854(3) 0.5716(2) 0.12706(16) 0.0348(13) Uani d . 1 . . C
    H19D 0.5616 0.6062 0.1332 0.042 Uiso calc R 1 . . H
    C20D 0.5347(3) 0.5151(2) 0.11244(17) 0.0369(13) Uani d . 1 . . C
    H20D 0.4754 0.5108 0.1090 0.044 Uiso calc R 1 . . H
    C21D 0.5688(3) 0.4649(2) 0.10284(15) 0.0305(12) Uani d . 1 . . C
    H21D 0.5329 0.4264 0.0931 0.037 Uiso calc R 1 . . H
    C22D 0.6344(3) 0.2560(2) 0.02562(15) 0.0250(11) Uani d . 1 . . C
    C23D 0.5471(3) 0.2440(2) 0.01873(16) 0.0274(11) Uani d . 1 . . C
    H23D 0.5166 0.2710 0.0352 0.033 Uiso calc R 1 . . H
    C24D 0.5042(3) 0.1937(2) -0.01152(17) 0.0368(13) Uani d . 1 . . C
    H24D 0.4445 0.1855 -0.0150 0.044 Uiso calc R 1 . . H
    C25D 0.5484(3) 0.1548(2) -0.03701(18) 0.0428(14) Uani d . 1 . . C
    H25D 0.5194 0.1212 -0.0589 0.051 Uiso calc R 1 . . H
    C26D 0.6342(4) 0.1658(2) -0.03004(17) 0.0436(14) Uani d . 1 . . C
    H26D 0.6642 0.1387 -0.0468 0.052 Uiso calc R 1 . . H
    C27D 0.6778(3) 0.2151(2) 0.00078(16) 0.0355(13) Uani d . 1 . . C
    H27D 0.7372 0.2216 0.0053 0.043 Uiso calc R 1 . . H
    C28D 0.9178(2) 0.41447(19) 0.21343(15) 0.0203(10) Uani d . 1 . . C
    C29D 0.9206(3) 0.3566(2) 0.21759(15) 0.0249(11) Uani d . 1 . . C
    H29D 0.9386 0.3522 0.2451 0.030 Uiso calc R 1 . . H
    C30D 0.8983(3) 0.30554(19) 0.18333(15) 0.0213(10) Uani d . 1 . . C
    C31D 0.9244(3) 0.46419(19) 0.25426(14) 0.0206(10) Uani d . 1 . . C
    C32D 0.8855(3) 0.51173(19) 0.25262(16) 0.0251(11) Uani d . 1 . . C
    H32D 0.8590 0.5132 0.2259 0.030 Uiso calc R 1 . . H
    C33D 0.8857(3) 0.5564(2) 0.28979(16) 0.0307(12) Uani d . 1 . . C
    H33D 0.8572 0.5877 0.2887 0.037 Uiso calc R 1 . . H
    C34D 0.9262(3) 0.5566(2) 0.32819(16) 0.0343(12) Uani d . 1 . . C
    H34D 0.9264 0.5881 0.3534 0.041 Uiso calc R 1 . . H
    C35D 0.9671(3) 0.5106(2) 0.33023(16) 0.0355(13) Uani d . 1 . . C
    H35D 0.9958 0.5106 0.3567 0.043 Uiso calc R 1 . . H
    C36D 0.9653(3) 0.4650(2) 0.29323(15) 0.0277(12) Uani d . 1 . . C
    H36D 0.9929 0.4334 0.2946 0.033 Uiso calc R 1 . . H
    C37D 0.8946(3) 0.2453(2) 0.19293(14) 0.0240(11) Uani d . 1 . . C
    C38D 0.9542(3) 0.2363(2) 0.22199(14) 0.0312(12) Uani d . 1 . . C
    H38D 1.0005 0.2679 0.2350 0.037 Uiso calc R 1 . . H
    C39D 0.9448(3) 0.1810(2) 0.23162(16) 0.0383(14) Uani d . 1 . . C
    H39D 0.9855 0.1747 0.2511 0.046 Uiso calc R 1 . . H
    C40D 0.8787(4) 0.1357(2) 0.21383(18) 0.0497(16) Uani d . 1 . . C
    H40D 0.8726 0.0986 0.2216 0.060 Uiso calc R 1 . . H
    C41D 0.8193(3) 0.1430(2) 0.18417(18) 0.0455(15) Uani d . 1 . . C
    H41D 0.7735 0.1110 0.1712 0.055 Uiso calc R 1 . . H
    C42D 0.8288(3) 0.1984(2) 0.17400(16) 0.0353(13) Uani d . 1 . . C
    H42D 0.7892 0.2039 0.1536 0.042 Uiso calc R 1 . . H
    C43D 0.9959(3) 0.2980(2) 0.02983(15) 0.0230(11) Uani d . 1 . . C
    C44D 1.0754(3) 0.32613(19) 0.05106(14) 0.0221(11) Uani d . 1 . . C
    H44D 1.1234 0.3147 0.0380 0.027 Uiso calc R 1 . . H
    C45D 1.0882(3) 0.3701(2) 0.09038(15) 0.0227(11) Uani d . 1 . . C
    C46D 0.9892(3) 0.25290(19) -0.01317(14) 0.0227(11) Uani d . 1 . . C
    C47D 0.9177(3) 0.2422(2) -0.04176(15) 0.0310(12) Uani d . 1 . . C
    H47D 0.8737 0.2624 -0.0328 0.037 Uiso calc R 1 . . H
    C48D 0.9090(3) 0.2032(2) -0.08240(17) 0.0393(14) Uani d . 1 . . C
    H48D 0.8599 0.1970 -0.1012 0.047 Uiso calc R 1 . . H
    C49D 0.9728(3) 0.1730(2) -0.09565(17) 0.0413(14) Uani d . 1 . . C
    H49D 0.9681 0.1465 -0.1238 0.050 Uiso calc R 1 . . H
    C50D 1.0432(3) 0.1819(2) -0.06751(17) 0.0387(14) Uani d . 1 . . C
    H50D 1.0861 0.1605 -0.0762 0.046 Uiso calc R 1 . . H
    C51D 1.0516(3) 0.2215(2) -0.02697(16) 0.0305(12) Uani d . 1 . . C
    H51D 1.1008 0.2275 -0.0082 0.037 Uiso calc R 1 . . H
    C52D 1.1764(3) 0.3990(2) 0.10948(14) 0.0231(11) Uani d . 1 . . C
    C53D 1.2427(3) 0.3691(2) 0.10180(14) 0.0225(10) Uani d . 1 . . C
    H53D 1.2331 0.3309 0.0817 0.027 Uiso calc R 1 . . H
    C54D 1.3217(3) 0.3938(2) 0.12284(16) 0.0308(12) Uani d . 1 . . C
    H54D 1.3655 0.3722 0.1178 0.037 Uiso calc R 1 . . H
    C55D 1.3369(3) 0.4501(2) 0.15119(17) 0.0380(13) Uani d . 1 . . C
    H55D 1.3910 0.4669 0.1660 0.046 Uiso calc R 1 . . H
    C56D 1.2737(3) 0.4820(2) 0.15821(17) 0.0359(13) Uani d . 1 . . C
    H56D 1.2852 0.5215 0.1766 0.043 Uiso calc R 1 . . H
    C57D 1.1931(3) 0.4562(2) 0.13831(16) 0.0317(12) Uani d . 1 . . C
    H57D 1.1492 0.4775 0.1443 0.038 Uiso calc R 1 . . H
    Eu1E 0.286909(14) 0.575887(11) 0.533437(8) 0.02480(6) Uani d . 1 . . Eu
    N1E 0.2412(2) 0.58925(17) 0.45699(13) 0.0291(10) Uani d . 1 . . N
    O1E 0.16674(18) 0.59698(13) 0.56892(10) 0.0274(8) Uani d . 1 . . O
    C1E 0.2175(3) 0.5430(2) 0.42302(16) 0.0335(12) Uani d . 1 . . C
    H1EA 0.2136 0.5040 0.4274 0.040 Uiso calc R 1 . . H
    N2E 0.2790(2) 0.68469(17) 0.52705(13) 0.0285(10) Uani d . 1 . . N
    O2E 0.17161(19) 0.49528(14) 0.50503(10) 0.0309(8) Uani d . 1 . . O
    C2E 0.1975(3) 0.5478(2) 0.38072(16) 0.0402(14) Uani d . 1 . . C
    H2EA 0.1779 0.5131 0.3576 0.048 Uiso calc R 1 . . H
    O3E 0.33862(19) 0.63243(14) 0.60377(11) 0.0315(8) Uani d . 1 . . O
    C3E 0.2071(3) 0.6035(3) 0.37386(18) 0.0452(15) Uani d . 1 . . C
    H3EA 0.1958 0.6080 0.3454 0.054 Uiso calc R 1 . . H
    O4E 0.2982(2) 0.50864(14) 0.57594(11) 0.0330(8) Uani d . 1 . . O
    C4E 0.2336(3) 0.6542(3) 0.40835(17) 0.0394(14) Uani d . 1 . . C
    O5E 0.3486(2) 0.50988(13) 0.48374(11) 0.0328(8) Uani d . 1 . . O
    C5E 0.2481(4) 0.7143(3) 0.4034(2) 0.0574(18) Uani d . 1 . . C
    H5EA 0.2419 0.7208 0.3751 0.069 Uiso calc R 1 . . H
    O6E 0.42175(19) 0.62523(14) 0.52243(11) 0.0362(9) Uani d . 1 . . O
    C6E 0.2701(4) 0.7612(3) 0.4376(2) 0.0540(17) Uani d . 1 . . C
    H6EA 0.2802 0.8005 0.4330 0.065 Uiso calc R 1 . . H
    C7E 0.2790(3) 0.7545(2) 0.48103(19) 0.0410(14) Uani d . 1 . . C
    C8E 0.2935(4) 0.8012(3) 0.5183(2) 0.0540(17) Uani d . 1 . . C
    H8EA 0.2996 0.8412 0.5158 0.065 Uiso calc R 1 . . H
    C9E 0.2989(4) 0.7905(2) 0.5586(2) 0.0544(17) Uani d . 1 . . C
    H9EA 0.3069 0.8224 0.5842 0.065 Uiso calc R 1 . . H
    C10E 0.2925(3) 0.7313(2) 0.56114(17) 0.0406(14) Uani d . 1 . . C
    H10E 0.2981 0.7241 0.5892 0.049 Uiso calc R 1 . . H
    C11E 0.2705(3) 0.6951(2) 0.48693(16) 0.0309(12) Uani d . 1 . . C
    C12E 0.2491(3) 0.6450(2) 0.45013(16) 0.0311(12) Uani d . 1 . . C
    C13E 0.0969(3) 0.5665(2) 0.57503(15) 0.0255(11) Uani d . 1 . . C
    C14E 0.0653(3) 0.5057(2) 0.55414(14) 0.0259(11) Uani d . 1 . . C
    H14E 0.0148 0.4857 0.5633 0.031 Uiso calc R 1 . . H
    C15E 0.1043(3) 0.4732(2) 0.52066(15) 0.0244(11) Uani d . 1 . . C
    C16E 0.0459(3) 0.5990(2) 0.60772(15) 0.0237(11) Uani d . 1 . . C
    C17E 0.0880(3) 0.6468(2) 0.64098(15) 0.0298(12) Uani d . 1 . . C
    H17E 0.1476 0.6578 0.6427 0.036 Uiso calc R 1 . . H
    C18E 0.0437(3) 0.6787(2) 0.67174(16) 0.0357(13) Uani d . 1 . . C
    H18E 0.0730 0.7108 0.6947 0.043 Uiso calc R 1 . . H
    C19E -0.0437(3) 0.6631(2) 0.66857(16) 0.0345(13) Uani d . 1 . . C
    H19E -0.0745 0.6848 0.6893 0.041 Uiso calc R 1 . . H
    C20E -0.0859(3) 0.6160(2) 0.63524(16) 0.0344(13) Uani d . 1 . . C
    H20E -0.1456 0.6055 0.6330 0.041 Uiso calc R 1 . . H
    C21E -0.0413(3) 0.5840(2) 0.60510(15) 0.0296(12) Uani d . 1 . . C
    H21E -0.0707 0.5515 0.5824 0.036 Uiso calc R 1 . . H
    C22E 0.0681(3) 0.4080(2) 0.50107(14) 0.0243(11) Uani d . 1 . . C
    C23E -0.0171(3) 0.3829(2) 0.49832(15) 0.0286(12) Uani d . 1 . . C
    H23E -0.0550 0.4067 0.5112 0.034 Uiso calc R 1 . . H
    C24E -0.0475(3) 0.3231(2) 0.47680(16) 0.0339(13) Uani d . 1 . . C
    H24E -0.1062 0.3065 0.4747 0.041 Uiso calc R 1 . . H
    C25E 0.0067(3) 0.2873(2) 0.45846(16) 0.0336(13) Uani d . 1 . . C
    H25E -0.0143 0.2463 0.4440 0.040 Uiso calc R 1 . . H
    C26E 0.0926(3) 0.3123(2) 0.46150(16) 0.0349(13) Uani d . 1 . . C
    H26E 0.1306 0.2883 0.4492 0.042 Uiso calc R 1 . . H
    C27E 0.1224(3) 0.3716(2) 0.48223(16) 0.0308(12) Uani d . 1 . . C
    H27E 0.1810 0.3882 0.4838 0.037 Uiso calc R 1 . . H
    C28E 0.3273(3) 0.6229(2) 0.64115(16) 0.0284(12) Uani d . 1 . . C
    C29E 0.3083(3) 0.5653(2) 0.64913(16) 0.0311(12) Uani d . 1 . . C
    H29E 0.3015 0.5625 0.6783 0.037 Uiso calc R 1 . . H
    C30E 0.2991(3) 0.5120(2) 0.61633(17) 0.0312(12) Uani d . 1 . . C
    C31E 0.3364(3) 0.6770(2) 0.67833(17) 0.0349(13) Uani d . 1 . . C
    C32E 0.3882(3) 0.7308(2) 0.67442(18) 0.0386(14) Uani d . 1 . . C
    H32E 0.4182 0.7318 0.6492 0.046 Uiso calc R 1 . . H
    C33E 0.3950(3) 0.7825(2) 0.7077(2) 0.0516(18) Uani d . 1 . . C
    H33E 0.4292 0.8191 0.7051 0.062 Uiso calc R 1 . . H
    C34E 0.3522(4) 0.7809(3) 0.7447(2) 0.059(2) Uani d . 1 . . C
    H34E 0.3581 0.8161 0.7677 0.071 Uiso calc R 1 . . H
    C35E 0.3007(4) 0.7280(3) 0.7481(2) 0.064(2) Uani d . 1 . . C
    H35E 0.2699 0.7271 0.7731 0.077 Uiso calc R 1 . . H
    C36E 0.2941(4) 0.6765(2) 0.71538(18) 0.0464(15) Uani d . 1 . . C
    H36E 0.2599 0.6401 0.7184 0.056 Uiso calc R 1 . . H
    C37E 0.2908(3) 0.4540(2) 0.62956(16) 0.0292(12) Uani d . 1 . . C
    C38E 0.3341(3) 0.4486(2) 0.66610(17) 0.0362(13) Uani d . 1 . . C
    H38E 0.3706 0.4827 0.6844 0.043 Uiso calc R 1 . . H
    C39E 0.3241(3) 0.3929(3) 0.67592(19) 0.0473(16) Uani d . 1 . . C
    H39E 0.3545 0.3893 0.7008 0.057 Uiso calc R 1 . . H
    C40E 0.2710(4) 0.3435(3) 0.6501(2) 0.0582(18) Uani d . 1 . . C
    H40E 0.2632 0.3060 0.6576 0.070 Uiso calc R 1 . . H
    C41E 0.2285(4) 0.3482(2) 0.61297(19) 0.0528(16) Uani d . 1 . . C
    H41E 0.1920 0.3138 0.5948 0.063 Uiso calc R 1 . . H
    C42E 0.2392(3) 0.4030(2) 0.60232(17) 0.0400(14) Uani d . 1 . . C
    H42E 0.2114 0.4058 0.5764 0.048 Uiso calc R 1 . . H
    C43E 0.4155(3) 0.5100(2) 0.46336(16) 0.0286(12) Uani d . 1 . . C
    C44E 0.4856(3) 0.5582(2) 0.47358(16) 0.0306(12) Uani d . 1 . . C
    H44E 0.5358 0.5530 0.4599 0.037 Uiso calc R 1 . . H
    C45E 0.4859(3) 0.6132(2) 0.50259(16) 0.0282(12) Uani d . 1 . . C
    C46E 0.4140(3) 0.4558(2) 0.42720(16) 0.0294(12) Uani d . 1 . . C
    C47E 0.3448(4) 0.4093(2) 0.42167(19) 0.0536(16) Uani d . 1 . . C
    H47E 0.3022 0.4124 0.4415 0.064 Uiso calc R 1 . . H
    C48E 0.3360(5) 0.3587(3) 0.3883(2) 0.071(2) Uani d . 1 . . C
    H48E 0.2873 0.3274 0.3848 0.085 Uiso calc R 1 . . H
    C49E 0.3982(4) 0.3533(3) 0.3598(2) 0.0568(18) Uani d . 1 . . C
    H49E 0.3932 0.3179 0.3370 0.068 Uiso calc R 1 . . H
    C50E 0.4673(4) 0.3993(3) 0.3646(2) 0.069(2) Uani d . 1 . . C
    H50E 0.5100 0.3961 0.3448 0.083 Uiso calc R 1 . . H
    C51E 0.4748(3) 0.4500(3) 0.39814(19) 0.0529(17) Uani d . 1 . . C
    H51E 0.5229 0.4816 0.4012 0.063 Uiso calc R 1 . . H
    C52E 0.5608(3) 0.6642(2) 0.51030(16) 0.0286(12) Uani d . 1 . . C
    C53E 0.5573(3) 0.7165(2) 0.54136(18) 0.0447(15) Uani d . 1 . . C
    H53E 0.5096 0.7181 0.5579 0.054 Uiso calc R 1 . . H
    C54E 0.6226(3) 0.7660(3) 0.5483(2) 0.0577(18) Uani d . 1 . . C
    H54E 0.6190 0.8016 0.5692 0.069 Uiso calc R 1 . . H
    C55E 0.6928(3) 0.7644(3) 0.5254(2) 0.0555(17) Uani d . 1 . . C
    H55E 0.7377 0.7985 0.5306 0.067 Uiso calc R 1 . . H
    C56E 0.6975(3) 0.7134(3) 0.49520(19) 0.0536(17) Uani d . 1 . . C
    H56E 0.7457 0.7122 0.4790 0.064 Uiso calc R 1 . . H
    C57E 0.6324(3) 0.6630(2) 0.48781(17) 0.0417(14) Uani d . 1 . . C
    H57F 0.6371 0.6274 0.4671 0.050 Uiso calc R 1 . . H
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    Eu1A O4A . 2.312(3) y
    Eu1A O3A . 2.339(3) y
    Eu1A O1A . 2.351(3) y
    Eu1A O6A . 2.354(3) y
    Eu1A O2A . 2.382(3) y
    Eu1A O5A . 2.413(3) y
    Eu1A N1A . 2.651(4) y
    Eu1A N2A . 2.661(4) y
    N1A C1A . 1.326(6) ?
    N1A C12A . 1.362(6) ?
    O1A C13A . 1.267(5) y
    C1A C2A . 1.409(6) ?
    C1A H1AA . 0.95 ?
    N2A C10A . 1.308(6) ?
    N2A C11A . 1.374(6) ?
    O2A C15A . 1.272(5) y
    C2A C3A . 1.364(7) ?
    C2A H2AA . 0.95 ?
    O3A C28A . 1.291(5) y
    C3A C4A . 1.390(7) ?
    C3A H3AA . 0.95 ?
    O4A C30A . 1.272(5) y
    C4A C12A . 1.412(6) ?
    C4A C5A . 1.440(7) ?
    O5A C43A . 1.272(5) y
    C5A C6A . 1.338(8) ?
    C5A H5AA . 0.95 ?
    O6A C45A . 1.278(5) y
    C6A C7A . 1.420(7) ?
    C6A H6AA . 0.95 ?
    C7A C8A . 1.378(7) ?
    C7A C11A . 1.412(7) ?
    C8A C9A . 1.350(8) ?
    C8A H8AA . 0.95 ?
    C9A C10A . 1.397(8) ?
    C9A H9AA . 0.95 ?
    C10A H10A . 0.95 ?
    C11A C12A . 1.427(6) ?
    C13A C14A . 1.408(6) y
    C13A C16A . 1.513(6) y
    C14A C15A . 1.401(6) y
    C14A H14A . 0.95 ?
    C15A C22A . 1.506(6) y
    C16A C17A . 1.380(6) ?
    C16A C21A . 1.394(6) ?
    C17A C18A . 1.375(7) ?
    C17A H17A . 0.95 ?
    C18A C19A . 1.391(7) ?
    C18A H18A . 0.95 ?
    C19A C20A . 1.369(7) ?
    C19A H19A . 0.95 ?
    C20A C21A . 1.371(6) ?
    C20A H20A . 0.95 ?
    C21A H21A . 0.95 ?
    C22A C23A . 1.382(6) ?
    C22A C27A . 1.395(6) ?
    C23A C24A . 1.373(7) ?
    C23A H23A . 0.95 ?
    C24A C25A . 1.388(7) ?
    C24A H24A . 0.95 ?
    C25A C26A . 1.374(6) ?
    C25A H25A . 0.95 ?
    C26A C27A . 1.379(7) ?
    C26A H26A . 0.95 ?
    C27A H27A . 0.95 ?
    C28A C29A . 1.385(6) y
    C28A C31A . 1.498(6) y
    C29A C30A . 1.406(6) y
    C29A H29A . 0.95 ?
    C30A C37A . 1.503(6) y
    C31A C36A . 1.389(6) ?
    C31A C32A . 1.404(6) ?
    C32A C33A . 1.376(7) ?
    C32A H32A . 0.95 ?
    C33A C34A . 1.371(7) ?
    C33A H33A . 0.95 ?
    C34A C35A . 1.379(7) ?
    C34A H34A . 0.95 ?
    C35A C36A . 1.383(6) ?
    C35A H35A . 0.95 ?
    C36A H36A . 0.95 ?
    C37A C42A . 1.377(6) ?
    C37A C38A . 1.396(6) ?
    C38A C39A . 1.379(6) ?
    C38A H38A . 0.95 ?
    C39A C40A . 1.376(7) ?
    C39A H39A . 0.95 ?
    C40A C41A . 1.375(7) ?
    C40A H40A . 0.95 ?
    C41A C42A . 1.382(6) ?
    C41A H41A . 0.95 ?
    C42A H42A . 0.95 ?
    C43A C44A . 1.406(6) y
    C43A C46A . 1.483(6) y
    C44A C45A . 1.398(6) y
    C44A H44A . 0.95 ?
    C45A C52A . 1.494(6) y
    C46A C51A . 1.396(7) ?
    C46A C47A . 1.397(7) ?
    C47A C48A . 1.377(7) ?
    C47A H47A . 0.95 ?
    C48A C49A . 1.397(8) ?
    C48A H48A . 0.95 ?
    C49A C50A . 1.377(9) ?
    C49A H49A . 0.95 ?
    C50A C51A . 1.376(8) ?
    C50A H50A . 0.95 ?
    C51A H51A . 0.95 ?
    C52A C57A . 1.381(6) ?
    C52A C53A . 1.402(6) ?
    C53A C54A . 1.383(6) ?
    C53A H53A . 0.95 ?
    C54A C55A . 1.370(7) ?
    C54A H54A . 0.95 ?
    C55A C56A . 1.389(6) ?
    C55A H55A . 0.95 ?
    C56A C57A . 1.386(6) ?
    C56A H56A . 0.95 ?
    C57A H57A . 0.95 ?
    Eu1B O4B . 2.332(3) ?
    Eu1B O3B . 2.351(3) ?
    Eu1B O5B . 2.358(3) ?
    Eu1B O2B . 2.359(3) ?
    Eu1B O1B . 2.362(3) ?
    Eu1B O6B . 2.363(3) ?
    Eu1B N1B . 2.627(4) ?
    Eu1B N2B . 2.650(4) ?
    N1B C1B . 1.320(6) ?
    N1B C12B . 1.378(6) ?
    O1B C13B . 1.264(5) ?
    C1B C2B . 1.415(8) ?
    C1B H1BA . 0.95 ?
    N2B C10B . 1.327(6) ?
    N2B C11B . 1.364(6) ?
    O2B C15B . 1.258(5) ?
    C2B C3B . 1.357(9) ?
    C2B H2BA . 0.95 ?
    O3B C28B . 1.281(5) ?
    C3B C4B . 1.412(8) ?
    C3B H3BA . 0.95 ?
    O4B C30B . 1.274(5) ?
    C4B C12B . 1.410(7) ?
    C4B C5B . 1.417(9) ?
    O5B C43B . 1.271(5) ?
    C5B C6B . 1.334(9) ?
    C5B H5BA . 0.95 ?
    O6B C45B . 1.282(5) ?
    C6B C7B . 1.425(8) ?
    C6B H6BA . 0.95 ?
    C7B C8B . 1.409(8) ?
    C7B C11B . 1.410(7) ?
    C8B C9B . 1.353(8) ?
    C8B H8BA . 0.95 ?
    C9B C10B . 1.406(6) ?
    C9B H9BA . 0.95 ?
    C10B H10B . 0.95 ?
    C11B C12B . 1.417(7) ?
    C13B C14B . 1.402(6) ?
    C13B C16B . 1.513(6) ?
    C14B C15B . 1.413(6) ?
    C14B H14B . 0.95 ?
    C15B C22B . 1.511(6) ?
    C16B C21B . 1.383(6) ?
    C16B C17B . 1.392(6) ?
    C17B C18B . 1.399(7) ?
    C17B H17B . 0.95 ?
    C18B C19B . 1.381(6) ?
    C18B H18B . 0.95 ?
    C19B C20B . 1.381(6) ?
    C19B H19B . 0.95 ?
    C20B C21B . 1.378(6) ?
    C20B H20B . 0.95 ?
    C21B H21B . 0.95 ?
    C22B C23B . 1.379(6) ?
    C22B C27B . 1.395(7) ?
    C23B C24B . 1.386(7) ?
    C23B H23B . 0.95 ?
    C24B C25B . 1.387(8) ?
    C24B H24B . 0.95 ?
    C25B C26B . 1.368(7) ?
    C25B H25B . 0.95 ?
    C26B C27B . 1.369(7) ?
    C26B H26B . 0.95 ?
    C27B H27B . 0.95 ?
    C28B C29B . 1.399(6) ?
    C28B C31B . 1.492(6) ?
    C29B C30B . 1.405(6) ?
    C29B H29B . 0.95 ?
    C30B C37B . 1.502(6) ?
    C31B C32B . 1.386(6) ?
    C31B C36B . 1.388(6) ?
    C32B C33B . 1.372(7) ?
    C32B H32B . 0.95 ?
    C33B C34B . 1.385(7) ?
    C33B H33B . 0.95 ?
    C34B C35B . 1.364(7) ?
    C34B H34B . 0.95 ?
    C35B C36B . 1.390(6) ?
    C35B H35B . 0.95 ?
    C36B H36B . 0.95 ?
    C37B C38B . 1.394(6) ?
    C37B C42B . 1.395(6) ?
    C38B C39B . 1.388(6) ?
    C38B H38B . 0.95 ?
    C39B C40B . 1.372(7) ?
    C39B H39B . 0.95 ?
    C40B C41B . 1.396(7) ?
    C40B H40B . 0.95 ?
    C41B C42B . 1.385(6) ?
    C41B H41B . 0.95 ?
    C42B H42B . 0.95 ?
    C43B C44B . 1.398(6) ?
    C43B C46B . 1.496(6) ?
    C44B C45B . 1.403(6) ?
    C44B H44B . 0.95 ?
    C45B C52B . 1.504(6) ?
    C46B C51B . 1.391(7) ?
    C46B C47B . 1.393(6) ?
    C47B C48B . 1.388(6) ?
    C47B H47B . 0.95 ?
    C48B C49B . 1.389(7) ?
    C48B H48B . 0.95 ?
    C49B C50B . 1.363(7) ?
    C49B H49B . 0.95 ?
    C50B C51B . 1.385(7) ?
    C50B H50B . 0.95 ?
    C51B H51B . 0.95 ?
    C52B C57B . 1.375(7) ?
    C52B C53B . 1.396(6) ?
    C53B C54B . 1.386(7) ?
    C53B H53B . 0.95 ?
    C54B C55B . 1.366(7) ?
    C54B H54B . 0.95 ?
    C55B C56B . 1.379(7) ?
    C55B H55B . 0.95 ?
    C56B C57B . 1.379(7) ?
    C56B H56B . 0.95 ?
    C57B H57B . 0.95 ?
    Eu1C O5C . 2.319(3) ?
    Eu1C O1C . 2.326(3) ?
    Eu1C O3C . 2.354(3) ?
    Eu1C O4C . 2.361(3) ?
    Eu1C O6C . 2.382(3) ?
    Eu1C O2C . 2.403(3) ?
    Eu1C N1C . 2.635(4) ?
    Eu1C N2C . 2.651(4) ?
    N1C C1C . 1.330(6) ?
    N1C C12C . 1.352(5) ?
    O1C C13C . 1.279(5) ?
    C1C C2C . 1.399(6) ?
    C1C H1CA . 0.95 ?
    N2C C10C . 1.327(6) ?
    N2C C11C . 1.360(5) ?
    O2C C15C . 1.274(4) ?
    C2C C3C . 1.378(7) ?
    C2C H2CA . 0.95 ?
    O3C C28C . 1.276(5) ?
    C3C C4C . 1.393(7) ?
    C3C H3CA . 0.95 ?
    O4C C30C . 1.266(5) ?
    C4C C12C . 1.417(6) ?
    C4C C5C . 1.435(7) ?
    O5C C43C . 1.274(5) ?
    C5C C6C . 1.331(7) ?
    C5C H5CA . 0.95 ?
    O6C C45C . 1.268(5) ?
    C6C C7C . 1.427(7) ?
    C6C H6CA . 0.95 ?
    C7C C8C . 1.393(7) ?
    C7C C11C . 1.413(6) ?
    C8C C9C . 1.360(7) ?
    C8C H8CA . 0.95 ?
    C9C C10C . 1.412(6) ?
    C9C H9CA . 0.95 ?
    C10C H10C . 0.95 ?
    C11C C12C . 1.442(6) ?
    C13C C14C . 1.390(6) ?
    C13C C16C . 1.501(6) ?
    C14C C15C . 1.409(6) ?
    C14C H14C . 0.95 ?
    C15C C22C . 1.498(6) ?
    C16C C17C . 1.371(6) ?
    C16C C21C . 1.391(6) ?
    C17C C18C . 1.390(6) ?
    C17C H17C . 0.95 ?
    C18C C19C . 1.381(6) ?
    C18C H18C . 0.95 ?
    C19C C20C . 1.379(7) ?
    C19C H19C . 0.95 ?
    C20C C21C . 1.392(6) ?
    C20C H20C . 0.95 ?
    C21C H21C . 0.95 ?
    C22C C27C . 1.393(6) ?
    C22C C23C . 1.399(6) ?
    C23C C24C . 1.372(6) ?
    C23C H23C . 0.95 ?
    C24C C25C . 1.388(7) ?
    C24C H24C . 0.95 ?
    C25C C26C . 1.390(6) ?
    C25C H25C . 0.95 ?
    C26C C27C . 1.380(6) ?
    C26C H26C . 0.95 ?
    C27C H27C . 0.95 ?
    C28C C29C . 1.403(6) ?
    C28C C31C . 1.496(6) ?
    C29C C30C . 1.391(7) ?
    C29C H29C . 0.95 ?
    C30C C37C . 1.520(6) ?
    C31C C32C . 1.389(6) ?
    C31C C36C . 1.392(6) ?
    C32C C33C . 1.380(7) ?
    C32C H32C . 0.95 ?
    C33C C34C . 1.369(7) ?
    C33C H33C . 0.95 ?
    C34C C35C . 1.386(6) ?
    C34C H34C . 0.95 ?
    C35C C36C . 1.379(7) ?
    C35C H35C . 0.95 ?
    C36C H36C . 0.95 ?
    C37C C42C . 1.378(7) ?
    C37C C38C . 1.391(6) ?
    C38C C39C . 1.393(6) ?
    C38C H38C . 0.95 ?
    C39C C40C . 1.362(7) ?
    C39C H39C . 0.95 ?
    C40C C41C . 1.397(7) ?
    C40C H40C . 0.95 ?
    C41C C42C . 1.384(7) ?
    C41C H41C . 0.95 ?
    C42C H42C . 0.95 ?
    C43C C44C . 1.397(6) ?
    C43C C46C . 1.506(6) ?
    C44C C45C . 1.402(6) ?
    C44C H44C . 0.95 ?
    C45C C52C . 1.511(6) ?
    C46C C51C . 1.369(6) ?
    C46C C47C . 1.394(6) ?
    C47C C48C . 1.383(6) ?
    C47C H47C . 0.95 ?
    C48C C49C . 1.374(6) ?
    C48C H48C . 0.95 ?
    C49C C50C . 1.376(7) ?
    C49C H49C . 0.95 ?
    C50C C51C . 1.380(7) ?
    C50C H50C . 0.95 ?
    C51C H51C . 0.95 ?
    C52C C57C . 1.368(7) ?
    C52C C53C . 1.401(6) ?
    C53C C54C . 1.390(7) ?
    C53C H53C . 0.95 ?
    C54C C55C . 1.336(8) ?
    C54C H54C . 0.95 ?
    C55C C56C . 1.374(9) ?
    C55C H55C . 0.95 ?
    C56C C57C . 1.403(8) ?
    C56C H56C . 0.95 ?
    C57C H57C . 0.95 ?
    Eu1D O1D . 2.338(3) ?
    Eu1D O2D . 2.349(3) ?
    Eu1D O4D . 2.353(3) ?
    Eu1D O5D . 2.355(3) ?
    Eu1D O6D . 2.371(3) ?
    Eu1D O3D . 2.377(3) ?
    Eu1D N2D . 2.625(4) ?
    Eu1D N1D . 2.640(4) ?
    N1D C1D . 1.318(5) ?
    N1D C12D . 1.359(6) ?
    O1D C13D . 1.275(5) ?
    C1D C2D . 1.393(6) ?
    C1D H1DA . 0.95 ?
    N2D C10D . 1.324(6) ?
    N2D C11D . 1.372(5) ?
    O2D C15D . 1.285(4) ?
    C2D C3D . 1.375(6) ?
    C2D H2DA . 0.95 ?
    O3D C28D . 1.270(5) ?
    C3D C4D . 1.399(7) ?
    C3D H3DA . 0.95 ?
    O4D C30D . 1.278(5) ?
    C4D C12D . 1.419(6) ?
    C4D C5D . 1.429(7) ?
    O5D C43D . 1.275(5) ?
    C5D C6D . 1.350(7) ?
    C5D H5DA . 0.95 ?
    O6D C45D . 1.275(5) ?
    C6D C7D . 1.433(6) ?
    C6D H6DA . 0.95 ?
    C7D C8D . 1.403(6) ?
    C7D C11D . 1.409(6) ?
    C8D C9D . 1.375(6) ?
    C8D H8DA . 0.95 ?
    C9D C10D . 1.399(6) ?
    C9D H9DA . 0.95 ?
    C10D H10D . 0.95 ?
    C11D C12D . 1.440(6) ?
    C13D C14D . 1.392(6) ?
    C13D C16D . 1.501(6) ?
    C14D C15D . 1.403(6) ?
    C14D H14D . 0.95 ?
    C15D C22D . 1.501(6) ?
    C16D C17D . 1.384(6) ?
    C16D C21D . 1.393(6) ?
    C17D C18D . 1.387(5) ?
    C17D H17D . 0.95 ?
    C18D C19D . 1.377(6) ?
    C18D H18D . 0.95 ?
    C19D C20D . 1.381(7) ?
    C19D H19D . 0.95 ?
    C20D C21D . 1.376(6) ?
    C20D H20D . 0.95 ?
    C21D H21D . 0.95 ?
    C22D C23D . 1.393(6) ?
    C22D C27D . 1.408(6) ?
    C23D C24D . 1.377(6) ?
    C23D H23D . 0.95 ?
    C24D C25D . 1.395(7) ?
    C24D H24D . 0.95 ?
    C25D C26D . 1.369(7) ?
    C25D H25D . 0.95 ?
    C26D C27D . 1.377(6) ?
    C26D H26D . 0.95 ?
    C27D H27D . 0.95 ?
    C28D C29D . 1.408(6) ?
    C28D C31D . 1.508(6) ?
    C29D C30D . 1.390(6) ?
    C29D H29D . 0.95 ?
    C30D C37D . 1.508(6) ?
    C31D C36D . 1.383(6) ?
    C31D C32D . 1.401(5) ?
    C32D C33D . 1.378(6) ?
    C32D H32D . 0.95 ?
    C33D C34D . 1.369(6) ?
    C33D H33D . 0.95 ?
    C34D C35D . 1.390(6) ?
    C34D H34D . 0.95 ?
    C35D C36D . 1.383(6) ?
    C35D H35D . 0.95 ?
    C36D H36D . 0.95 ?
    C37D C42D . 1.378(6) ?
    C37D C38D . 1.401(5) ?
    C38D C39D . 1.386(6) ?
    C38D H38D . 0.95 ?
    C39D C40D . 1.353(7) ?
    C39D H39D . 0.95 ?
    C40D C41D . 1.394(7) ?
    C40D H40D . 0.95 ?
    C41D C42D . 1.396(6) ?
    C41D H41D . 0.95 ?
    C42D H42D . 0.95 ?
    C43D C44D . 1.401(6) ?
    C43D C46D . 1.499(6) ?
    C44D C45D . 1.396(6) ?
    C44D H44D . 0.95 ?
    C45D C52D . 1.502(6) ?
    C46D C51D . 1.392(6) ?
    C46D C47D . 1.399(6) ?
    C47D C48D . 1.376(6) ?
    C47D H47D . 0.95 ?
    C48D C49D . 1.390(6) ?
    C48D H48D . 0.95 ?
    C49D C50D . 1.384(6) ?
    C49D H49D . 0.95 ?
    C50D C51D . 1.381(6) ?
    C50D H50D . 0.95 ?
    C51D H51D . 0.95 ?
    C52D C53D . 1.398(5) ?
    C52D C57D . 1.402(6) ?
    C53D C54D . 1.382(6) ?
    C53D H53D . 0.95 ?
    C54D C55D . 1.381(6) ?
    C54D H54D . 0.95 ?
    C55D C56D . 1.383(6) ?
    C55D H55D . 0.95 ?
    C56D C57D . 1.393(6) ?
    C56D H56D . 0.95 ?
    C57D H57D . 0.95 ?
    Eu1E O5E . 2.331(3) ?
    Eu1E O4E . 2.339(3) ?
    Eu1E O3E . 2.342(3) ?
    Eu1E O6E . 2.344(3) ?
    Eu1E O1E . 2.361(3) ?
    Eu1E O2E . 2.365(3) ?
    Eu1E N1E . 2.626(4) ?
    Eu1E N2E . 2.641(4) ?
    N1E C1E . 1.320(6) ?
    N1E C12E . 1.361(6) ?
    O1E C13E . 1.262(5) ?
    C1E C2E . 1.408(6) ?
    C1E H1EA . 0.95 ?
    N2E C10E . 1.320(6) ?
    N2E C11E . 1.361(6) ?
    O2E C15E . 1.279(5) ?
    C2E C3E . 1.357(7) ?
    C2E H2EA . 0.95 ?
    O3E C28E . 1.269(5) ?
    C3E C4E . 1.396(7) ?
    C3E H3EA . 0.95 ?
    O4E C30E . 1.264(5) ?
    C4E C12E . 1.417(6) ?
    C4E C5E . 1.432(7) ?
    O5E C43E . 1.280(5) ?
    C5E C6E . 1.330(8) ?
    C5E H5EA . 0.95 ?
    O6E C45E . 1.277(5) ?
    C6E C7E . 1.432(7) ?
    C6E H6EA . 0.95 ?
    C7E C8E . 1.384(7) ?
    C7E C11E . 1.433(6) ?
    C8E C9E . 1.363(7) ?
    C8E H8EA . 0.95 ?
    C9E C10E . 1.396(7) ?
    C9E H9EA . 0.95 ?
    C10E H10E . 0.95 ?
    C11E C12E . 1.424(7) ?
    C13E C14E . 1.407(6) ?
    C13E C16E . 1.505(6) ?
    C14E C15E . 1.399(6) ?
    C14E H14E . 0.95 ?
    C15E C22E . 1.497(6) ?
    C16E C21E . 1.388(6) ?
    C16E C17E . 1.389(6) ?
    C17E C18E . 1.391(6) ?
    C17E H17E . 0.95 ?
    C18E C19E . 1.391(6) ?
    C18E H18E . 0.95 ?
    C19E C20E . 1.382(6) ?
    C19E H19E . 0.95 ?
    C20E C21E . 1.384(6) ?
    C20E H20E . 0.95 ?
    C21E H21E . 0.95 ?
    C22E C23E . 1.386(6) ?
    C22E C27E . 1.398(6) ?
    C23E C24E . 1.390(6) ?
    C23E H23E . 0.95 ?
    C24E C25E . 1.383(6) ?
    C24E H24E . 0.95 ?
    C25E C26E . 1.395(6) ?
    C25E H25E . 0.95 ?
    C26E C27E . 1.372(6) ?
    C26E H26E . 0.95 ?
    C27E H27E . 0.95 ?
    C28E C29E . 1.412(6) ?
    C28E C31E . 1.492(7) ?
    C29E C30E . 1.403(6) ?
    C29E H29E . 0.95 ?
    C30E C37E . 1.501(6) ?
    C31E C36E . 1.378(7) ?
    C31E C32E . 1.406(7) ?
    C32E C33E . 1.389(7) ?
    C32E H32E . 0.95 ?
    C33E C34E . 1.384(8) ?
    C33E H33E . 0.95 ?
    C34E C35E . 1.383(9) ?
    C34E H34E . 0.95 ?
    C35E C36E . 1.375(7) ?
    C35E H35E . 0.95 ?
    C36E H36E . 0.95 ?
    C37E C38E . 1.386(6) ?
    C37E C42E . 1.398(7) ?
    C38E C39E . 1.395(7) ?
    C38E H38E . 0.95 ?
    C39E C40E . 1.369(8) ?
    C39E H39E . 0.95 ?
    C40E C41E . 1.390(7) ?
    C40E H40E . 0.95 ?
    C41E C42E . 1.386(7) ?
    C41E H41E . 0.95 ?
    C42E H42E . 0.95 ?
    C43E C44E . 1.406(7) ?
    C43E C46E . 1.493(6) ?
    C44E C45E . 1.395(6) ?
    C44E H44E . 0.95 ?
    C45E C52E . 1.497(6) ?
    C46E C51E . 1.374(7) ?
    C46E C47E . 1.378(7) ?
    C47E C48E . 1.369(7) ?
    C47E H47E . 0.95 ?
    C48E C49E . 1.379(8) ?
    C48E H48E . 0.95 ?
    C49E C50E . 1.372(8) ?
    C49E H49E . 0.95 ?
    C50E C51E . 1.377(7) ?
    C50E H50E . 0.95 ?
    C51E H51E . 0.95 ?
    C52E C57E . 1.383(6) ?
    C52E C53E . 1.391(7) ?
    C53E C54E . 1.378(7) ?
    C53E H53E . 0.95 ?
    C54E C55E . 1.370(7) ?
    C54E H54E . 0.95 ?
    C55E C56E . 1.360(7) ?
    C55E H55E . 0.95 ?
    C56E C57E . 1.389(7) ?
    C56E H56E . 0.95 ?
    C57E H57F . 0.95 ?
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    O4A Eu1A O3A . . 71.83(10) y
    O4A Eu1A O1A . . 145.26(11) y
    O3A Eu1A O1A . . 142.83(10) y
    O4A Eu1A O6A . . 102.09(10) y
    O3A Eu1A O6A . . 75.14(10) y
    O1A Eu1A O6A . . 92.87(10) y
    O4A Eu1A O2A . . 139.52(10) y
    O3A Eu1A O2A . . 74.83(10) y
    O1A Eu1A O2A . . 70.21(10) y
    O6A Eu1A O2A . . 90.76(10) y
    O4A Eu1A O5A . . 81.57(10) y
    O3A Eu1A O5A . . 131.45(11) y
    O1A Eu1A O5A . . 73.60(10) y
    O6A Eu1A O5A . . 71.68(11) y
    O2A Eu1A O5A . . 138.69(9) y
    O4A Eu1A N1A . . 79.84(11) y
    O3A Eu1A N1A . . 76.26(11) y
    O1A Eu1A N1A . . 102.90(11) y
    O6A Eu1A N1A . . 149.03(12) y
    O2A Eu1A N1A . . 70.40(10) y
    O5A Eu1A N1A . . 138.23(11) y
    O4A Eu1A N2A . . 73.72(11) y
    O3A Eu1A N2A . . 129.17(10) y
    O1A Eu1A N2A . . 77.34(11) y
    O6A Eu1A N2A . . 148.95(12) y
    O2A Eu1A N2A . . 112.64(12) y
    O5A Eu1A N2A . . 77.29(12) y
    N1A Eu1A N2A . . 61.69(12) y
    C1A N1A C12A . . 117.7(4) ?
    C1A N1A Eu1A . . 121.0(3) ?
    C12A N1A Eu1A . . 121.1(3) ?
    C13A O1A Eu1A . . 137.8(3) y
    N1A C1A C2A . . 123.2(5) ?
    N1A C1A H1AA . . 118.4 ?
    C2A C1A H1AA . . 118.4 ?
    C10A N2A C11A . . 117.3(4) ?
    C10A N2A Eu1A . . 122.2(3) ?
    C11A N2A Eu1A . . 120.5(3) ?
    C15A O2A Eu1A . . 137.9(3) y
    C3A C2A C1A . . 119.1(5) ?
    C3A C2A H2AA . . 120.4 ?
    C1A C2A H2AA . . 120.4 ?
    C28A O3A Eu1A . . 135.3(3) y
    C2A C3A C4A . . 119.3(5) ?
    C2A C3A H3AA . . 120.4 ?
    C4A C3A H3AA . . 120.4 ?
    C30A O4A Eu1A . . 136.8(3) y
    C3A C4A C12A . . 118.5(5) ?
    C3A C4A C5A . . 122.7(5) ?
    C12A C4A C5A . . 118.8(5) ?
    C43A O5A Eu1A . . 135.9(3) y
    C6A C5A C4A . . 121.3(5) ?
    C6A C5A H5AA . . 119.3 ?
    C4A C5A H5AA . . 119.3 ?
    C45A O6A Eu1A . . 137.4(3) y
    C5A C6A C7A . . 121.3(5) ?
    C5A C6A H6AA . . 119.4 ?
    C7A C6A H6AA . . 119.4 ?
    C8A C7A C11A . . 117.9(5) ?
    C8A C7A C6A . . 122.9(5) ?
    C11A C7A C6A . . 119.3(5) ?
    C9A C8A C7A . . 119.8(6) ?
    C9A C8A H8AA . . 120.1 ?
    C7A C8A H8AA . . 120.1 ?
    C8A C9A C10A . . 119.5(6) ?
    C8A C9A H9AA . . 120.3 ?
    C10A C9A H9AA . . 120.3 ?
    N2A C10A C9A . . 123.5(6) ?
    N2A C10A H10A . . 118.2 ?
    C9A C10A H10A . . 118.2 ?
    N2A C11A C7A . . 122.0(5) ?
    N2A C11A C12A . . 118.2(4) ?
    C7A C11A C12A . . 119.8(4) ?
    N1A C12A C4A . . 122.2(5) ?
    N1A C12A C11A . . 118.4(4) ?
    C4A C12A C11A . . 119.5(4) ?
    O1A C13A C14A . . 123.9(4) y
    O1A C13A C16A . . 115.0(4) y
    C14A C13A C16A . . 121.1(4) y
    C15A C14A C13A . . 123.5(4) y
    C15A C14A H14A . . 118.3 ?
    C13A C14A H14A . . 118.3 ?
    O2A C15A C14A . . 123.7(4) y
    O2A C15A C22A . . 116.5(4) y
    C14A C15A C22A . . 119.8(4) y
    C17A C16A C21A . . 118.8(4) ?
    C17A C16A C13A . . 118.9(4) ?
    C21A C16A C13A . . 122.3(4) ?
    C18A C17A C16A . . 120.7(5) ?
    C18A C17A H17A . . 119.6 ?
    C16A C17A H17A . . 119.6 ?
    C17A C18A C19A . . 119.6(5) ?
    C17A C18A H18A . . 120.2 ?
    C19A C18A H18A . . 120.2 ?
    C20A C19A C18A . . 120.1(5) ?
    C20A C19A H19A . . 120.0 ?
    C18A C19A H19A . . 120.0 ?
    C19A C20A C21A . . 120.1(5) ?
    C19A C20A H20A . . 120.0 ?
    C21A C20A H20A . . 120.0 ?
    C20A C21A C16A . . 120.7(5) ?
    C20A C21A H21A . . 119.7 ?
    C16A C21A H21A . . 119.7 ?
    C23A C22A C27A . . 118.0(4) ?
    C23A C22A C15A . . 123.8(4) ?
    C27A C22A C15A . . 118.2(4) ?
    C24A C23A C22A . . 120.9(5) ?
    C24A C23A H23A . . 119.5 ?
    C22A C23A H23A . . 119.5 ?
    C23A C24A C25A . . 120.2(5) ?
    C23A C24A H24A . . 119.9 ?
    C25A C24A H24A . . 119.9 ?
    C26A C25A C24A . . 119.9(5) ?
    C26A C25A H25A . . 120.1 ?
    C24A C25A H25A . . 120.1 ?
    C25A C26A C27A . . 119.4(5) ?
    C25A C26A H26A . . 120.3 ?
    C27A C26A H26A . . 120.3 ?
    C26A C27A C22A . . 121.5(4) ?
    C26A C27A H27A . . 119.3 ?
    C22A C27A H27A . . 119.3 ?
    O3A C28A C29A . . 123.6(4) y
    O3A C28A C31A . . 114.9(4) y
    C29A C28A C31A . . 121.4(4) y
    C28A C29A C30A . . 124.2(4) y
    C28A C29A H29A . . 117.9 ?
    C30A C29A H29A . . 117.9 ?
    O4A C30A C29A . . 123.8(4) y
    O4A C30A C37A . . 115.4(4) y
    C29A C30A C37A . . 120.8(4) y
    C36A C31A C32A . . 117.8(5) ?
    C36A C31A C28A . . 123.4(4) ?
    C32A C31A C28A . . 118.8(4) ?
    C33A C32A C31A . . 120.4(5) ?
    C33A C32A H32A . . 119.8 ?
    C31A C32A H32A . . 119.8 ?
    C34A C33A C32A . . 120.9(5) ?
    C34A C33A H33A . . 119.5 ?
    C32A C33A H33A . . 119.5 ?
    C33A C34A C35A . . 119.6(5) ?
    C33A C34A H34A . . 120.2 ?
    C35A C34A H34A . . 120.2 ?
    C34A C35A C36A . . 120.0(5) ?
    C34A C35A H35A . . 120.0 ?
    C36A C35A H35A . . 120.0 ?
    C35A C36A C31A . . 121.2(5) ?
    C35A C36A H36A . . 119.4 ?
    C31A C36A H36A . . 119.4 ?
    C42A C37A C38A . . 118.1(4) ?
    C42A C37A C30A . . 118.9(4) ?
    C38A C37A C30A . . 123.0(4) ?
    C39A C38A C37A . . 120.5(5) ?
    C39A C38A H38A . . 119.8 ?
    C37A C38A H38A . . 119.8 ?
    C40A C39A C38A . . 120.4(5) ?
    C40A C39A H39A . . 119.8 ?
    C38A C39A H39A . . 119.8 ?
    C41A C40A C39A . . 119.8(5) ?
    C41A C40A H40A . . 120.1 ?
    C39A C40A H40A . . 120.1 ?
    C40A C41A C42A . . 119.8(5) ?
    C40A C41A H41A . . 120.1 ?
    C42A C41A H41A . . 120.1 ?
    C37A C42A C41A . . 121.5(5) ?
    C37A C42A H42A . . 119.3 ?
    C41A C42A H42A . . 119.3 ?
    O5A C43A C44A . . 124.3(4) y
    O5A C43A C46A . . 118.4(4) y
    C44A C43A C46A . . 117.3(4) y
    C45A C44A C43A . . 125.0(4) y
    C45A C44A H44A . . 117.5 ?
    C43A C44A H44A . . 117.5 ?
    O6A C45A C44A . . 124.5(4) y
    O6A C45A C52A . . 116.4(4) y
    C44A C45A C52A . . 119.0(4) y
    C51A C46A C47A . . 117.7(5) ?
    C51A C46A C43A . . 122.8(5) ?
    C47A C46A C43A . . 119.4(5) ?
    C48A C47A C46A . . 121.2(6) ?
    C48A C47A H47A . . 119.4 ?
    C46A C47A H47A . . 119.4 ?
    C47A C48A C49A . . 119.8(6) ?
    C47A C48A H48A . . 120.1 ?
    C49A C48A H48A . . 120.1 ?
    C50A C49A C48A . . 119.7(6) ?
    C50A C49A H49A . . 120.1 ?
    C48A C49A H49A . . 120.1 ?
    C51A C50A C49A . . 120.1(6) ?
    C51A C50A H50A . . 120.0 ?
    C49A C50A H50A . . 120.0 ?
    C50A C51A C46A . . 121.5(6) ?
    C50A C51A H51A . . 119.3 ?
    C46A C51A H51A . . 119.3 ?
    C57A C52A C53A . . 118.0(4) ?
    C57A C52A C45A . . 119.8(4) ?
    C53A C52A C45A . . 122.2(4) ?
    C54A C53A C52A . . 120.1(5) ?
    C54A C53A H53A . . 119.9 ?
    C52A C53A H53A . . 119.9 ?
    C55A C54A C53A . . 120.6(5) ?
    C55A C54A H54A . . 119.7 ?
    C53A C54A H54A . . 119.7 ?
    C54A C55A C56A . . 120.6(5) ?
    C54A C55A H55A . . 119.7 ?
    C56A C55A H55A . . 119.7 ?
    C57A C56A C55A . . 118.4(5) ?
    C57A C56A H56A . . 120.8 ?
    C55A C56A H56A . . 120.8 ?
    C52A C57A C56A . . 122.2(4) ?
    C52A C57A H57A . . 118.9 ?
    C56A C57A H57A . . 118.9 ?
    O4B Eu1B O3B . . 71.10(11) ?
    O4B Eu1B O5B . . 82.57(10) ?
    O3B Eu1B O5B . . 137.06(11) ?
    O4B Eu1B O2B . . 145.96(10) ?
    O3B Eu1B O2B . . 76.22(11) ?
    O5B Eu1B O2B . . 129.55(10) ?
    O4B Eu1B O1B . . 138.45(10) ?
    O3B Eu1B O1B . . 145.37(11) ?
    O5B Eu1B O1B . . 74.70(11) ?
    O2B Eu1B O1B . . 70.56(11) ?
    O4B Eu1B O6B . . 100.71(11) ?
    O3B Eu1B O6B . . 80.99(11) ?
    O5B Eu1B O6B . . 71.09(11) ?
    O2B Eu1B O6B . . 83.08(11) ?
    O1B Eu1B O6B . . 104.02(10) ?
    O4B Eu1B N1B . . 90.08(11) ?
    O3B Eu1B N1B . . 78.94(13) ?
    O5B Eu1B N1B . . 135.66(13) ?
    O2B Eu1B N1B . . 74.33(11) ?
    O1B Eu1B N1B . . 82.93(12) ?
    O6B Eu1B N1B . . 152.71(13) ?
    O4B Eu1B N2B . . 71.26(11) ?
    O3B Eu1B N2B . . 124.28(10) ?
    O5B Eu1B N2B . . 74.66(11) ?
    O2B Eu1B N2B . . 122.73(12) ?
    O1B Eu1B N2B . . 69.42(10) ?
    O6B Eu1B N2B . . 145.59(12) ?
    N1B Eu1B N2B . . 61.66(13) ?
    C1B N1B C12B . . 117.4(5) ?
    C1B N1B Eu1B . . 122.2(4) ?
    C12B N1B Eu1B . . 118.9(3) ?
    C13B O1B Eu1B . . 137.9(3) ?
    N1B C1B C2B . . 124.1(6) ?
    N1B C1B H1BA . . 117.9 ?
    C2B C1B H1BA . . 117.9 ?
    C10B N2B C11B . . 117.7(4) ?
    C10B N2B Eu1B . . 122.5(3) ?
    C11B N2B Eu1B . . 118.7(3) ?
    C15B O2B Eu1B . . 137.3(3) ?
    C3B C2B C1B . . 118.2(6) ?
    C3B C2B H2BA . . 120.9 ?
    C1B C2B H2BA . . 120.9 ?
    C28B O3B Eu1B . . 138.6(3) ?
    C2B C3B C4B . . 120.5(6) ?
    C2B C3B H3BA . . 119.8 ?
    C4B C3B H3BA . . 119.8 ?
    C30B O4B Eu1B . . 139.1(3) ?
    C12B C4B C3B . . 117.3(6) ?
    C12B C4B C5B . . 119.5(6) ?
    C3B C4B C5B . . 123.1(6) ?
    C43B O5B Eu1B . . 138.2(3) ?
    C6B C5B C4B . . 121.3(6) ?
    C6B C5B H5BA . . 119.3 ?
    C4B C5B H5BA . . 119.3 ?
    C45B O6B Eu1B . . 137.3(3) ?
    C5B C6B C7B . . 120.9(6) ?
    C5B C6B H6BA . . 119.5 ?
    C7B C6B H6BA . . 119.5 ?
    C8B C7B C11B . . 116.6(5) ?
    C8B C7B C6B . . 123.9(6) ?
    C11B C7B C6B . . 119.4(6) ?
    C9B C8B C7B . . 121.1(5) ?
    C9B C8B H8BA . . 119.4 ?
    C7B C8B H8BA . . 119.4 ?
    C8B C9B C10B . . 118.1(6) ?
    C8B C9B H9BA . . 121.0 ?
    C10B C9B H9BA . . 121.0 ?
    N2B C10B C9B . . 123.7(5) ?
    N2B C10B H10B . . 118.2 ?
    C9B C10B H10B . . 118.2 ?
    N2B C11B C7B . . 122.6(5) ?
    N2B C11B C12B . . 118.0(5) ?
    C7B C11B C12B . . 119.4(5) ?
    N1B C12B C4B . . 122.4(5) ?
    N1B C12B C11B . . 118.1(5) ?
    C4B C12B C11B . . 119.5(5) ?
    O1B C13B C14B . . 124.4(4) ?
    O1B C13B C16B . . 116.3(4) ?
    C14B C13B C16B . . 119.2(4) ?
    C13B C14B C15B . . 122.6(4) ?
    C13B C14B H14B . . 118.7 ?
    C15B C14B H14B . . 118.7 ?
    O2B C15B C14B . . 124.5(4) ?
    O2B C15B C22B . . 116.5(4) ?
    C14B C15B C22B . . 118.8(4) ?
    C21B C16B C17B . . 118.6(4) ?
    C21B C16B C13B . . 124.1(4) ?
    C17B C16B C13B . . 117.3(4) ?
    C16B C17B C18B . . 120.6(5) ?
    C16B C17B H17B . . 119.7 ?
    C18B C17B H17B . . 119.7 ?
    C19B C18B C17B . . 119.5(5) ?
    C19B C18B H18B . . 120.2 ?
    C17B C18B H18B . . 120.2 ?
    C20B C19B C18B . . 119.9(5) ?
    C20B C19B H19B . . 120.1 ?
    C18B C19B H19B . . 120.1 ?
    C21B C20B C19B . . 120.4(5) ?
    C21B C20B H20B . . 119.8 ?
    C19B C20B H20B . . 119.8 ?
    C20B C21B C16B . . 121.0(5) ?
    C20B C21B H21B . . 119.5 ?
    C16B C21B H21B . . 119.5 ?
    C23B C22B C27B . . 118.0(5) ?
    C23B C22B C15B . . 124.6(5) ?
    C27B C22B C15B . . 117.4(4) ?
    C22B C23B C24B . . 121.1(5) ?
    C22B C23B H23B . . 119.5 ?
    C24B C23B H23B . . 119.5 ?
    C23B C24B C25B . . 119.9(5) ?
    C23B C24B H24B . . 120.0 ?
    C25B C24B H24B . . 120.0 ?
    C26B C25B C24B . . 119.1(6) ?
    C26B C25B H25B . . 120.5 ?
    C24B C25B H25B . . 120.5 ?
    C25B C26B C27B . . 121.1(6) ?
    C25B C26B H26B . . 119.5 ?
    C27B C26B H26B . . 119.5 ?
    C26B C27B C22B . . 120.8(5) ?
    C26B C27B H27B . . 119.6 ?
    C22B C27B H27B . . 119.6 ?
    O3B C28B C29B . . 123.0(4) ?
    O3B C28B C31B . . 116.3(4) ?
    C29B C28B C31B . . 120.7(4) ?
    C28B C29B C30B . . 124.4(4) ?
    C28B C29B H29B . . 117.8 ?
    C30B C29B H29B . . 117.8 ?
    O4B C30B C29B . . 123.3(4) ?
    O4B C30B C37B . . 115.8(4) ?
    C29B C30B C37B . . 120.9(4) ?
    C32B C31B C36B . . 117.2(5) ?
    C32B C31B C28B . . 118.7(4) ?
    C36B C31B C28B . . 124.0(4) ?
    C33B C32B C31B . . 121.8(5) ?
    C33B C32B H32B . . 119.1 ?
    C31B C32B H32B . . 119.1 ?
    C32B C33B C34B . . 120.2(5) ?
    C32B C33B H33B . . 119.9 ?
    C34B C33B H33B . . 119.9 ?
    C35B C34B C33B . . 119.2(5) ?
    C35B C34B H34B . . 120.4 ?
    C33B C34B H34B . . 120.4 ?
    C34B C35B C36B . . 120.5(5) ?
    C34B C35B H35B . . 119.7 ?
    C36B C35B H35B . . 119.7 ?
    C31B C36B C35B . . 121.0(4) ?
    C31B C36B H36B . . 119.5 ?
    C35B C36B H36B . . 119.5 ?
    C38B C37B C42B . . 119.0(4) ?
    C38B C37B C30B . . 122.6(4) ?
    C42B C37B C30B . . 118.4(4) ?
    C39B C38B C37B . . 120.2(5) ?
    C39B C38B H38B . . 119.9 ?
    C37B C38B H38B . . 119.9 ?
    C40B C39B C38B . . 120.4(5) ?
    C40B C39B H39B . . 119.8 ?
    C38B C39B H39B . . 119.8 ?
    C39B C40B C41B . . 120.1(4) ?
    C39B C40B H40B . . 119.9 ?
    C41B C40B H40B . . 119.9 ?
    C42B C41B C40B . . 119.6(5) ?
    C42B C41B H41B . . 120.2 ?
    C40B C41B H41B . . 120.2 ?
    C41B C42B C37B . . 120.5(4) ?
    C41B C42B H42B . . 119.7 ?
    C37B C42B H42B . . 119.7 ?
    O5B C43B C44B . . 124.4(4) ?
    O5B C43B C46B . . 116.0(4) ?
    C44B C43B C46B . . 119.5(4) ?
    C43B C44B C45B . . 123.5(4) y
    C43B C44B H44B . . 118.3 ?
    C45B C44B H44B . . 118.3 ?
    O6B C45B C44B . . 124.6(4) ?
    O6B C45B C52B . . 115.8(4) ?
    C44B C45B C52B . . 119.6(4) ?
    C51B C46B C47B . . 118.4(5) ?
    C51B C46B C43B . . 122.4(5) ?
    C47B C46B C43B . . 119.2(5) ?
    C48B C47B C46B . . 120.6(5) ?
    C48B C47B H47B . . 119.7 ?
    C46B C47B H47B . . 119.7 ?
    C47B C48B C49B . . 120.1(5) ?
    C47B C48B H48B . . 119.9 ?
    C49B C48B H48B . . 119.9 ?
    C50B C49B C48B . . 119.4(5) ?
    C50B C49B H49B . . 120.3 ?
    C48B C49B H49B . . 120.3 ?
    C49B C50B C51B . . 121.1(5) ?
    C49B C50B H50B . . 119.4 ?
    C51B C50B H50B . . 119.4 ?
    C50B C51B C46B . . 120.4(5) ?
    C50B C51B H51B . . 119.8 ?
    C46B C51B H51B . . 119.8 ?
    C57B C52B C53B . . 118.8(4) ?
    C57B C52B C45B . . 119.4(4) ?
    C53B C52B C45B . . 121.8(5) ?
    C54B C53B C52B . . 120.1(5) ?
    C54B C53B H53B . . 120.0 ?
    C52B C53B H53B . . 120.0 ?
    C55B C54B C53B . . 120.1(5) ?
    C55B C54B H54B . . 120.0 ?
    C53B C54B H54B . . 120.0 ?
    C54B C55B C56B . . 120.2(5) ?
    C54B C55B H55B . . 119.9 ?
    C56B C55B H55B . . 119.9 ?
    C57B C56B C55B . . 119.9(6) ?
    C57B C56B H56B . . 120.1 ?
    C55B C56B H56B . . 120.1 ?
    C52B C57B C56B . . 120.9(5) ?
    C52B C57B H57B . . 119.6 ?
    C56B C57B H57B . . 119.6 ?
    O5C Eu1C O1C . . 141.71(10) ?
    O5C Eu1C O3C . . 140.85(9) ?
    O1C Eu1C O3C . . 76.36(10) ?
    O5C Eu1C O4C . . 83.26(11) ?
    O1C Eu1C O4C . . 109.34(11) ?
    O3C Eu1C O4C . . 71.57(11) ?
    O5C Eu1C O6C . . 71.40(10) ?
    O1C Eu1C O6C . . 139.49(10) ?
    O3C Eu1C O6C . . 80.91(11) ?
    O4C Eu1C O6C . . 94.32(10) ?
    O5C Eu1C O2C . . 75.70(10) ?
    O1C Eu1C O2C . . 70.92(10) ?
    O3C Eu1C O2C . . 127.23(11) ?
    O4C Eu1C O2C . . 81.59(10) ?
    O6C Eu1C O2C . . 147.10(10) ?
    O5C Eu1C N1C . . 75.36(11) ?
    O1C Eu1C N1C . . 78.69(10) ?
    O3C Eu1C N1C . . 135.93(11) ?
    O4C Eu1C N1C . . 151.96(12) ?
    O6C Eu1C N1C . . 95.80(11) ?
    O2C Eu1C N1C . . 75.75(11) ?
    O5C Eu1C N2C . . 117.60(12) ?
    O1C Eu1C N2C . . 72.07(11) ?
    O3C Eu1C N2C . . 75.82(11) ?
    O4C Eu1C N2C . . 145.73(12) ?
    O6C Eu1C N2C . . 70.07(10) ?
    O2C Eu1C N2C . . 127.99(10) ?
    N1C Eu1C N2C . . 62.11(12) ?
    C1C N1C C12C . . 117.0(4) ?
    C1C N1C Eu1C . . 121.7(3) ?
    C12C N1C Eu1C . . 121.2(3) ?
    C13C O1C Eu1C . . 138.3(3) ?
    N1C C1C C2C . . 124.4(5) ?
    N1C C1C H1CA . . 117.8 ?
    C2C C1C H1CA . . 117.8 ?
    C10C N2C C11C . . 118.9(4) ?
    C10C N2C Eu1C . . 121.1(3) ?
    C11C N2C Eu1C . . 119.9(3) ?
    C15C O2C Eu1C . . 135.3(3) ?
    C3C C2C C1C . . 118.4(5) ?
    C3C C2C H2CA . . 120.8 ?
    C1C C2C H2CA . . 120.8 ?
    C28C O3C Eu1C . . 138.4(3) ?
    C2C C3C C4C . . 119.3(5) ?
    C2C C3C H3CA . . 120.4 ?
    C4C C3C H3CA . . 120.4 ?
    C30C O4C Eu1C . . 136.8(3) ?
    C3C C4C C12C . . 118.1(5) ?
    C3C C4C C5C . . 122.8(5) ?
    C12C C4C C5C . . 119.1(5) ?
    C43C O5C Eu1C . . 138.5(3) ?
    C6C C5C C4C . . 121.3(5) ?
    C6C C5C H5CA . . 119.4 ?
    C4C C5C H5CA . . 119.4 ?
    C45C O6C Eu1C . . 137.0(3) ?
    C5C C6C C7C . . 121.7(5) ?
    C5C C6C H6CA . . 119.1 ?
    C7C C6C H6CA . . 119.1 ?
    C8C C7C C11C . . 117.4(4) ?
    C8C C7C C6C . . 123.3(5) ?
    C11C C7C C6C . . 119.3(5) ?
    C9C C8C C7C . . 120.7(5) ?
    C9C C8C H8CA . . 119.7 ?
    C7C C8C H8CA . . 119.7 ?
    C8C C9C C10C . . 118.7(5) ?
    C8C C9C H9CA . . 120.6 ?
    C10C C9C H9CA . . 120.6 ?
    N2C C10C C9C . . 122.3(5) ?
    N2C C10C H10C . . 118.8 ?
    C9C C10C H10C . . 118.8 ?
    N2C C11C C7C . . 122.0(4) ?
    N2C C11C C12C . . 118.6(4) ?
    C7C C11C C12C . . 119.3(4) ?
    N1C C12C C4C . . 122.8(5) ?
    N1C C12C C11C . . 117.9(4) ?
    C4C C12C C11C . . 119.3(4) ?
    O1C C13C C14C . . 123.9(4) ?
    O1C C13C C16C . . 115.1(4) ?
    C14C C13C C16C . . 121.0(4) ?
    C13C C14C C15C . . 124.5(4) ?
    C13C C14C H14C . . 117.8 ?
    C15C C14C H14C . . 117.8 ?
    O2C C15C C14C . . 123.6(4) ?
    O2C C15C C22C . . 117.0(4) ?
    C14C C15C C22C . . 119.4(4) ?
    C17C C16C C21C . . 118.5(4) ?
    C17C C16C C13C . . 119.0(4) ?
    C21C C16C C13C . . 122.5(4) ?
    C16C C17C C18C . . 121.9(4) ?
    C16C C17C H17C . . 119.0 ?
    C18C C17C H17C . . 119.0 ?
    C19C C18C C17C . . 118.9(5) ?
    C19C C18C H18C . . 120.5 ?
    C17C C18C H18C . . 120.5 ?
    C20C C19C C18C . . 120.4(4) ?
    C20C C19C H19C . . 119.8 ?
    C18C C19C H19C . . 119.8 ?
    C19C C20C C21C . . 119.9(5) ?
    C19C C20C H20C . . 120.1 ?
    C21C C20C H20C . . 120.1 ?
    C16C C21C C20C . . 120.4(5) ?
    C16C C21C H21C . . 119.8 ?
    C20C C21C H21C . . 119.8 ?
    C27C C22C C23C . . 118.4(4) ?
    C27C C22C C15C . . 119.2(4) ?
    C23C C22C C15C . . 122.4(4) ?
    C24C C23C C22C . . 120.9(4) ?
    C24C C23C H23C . . 119.5 ?
    C22C C23C H23C . . 119.5 ?
    C23C C24C C25C . . 120.7(4) ?
    C23C C24C H24C . . 119.6 ?
    C25C C24C H24C . . 119.6 ?
    C24C C25C C26C . . 118.7(5) ?
    C24C C25C H25C . . 120.6 ?
    C26C C25C H25C . . 120.6 ?
    C27C C26C C25C . . 120.9(5) ?
    C27C C26C H26C . . 119.5 ?
    C25C C26C H26C . . 119.5 ?
    C26C C27C C22C . . 120.4(4) ?
    C26C C27C H27C . . 119.8 ?
    C22C C27C H27C . . 119.8 ?
    O3C C28C C29C . . 123.4(5) ?
    O3C C28C C31C . . 116.3(4) ?
    C29C C28C C31C . . 120.3(4) ?
    C30C C29C C28C . . 124.2(5) ?
    C30C C29C H29C . . 117.9 ?
    C28C C29C H29C . . 117.9 ?
    O4C C30C C29C . . 125.3(4) ?
    O4C C30C C37C . . 116.2(4) ?
    C29C C30C C37C . . 118.5(4) ?
    C32C C31C C36C . . 118.4(5) ?
    C32C C31C C28C . . 119.3(4) ?
    C36C C31C C28C . . 122.3(4) ?
    C33C C32C C31C . . 120.8(5) ?
    C33C C32C H32C . . 119.6 ?
    C31C C32C H32C . . 119.6 ?
    C34C C33C C32C . . 120.4(5) ?
    C34C C33C H33C . . 119.8 ?
    C32C C33C H33C . . 119.8 ?
    C33C C34C C35C . . 119.7(5) ?
    C33C C34C H34C . . 120.2 ?
    C35C C34C H34C . . 120.2 ?
    C36C C35C C34C . . 120.2(5) ?
    C36C C35C H35C . . 119.9 ?
    C34C C35C H35C . . 119.9 ?
    C35C C36C C31C . . 120.5(4) ?
    C35C C36C H36C . . 119.7 ?
    C31C C36C H36C . . 119.7 ?
    C42C C37C C38C . . 119.2(4) ?
    C42C C37C C30C . . 118.8(4) ?
    C38C C37C C30C . . 121.9(5) ?
    C37C C38C C39C . . 119.7(5) ?
    C37C C38C H38C . . 120.2 ?
    C39C C38C H38C . . 120.2 ?
    C40C C39C C38C . . 120.4(5) ?
    C40C C39C H39C . . 119.8 ?
    C38C C39C H39C . . 119.8 ?
    C39C C40C C41C . . 120.7(5) ?
    C39C C40C H40C . . 119.7 ?
    C41C C40C H40C . . 119.7 ?
    C42C C41C C40C . . 118.5(6) ?
    C42C C41C H41C . . 120.7 ?
    C40C C41C H41C . . 120.7 ?
    C37C C42C C41C . . 121.4(5) ?
    C37C C42C H42C . . 119.3 ?
    C41C C42C H42C . . 119.3 ?
    O5C C43C C44C . . 124.7(4) ?
    O5C C43C C46C . . 114.8(4) ?
    C44C C43C C46C . . 120.5(4) ?
    C43C C44C C45C . . 123.2(4) ?
    C43C C44C H44C . . 118.4 ?
    C45C C44C H44C . . 118.4 ?
    O6C C45C C44C . . 124.5(4) ?
    O6C C45C C52C . . 116.3(4) ?
    C44C C45C C52C . . 119.2(4) ?
    C51C C46C C47C . . 118.0(4) ?
    C51C C46C C43C . . 124.4(4) ?
    C47C C46C C43C . . 117.6(4) ?
    C48C C47C C46C . . 121.1(4) ?
    C48C C47C H47C . . 119.5 ?
    C46C C47C H47C . . 119.5 ?
    C49C C48C C47C . . 120.3(5) ?
    C49C C48C H48C . . 119.9 ?
    C47C C48C H48C . . 119.9 ?
    C48C C49C C50C . . 118.5(5) ?
    C48C C49C H49C . . 120.8 ?
    C50C C49C H49C . . 120.8 ?
    C49C C50C C51C . . 121.4(5) ?
    C49C C50C H50C . . 119.3 ?
    C51C C50C H50C . . 119.3 ?
    C46C C51C C50C . . 120.7(5) ?
    C46C C51C H51C . . 119.7 ?
    C50C C51C H51C . . 119.7 ?
    C57C C52C C53C . . 119.0(5) ?
    C57C C52C C45C . . 118.5(5) ?
    C53C C52C C45C . . 122.4(5) ?
    C54C C53C C52C . . 119.2(5) ?
    C54C C53C H53C . . 120.4 ?
    C52C C53C H53C . . 120.4 ?
    C55C C54C C53C . . 121.3(6) ?
    C55C C54C H54C . . 119.3 ?
    C53C C54C H54C . . 119.3 ?
    C54C C55C C56C . . 120.7(6) ?
    C54C C55C H55C . . 119.7 ?
    C56C C55C H55C . . 119.7 ?
    C55C C56C C57C . . 119.3(7) ?
    C55C C56C H56C . . 120.4 ?
    C57C C56C H56C . . 120.4 ?
    C52C C57C C56C . . 120.5(6) ?
    C52C C57C H57C . . 119.8 ?
    C56C C57C H57C . . 119.8 ?
    O1D Eu1D O2D . . 72.02(10) ?
    O1D Eu1D O4D . . 112.52(10) ?
    O2D Eu1D O4D . . 78.45(10) ?
    O1D Eu1D O5D . . 135.71(9) ?
    O2D Eu1D O5D . . 76.78(10) ?
    O4D Eu1D O5D . . 90.57(10) ?
    O1D Eu1D O6D . . 142.93(10) ?
    O2D Eu1D O6D . . 144.80(10) ?
    O4D Eu1D O6D . . 86.77(10) ?
    O5D Eu1D O6D . . 71.57(10) ?
    O1D Eu1D O3D . . 77.07(9) ?
    O2D Eu1D O3D . . 123.64(11) ?
    O4D Eu1D O3D . . 71.56(10) ?
    O5D Eu1D O3D . . 147.21(9) ?
    O6D Eu1D O3D . . 79.97(10) ?
    O1D Eu1D N2D . . 73.56(10) ?
    O2D Eu1D N2D . . 134.40(9) ?
    O4D Eu1D N2D . . 143.42(11) ?
    O5D Eu1D N2D . . 110.15(11) ?
    O6D Eu1D N2D . . 72.66(10) ?
    O3D Eu1D N2D . . 75.21(11) ?
    O1D Eu1D N1D . . 73.05(10) ?
    O2D Eu1D N1D . . 79.25(11) ?
    O4D Eu1D N1D . . 153.71(11) ?
    O5D Eu1D N1D . . 70.85(10) ?
    O6D Eu1D N1D . . 103.90(10) ?
    O3D Eu1D N1D . . 133.45(11) ?
    N2D Eu1D N1D . . 62.62(11) ?
    C1D N1D C12D . . 117.9(4) ?
    C1D N1D Eu1D . . 122.0(3) ?
    C12D N1D Eu1D . . 120.0(3) ?
    C13D O1D Eu1D . . 135.9(3) ?
    N1D C1D C2D . . 124.2(4) ?
    N1D C1D H1DA . . 117.9 ?
    C2D C1D H1DA . . 117.9 ?
    C10D N2D C11D . . 117.7(4) ?
    C10D N2D Eu1D . . 121.7(3) ?
    C11D N2D Eu1D . . 120.6(3) ?
    C15D O2D Eu1D . . 135.0(3) ?
    C3D C2D C1D . . 118.4(5) ?
    C3D C2D H2DA . . 120.8 ?
    C1D C2D H2DA . . 120.8 ?
    C28D O3D Eu1D . . 137.0(3) ?
    C2D C3D C4D . . 119.9(4) ?
    C2D C3D H3DA . . 120.1 ?
    C4D C3D H3DA . . 120.1 ?
    C30D O4D Eu1D . . 135.6(3) ?
    C3D C4D C12D . . 117.4(4) ?
    C3D C4D C5D . . 123.1(4) ?
    C12D C4D C5D . . 119.5(5) ?
    C43D O5D Eu1D . . 138.1(3) ?
    C6D C5D C4D . . 121.3(4) ?
    C6D C5D H5DA . . 119.3 ?
    C4D C5D H5DA . . 119.3 ?
    C45D O6D Eu1D . . 136.8(3) ?
    C5D C6D C7D . . 120.9(5) ?
    C5D C6D H6DA . . 119.5 ?
    C7D C6D H6DA . . 119.5 ?
    C8D C7D C11D . . 117.7(4) ?
    C8D C7D C6D . . 122.8(5) ?
    C11D C7D C6D . . 119.4(5) ?
    C9D C8D C7D . . 119.8(5) ?
    C9D C8D H8DA . . 120.1 ?
    C7D C8D H8DA . . 120.1 ?
    C8D C9D C10D . . 118.5(5) ?
    C8D C9D H9DA . . 120.7 ?
    C10D C9D H9DA . . 120.7 ?
    N2D C10D C9D . . 123.9(4) ?
    N2D C10D H10D . . 118.1 ?
    C9D C10D H10D . . 118.1 ?
    N2D C11D C7D . . 122.3(4) ?
    N2D C11D C12D . . 117.9(4) ?
    C7D C11D C12D . . 119.9(4) ?
    N1D C12D C4D . . 122.2(4) ?
    N1D C12D C11D . . 118.8(4) ?
    C4D C12D C11D . . 119.0(4) ?
    O1D C13D C14D . . 124.7(4) ?
    O1D C13D C16D . . 115.2(4) ?
    C14D C13D C16D . . 120.0(4) ?
    C13D C14D C15D . . 124.3(4) ?
    C13D C14D H14D . . 117.9 ?
    C15D C14D H14D . . 117.9 ?
    O2D C15D C14D . . 123.7(4) ?
    O2D C15D C22D . . 116.1(4) ?
    C14D C15D C22D . . 120.2(4) ?
    C17D C16D C21D . . 118.0(4) ?
    C17D C16D C13D . . 119.1(4) ?
    C21D C16D C13D . . 122.9(4) ?
    C16D C17D C18D . . 121.2(4) ?
    C16D C17D H17D . . 119.4 ?
    C18D C17D H17D . . 119.4 ?
    C19D C18D C17D . . 120.2(5) ?
    C19D C18D H18D . . 119.9 ?
    C17D C18D H18D . . 119.9 ?
    C18D C19D C20D . . 119.1(4) ?
    C18D C19D H19D . . 120.5 ?
    C20D C19D H19D . . 120.5 ?
    C21D C20D C19D . . 120.9(4) ?
    C21D C20D H20D . . 119.6 ?
    C19D C20D H20D . . 119.6 ?
    C20D C21D C16D . . 120.7(5) ?
    C20D C21D H21D . . 119.7 ?
    C16D C21D H21D . . 119.7 ?
    C23D C22D C27D . . 118.1(4) ?
    C23D C22D C15D . . 123.4(4) ?
    C27D C22D C15D . . 118.5(4) ?
    C24D C23D C22D . . 121.1(4) ?
    C24D C23D H23D . . 119.4 ?
    C22D C23D H23D . . 119.4 ?
    C23D C24D C25D . . 120.0(5) ?
    C23D C24D H24D . . 120.0 ?
    C25D C24D H24D . . 120.0 ?
    C26D C25D C24D . . 119.2(5) ?
    C26D C25D H25D . . 120.4 ?
    C24D C25D H25D . . 120.4 ?
    C25D C26D C27D . . 121.4(5) ?
    C25D C26D H26D . . 119.3 ?
    C27D C26D H26D . . 119.3 ?
    C26D C27D C22D . . 120.1(5) ?
    C26D C27D H27D . . 120.0 ?
    C22D C27D H27D . . 120.0 ?
    O3D C28D C29D . . 124.2(4) ?
    O3D C28D C31D . . 117.1(4) ?
    C29D C28D C31D . . 118.5(4) ?
    C30D C29D C28D . . 123.2(4) ?
    C30D C29D H29D . . 118.4 ?
    C28D C29D H29D . . 118.4 ?
    O4D C30D C29D . . 125.9(4) ?
    O4D C30D C37D . . 115.7(4) ?
    C29D C30D C37D . . 118.2(4) ?
    C36D C31D C32D . . 118.4(4) ?
    C36D C31D C28D . . 123.8(4) ?
    C32D C31D C28D . . 117.8(4) ?
    C33D C32D C31D . . 119.8(4) ?
    C33D C32D H32D . . 120.1 ?
    C31D C32D H32D . . 120.1 ?
    C34D C33D C32D . . 121.1(4) ?
    C34D C33D H33D . . 119.4 ?
    C32D C33D H33D . . 119.4 ?
    C33D C34D C35D . . 119.9(5) ?
    C33D C34D H34D . . 120.0 ?
    C35D C34D H34D . . 120.0 ?
    C36D C35D C34D . . 119.1(4) ?
    C36D C35D H35D . . 120.5 ?
    C34D C35D H35D . . 120.5 ?
    C35D C36D C31D . . 121.6(4) ?
    C35D C36D H36D . . 119.2 ?
    C31D C36D H36D . . 119.2 ?
    C42D C37D C38D . . 119.0(4) ?
    C42D C37D C30D . . 119.0(4) ?
    C38D C37D C30D . . 121.9(4) ?
    C39D C38D C37D . . 119.4(5) ?
    C39D C38D H38D . . 120.3 ?
    C37D C38D H38D . . 120.3 ?
    C40D C39D C38D . . 121.1(5) ?
    C40D C39D H39D . . 119.4 ?
    C38D C39D H39D . . 119.4 ?
    C39D C40D C41D . . 120.7(5) ?
    C39D C40D H40D . . 119.6 ?
    C41D C40D H40D . . 119.6 ?
    C40D C41D C42D . . 118.4(5) ?
    C40D C41D H41D . . 120.8 ?
    C42D C41D H41D . . 120.8 ?
    C37D C42D C41D . . 121.3(4) ?
    C37D C42D H42D . . 119.4 ?
    C41D C42D H42D . . 119.4 ?
    O5D C43D C44D . . 124.3(4) ?
    O5D C43D C46D . . 116.0(4) ?
    C44D C43D C46D . . 119.6(4) ?
    C45D C44D C43D . . 123.8(4) ?
    C45D C44D H44D . . 118.1 ?
    C43D C44D H44D . . 118.1 ?
    O6D C45D C44D . . 125.2(4) ?
    O6D C45D C52D . . 115.4(4) ?
    C44D C45D C52D . . 119.4(4) ?
    C51D C46D C47D . . 117.4(4) ?
    C51D C46D C43D . . 123.4(4) ?
    C47D C46D C43D . . 119.2(4) ?
    C48D C47D C46D . . 122.1(4) ?
    C48D C47D H47D . . 118.9 ?
    C46D C47D H47D . . 118.9 ?
    C47D C48D C49D . . 119.3(4) ?
    C47D C48D H48D . . 120.3 ?
    C49D C48D H48D . . 120.3 ?
    C50D C49D C48D . . 119.5(5) ?
    C50D C49D H49D . . 120.2 ?
    C48D C49D H49D . . 120.2 ?
    C51D C50D C49D . . 120.7(4) ?
    C51D C50D H50D . . 119.7 ?
    C49D C50D H50D . . 119.7 ?
    C50D C51D C46D . . 120.9(4) ?
    C50D C51D H51D . . 119.5 ?
    C46D C51D H51D . . 119.5 ?
    C53D C52D C57D . . 117.9(4) ?
    C53D C52D C45D . . 122.0(4) ?
    C57D C52D C45D . . 120.0(4) ?
    C54D C53D C52D . . 121.5(4) ?
    C54D C53D H53D . . 119.2 ?
    C52D C53D H53D . . 119.2 ?
    C55D C54D C53D . . 119.7(4) ?
    C55D C54D H54D . . 120.2 ?
    C53D C54D H54D . . 120.2 ?
    C54D C55D C56D . . 120.3(5) ?
    C54D C55D H55D . . 119.8 ?
    C56D C55D H55D . . 119.8 ?
    C55D C56D C57D . . 120.0(5) ?
    C55D C56D H56D . . 120.0 ?
    C57D C56D H56D . . 120.0 ?
    C56D C57D C52D . . 120.4(4) ?
    C56D C57D H57D . . 119.8 ?
    C52D C57D H57D . . 119.8 ?
    O5E Eu1E O4E . . 81.92(11) ?
    O5E Eu1E O3E . . 128.94(10) ?
    O4E Eu1E O3E . . 72.42(11) ?
    O5E Eu1E O6E . . 70.66(11) ?
    O4E Eu1E O6E . . 109.44(11) ?
    O3E Eu1E O6E . . 77.35(12) ?
    O5E Eu1E O1E . . 149.03(11) ?
    O4E Eu1E O1E . . 89.37(11) ?
    O3E Eu1E O1E . . 75.06(11) ?
    O6E Eu1E O1E . . 139.78(11) ?
    O5E Eu1E O2E . . 77.74(11) ?
    O4E Eu1E O2E . . 76.96(11) ?
    O3E Eu1E O2E . . 134.20(11) ?
    O6E Eu1E O2E . . 146.16(11) ?
    O1E Eu1E O2E . . 71.34(11) ?
    O5E Eu1E N1E . . 75.40(11) ?
    O4E Eu1E N1E . . 146.63(12) ?
    O3E Eu1E N1E . . 140.90(11) ?
    O6E Eu1E N1E . . 85.87(12) ?
    O1E Eu1E N1E . . 97.58(11) ?
    O2E Eu1E N1E . . 74.55(11) ?
    O5E Eu1E N2E . . 124.02(12) ?
    O4E Eu1E N2E . . 150.36(12) ?
    O3E Eu1E N2E . . 79.27(11) ?
    O6E Eu1E N2E . . 71.78(11) ?
    O1E Eu1E N2E . . 74.76(11) ?
    O2E Eu1E N2E . . 119.32(11) ?
    N1E Eu1E N2E . . 61.90(12) ?
    C1E N1E C12E . . 117.5(4) ?
    C1E N1E Eu1E . . 121.8(3) ?
    C12E N1E Eu1E . . 120.5(3) ?
    C13E O1E Eu1E . . 135.6(3) ?
    N1E C1E C2E . . 124.1(5) ?
    N1E C1E H1EA . . 117.9 ?
    C2E C1E H1EA . . 117.9 ?
    C10E N2E C11E . . 117.8(4) ?
    C10E N2E Eu1E . . 122.4(3) ?
    C11E N2E Eu1E . . 119.4(3) ?
    C15E O2E Eu1E . . 133.7(3) ?
    C3E C2E C1E . . 118.2(5) ?
    C3E C2E H2EA . . 120.9 ?
    C1E C2E H2EA . . 120.9 ?
    C28E O3E Eu1E . . 132.5(3) ?
    C2E C3E C4E . . 120.3(5) ?
    C2E C3E H3EA . . 119.8 ?
    C4E C3E H3EA . . 119.8 ?
    C30E O4E Eu1E . . 134.1(3) ?
    C3E C4E C12E . . 117.6(5) ?
    C3E C4E C5E . . 123.5(5) ?
    C12E C4E C5E . . 118.8(5) ?
    C43E O5E Eu1E . . 139.4(3) ?
    C6E C5E C4E . . 121.2(5) ?
    C6E C5E H5EA . . 119.4 ?
    C4E C5E H5EA . . 119.4 ?
    C45E O6E Eu1E . . 139.0(3) ?
    C5E C6E C7E . . 122.1(5) ?
    C5E C6E H6EA . . 118.9 ?
    C7E C6E H6EA . . 118.9 ?
    C8E C7E C6E . . 125.0(5) ?
    C8E C7E C11E . . 116.9(5) ?
    C6E C7E C11E . . 118.1(5) ?
    C9E C8E C7E . . 121.1(5) ?
    C9E C8E H8EA . . 119.5 ?
    C7E C8E H8EA . . 119.5 ?
    C8E C9E C10E . . 118.1(5) ?
    C8E C9E H9EA . . 120.9 ?
    C10E C9E H9EA . . 120.9 ?
    N2E C10E C9E . . 124.1(5) ?
    N2E C10E H10E . . 117.9 ?
    C9E C10E H10E . . 117.9 ?
    N2E C11E C12E . . 118.4(4) ?
    N2E C11E C7E . . 122.0(5) ?
    C12E C11E C7E . . 119.5(5) ?
    N1E C12E C4E . . 122.3(5) ?
    N1E C12E C11E . . 117.9(4) ?
    C4E C12E C11E . . 119.8(4) ?
    O1E C13E C14E . . 124.9(4) ?
    O1E C13E C16E . . 115.9(4) ?
    C14E C13E C16E . . 119.3(4) ?
    C15E C14E C13E . . 123.5(5) ?
    C15E C14E H14E . . 118.3 ?
    C13E C14E H14E . . 118.3 ?
    O2E C15E C14E . . 124.2(5) ?
    O2E C15E C22E . . 115.7(4) ?
    C14E C15E C22E . . 120.2(4) ?
    C21E C16E C17E . . 119.0(4) ?
    C21E C16E C13E . . 122.4(4) ?
    C17E C16E C13E . . 118.5(4) ?
    C16E C17E C18E . . 120.8(5) ?
    C16E C17E H17E . . 119.6 ?
    C18E C17E H17E . . 119.6 ?
    C17E C18E C19E . . 119.4(5) ?
    C17E C18E H18E . . 120.3 ?
    C19E C18E H18E . . 120.3 ?
    C20E C19E C18E . . 120.0(5) ?
    C20E C19E H19E . . 120.0 ?
    C18E C19E H19E . . 120.0 ?
    C19E C20E C21E . . 120.2(5) ?
    C19E C20E H20E . . 119.9 ?
    C21E C20E H20E . . 119.9 ?
    C20E C21E C16E . . 120.6(5) ?
    C20E C21E H21E . . 119.7 ?
    C16E C21E H21E . . 119.7 ?
    C23E C22E C27E . . 118.4(4) ?
    C23E C22E C15E . . 123.2(4) ?
    C27E C22E C15E . . 118.2(4) ?
    C22E C23E C24E . . 120.4(4) ?
    C22E C23E H23E . . 119.8 ?
    C24E C23E H23E . . 119.8 ?
    C25E C24E C23E . . 120.7(5) ?
    C25E C24E H24E . . 119.6 ?
    C23E C24E H24E . . 119.6 ?
    C24E C25E C26E . . 119.0(5) ?
    C24E C25E H25E . . 120.5 ?
    C26E C25E H25E . . 120.5 ?
    C27E C26E C25E . . 120.3(4) ?
    C27E C26E H26E . . 119.9 ?
    C25E C26E H26E . . 119.9 ?
    C26E C27E C22E . . 121.2(5) ?
    C26E C27E H27E . . 119.4 ?
    C22E C27E H27E . . 119.4 ?
    O3E C28E C29E . . 124.0(4) ?
    O3E C28E C31E . . 116.5(4) ?
    C29E C28E C31E . . 119.5(5) ?
    C30E C29E C28E . . 123.5(5) ?
    C30E C29E H29E . . 118.2 ?
    C28E C29E H29E . . 118.2 ?
    O4E C30E C29E . . 125.0(4) ?
    O4E C30E C37E . . 116.6(4) ?
    C29E C30E C37E . . 118.4(4) ?
    C36E C31E C32E . . 119.3(5) ?
    C36E C31E C28E . . 122.6(5) ?
    C32E C31E C28E . . 118.1(5) ?
    C33E C32E C31E . . 119.4(6) ?
    C33E C32E H32E . . 120.3 ?
    C31E C32E H32E . . 120.3 ?
    C34E C33E C32E . . 120.3(6) ?
    C34E C33E H33E . . 119.8 ?
    C32E C33E H33E . . 119.8 ?
    C35E C34E C33E . . 119.9(6) ?
    C35E C34E H34E . . 120.0 ?
    C33E C34E H34E . . 120.0 ?
    C36E C35E C34E . . 120.0(7) ?
    C36E C35E H35E . . 120.0 ?
    C34E C35E H35E . . 120.0 ?
    C35E C36E C31E . . 121.0(6) ?
    C35E C36E H36E . . 119.5 ?
    C31E C36E H36E . . 119.5 ?
    C38E C37E C42E . . 119.2(4) ?
    C38E C37E C30E . . 123.3(5) ?
    C42E C37E C30E . . 117.5(4) ?
    C37E C38E C39E . . 119.9(5) ?
    C37E C38E H38E . . 120.0 ?
    C39E C38E H38E . . 120.0 ?
    C40E C39E C38E . . 120.8(5) ?
    C40E C39E H39E . . 119.6 ?
    C38E C39E H39E . . 119.6 ?
    C39E C40E C41E . . 119.7(5) ?
    C39E C40E H40E . . 120.1 ?
    C41E C40E H40E . . 120.1 ?
    C42E C41E C40E . . 120.1(6) ?
    C42E C41E H41E . . 119.9 ?
    C40E C41E H41E . . 119.9 ?
    C41E C42E C37E . . 120.2(5) ?
    C41E C42E H42E . . 119.9 ?
    C37E C42E H42E . . 119.9 ?
    O5E C43E C44E . . 122.8(5) ?
    O5E C43E C46E . . 115.5(4) ?
    C44E C43E C46E . . 121.7(5) ?
    C45E C44E C43E . . 123.9(5) ?
    C45E C44E H44E . . 118.1 ?
    C43E C44E H44E . . 118.1 ?
    O6E C45E C44E . . 123.3(5) ?
    O6E C45E C52E . . 115.0(4) ?
    C44E C45E C52E . . 121.6(5) ?
    C51E C46E C47E . . 117.9(5) ?
    C51E C46E C43E . . 124.7(5) ?
    C47E C46E C43E . . 117.3(5) ?
    C48E C47E C46E . . 121.7(6) ?
    C48E C47E H47E . . 119.2 ?
    C46E C47E H47E . . 119.2 ?
    C47E C48E C49E . . 119.6(6) ?
    C47E C48E H48E . . 120.2 ?
    C49E C48E H48E . . 120.2 ?
    C50E C49E C48E . . 119.6(6) ?
    C50E C49E H49E . . 120.2 ?
    C48E C49E H49E . . 120.2 ?
    C49E C50E C51E . . 119.9(6) ?
    C49E C50E H50E . . 120.0 ?
    C51E C50E H50E . . 120.0 ?
    C46E C51E C50E . . 121.3(6) ?
    C46E C51E H51E . . 119.4 ?
    C50E C51E H51E . . 119.4 ?
    C57E C52E C53E . . 118.1(5) ?
    C57E C52E C45E . . 124.1(5) ?
    C53E C52E C45E . . 117.8(5) ?
    C54E C53E C52E . . 120.4(5) ?
    C54E C53E H53E . . 119.8 ?
    C52E C53E H53E . . 119.8 ?
    C55E C54E C53E . . 120.9(6) ?
    C55E C54E H54E . . 119.6 ?
    C53E C54E H54E . . 119.6 ?
    C56E C55E C54E . . 119.4(5) ?
    C56E C55E H55E . . 120.3 ?
    C54E C55E H55E . . 120.3 ?
    C55E C56E C57E . . 120.6(5) ?
    C55E C56E H56E . . 119.7 ?
    C57E C56E H56E . . 119.7 ?
    C52E C57E C56E . . 120.6(5) ?
    C52E C57E H57F . . 119.7 ?
    C56E C57E H57F . . 119.7 ?
loop_
    _geom_hbond_atom_site_label_D
    _geom_hbond_atom_site_label_H
    _geom_hbond_atom_site_label_A
    _geom_hbond_site_symmetry_A
    _geom_hbond_distance_DH
    _geom_hbond_distance_HA
    _geom_hbond_distance_DA
    _geom_hbond_angle_DHA
    C1A H1AA O3A 1_555 0.95 2.54 3.119(6) 120
    C10A H10A O5A 1_555 0.95 2.40 3.094(8) 129
    C10B H10B O5B 1_555 0.95 2.44 2.997(6) 118
    C10C H10C O3C 1_555 0.95 2.38 3.016(6) 124
    C10D H10D O3D 1_555 0.95 2.42 3.017(6) 121
    C10E H10E O3E 1_555 0.95 2.51 3.153(6) 125
    C17A H17A O1A 1_555 0.95 2.38 2.716(6) 100
    C32B H32B O3B 1_555 0.95 2.40 2.736(7) 100
    C47C H47C O5C 1_555 0.95 2.36 2.702(6) 100
    C47E H47E O5E 1_555 0.95 2.32 2.679(6) 101
    C53E H53E O6E 1_555 0.95 2.36 2.692(6) 100
    C57C H57C O6C 1_555 0.95 2.40 2.730(7) 100
