##############################################################################
###                                                                        ###
###        Electronic paper (Acta Crystallographica Section E)             ###
###                                                                        ###
##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in Acta     #
# Crystallographica Section E. It conforms to the requirements of Notes      #
# for Authors for Section E, and has been peer reviewed under the auspices   #
# of the IUCr Commission on Journals.                                        #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.1.    #
#                                                                            #
# Software is freely available for graphical display of the structure(s) in  #
# this CIF.  For information consult the CIF home page http://www.iucr.org/  #
# cif/home.html                                                              #
#                                                                            #
#            Copyright International Union of Crystallography                #
#                                                                            #
##############################################################################
                                             
data_I
_audit_creation_method     SHELXL-97
_chemical_name_systematic
;
 Lithium Borodilactate
;
_chemical_name_common     ?
_chemical_formula_moiety     'Li 1+, C6 H8 B O6 1-'
_chemical_formula_sum     'C6 H8 B Li O6'
_chemical_formula_iupac     'Li 1+, C6 H8 B O6 1-'
_chemical_formula_weight     193.88
_symmetry_cell_setting     Monoclinic
_symmetry_space_group_name_H-M     'P 21'
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, y+1/2, -z'
_cell_length_a     6.7089(16)
_cell_length_b     12.0650(15)
_cell_length_c     11.0782(16)
_cell_angle_alpha     90.00
_cell_angle_beta     97.472(17)
_cell_angle_gamma     90.00
_cell_volume     889.1(3)
_cell_formula_units_Z     4
_cell_measurement_reflns_used     25
_cell_measurement_theta_min     20
_cell_measurement_theta_max     30
_cell_measurement_temperature     293(2)
_exptl_crystal_description     prisma
_exptl_crystal_colour     white
_exptl_crystal_size_max     0.23
_exptl_crystal_size_mid     0.15
_exptl_crystal_size_min     0.10
_exptl_crystal_density_diffrn     1.448
_exptl_crystal_density_meas     1.40
_exptl_crystal_density_method
                                'flotation in bromoform and glacial acetic acid'
_exptl_crystal_F_000     400
_exptl_absorpt_coefficient_mu     0.125
_exptl_absorpt_correction_type     '\y scan'
_exptl_absorpt_process_details     '(North et al., 1968)'
_exptl_absorpt_correction_T_min     0.972
_exptl_absorpt_correction_T_max     0.988
_exptl_special_details
;
 ?
;
_diffrn_ambient_temperature     293(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'fine-focus sealed tube'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type     'Enraf-Nonius CAD-4'
_diffrn_measurement_method     ω-2θ
_diffrn_detector_area_resol_mean     ?
_diffrn_reflns_number     1801
_diffrn_reflns_av_R_equivalents     0.0199
_diffrn_reflns_av_sigmaI/netI     0.0221
_diffrn_reflns_theta_min     2.51
_diffrn_reflns_theta_max     24.96
_diffrn_reflns_theta_full     24.96
_diffrn_measured_fraction_theta_max     0.999
_diffrn_measured_fraction_theta_full     0.999
_diffrn_reflns_limit_h_min     0
_diffrn_reflns_limit_h_max     7
_diffrn_reflns_limit_k_min     -14
_diffrn_reflns_limit_k_max     14
_diffrn_reflns_limit_l_min     -13
_diffrn_reflns_limit_l_max     13
_diffrn_standards_number     2
_diffrn_standards_interval_count     ?
_diffrn_standards_interval_time     100
_diffrn_standards_decay_%     0
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
_reflns_number_total     1655
_reflns_number_gt     1496
_reflns_threshold_expression     I>2σ(I)
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.0346
_refine_ls_R_factor_gt     0.0278
_refine_ls_wR_factor_gt     0.0712
_refine_ls_wR_factor_ref     0.0789
_refine_ls_goodness_of_fit_ref     0.993
_refine_ls_restrained_S_all     0.993
_refine_ls_number_reflns     1655
_refine_ls_number_parameters     258
_refine_ls_number_restraints     1
_refine_ls_hydrogen_treatment     constr
_refine_ls_weighting_scheme
      'calc w = 1/[\s^2^(Fo^2^)+(0.0558P)^2^+0.114P] where P = (Fo^2^+2Fc^2^)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     <0.001
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.177
_refine_diff_density_min     -0.186
_refine_ls_extinction_method     SHELXL97
_refine_ls_extinction_coef     0.021(4)
_refine_ls_extinction_expression
                                  'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^'
_refine_ls_abs_structure_details     ?
_refine_ls_abs_structure_Flack     ?
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'B' 'B' 0.0013 0.0007
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Li' 'Li' -0.0003 0.0001
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'CAD-4 EXPRESS (Enraf-Nonius, 1994)'
_computing_cell_refinement     'CAD-4 EXPRESS'
_computing_data_reduction     'MolEN (Fair, 1990)'
_computing_structure_solution     'SHELXS97 (Sheldrick, 1997)'
_computing_structure_refinement     'SHELXL97 (Sheldrick, 1997)'
_computing_molecular_graphics     'PLATON (Spek, 2001)'
_computing_publication_material     'SHELXL97 '
loop_
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    _atom_site_type_symbol
    Li1 -0.4341(6) 0.0733(4) 0.0959(4) 0.0325(9) Uani d . 1 . . Li
    B1 0.2839(4) -0.1164(3) 0.1516(3) 0.0297(6) Uani d . 1 . . B
    O11 0.4128(3) -0.14247(15) 0.26104(15) 0.0316(4) Uani d . 1 . . O
    O12 0.3199(3) -0.20686(18) 0.06477(15) 0.0357(4) Uani d . 1 . . O
    O13 0.4807(3) -0.36792(18) 0.07402(18) 0.0458(5) Uani d . 1 . . O
    O14 0.0641(3) -0.12026(17) 0.16668(16) 0.0362(5) Uani d . 1 . . O
    O15 0.3107(2) -0.00737(17) 0.10269(16) 0.0331(4) Uani d . 1 . . O
    O16 -0.2081(3) -0.0230(2) 0.0997(2) 0.0501(6) Uani d . 1 . . O
    C11 0.4271(4) -0.2840(2) 0.1223(2) 0.0320(6) Uani d . 1 . . C
    C12 0.4737(4) -0.2559(2) 0.2562(2) 0.0334(6) Uani d . 1 . . C
    H12 0.3896 -0.3014 0.3026 0.040 Uiso calc R 1 . . H
    C13 0.6905(5) -0.2732(3) 0.3053(3) 0.0486(8) Uani d . 1 . . C
    H13A 0.7736 -0.2291 0.2597 0.073 Uiso calc R 1 . . H
    H13B 0.7243 -0.3501 0.2982 0.073 Uiso calc R 1 . . H
    H13C 0.7125 -0.2516 0.3894 0.073 Uiso calc R 1 . . H
    C14 -0.0292(4) -0.0386(2) 0.1048(2) 0.0342(6) Uani d . 1 . . C
    C15 0.1189(4) 0.0293(2) 0.0436(2) 0.0369(6) Uani d . 1 . . C
    H15 0.1068 0.0082 -0.0425 0.044 Uiso calc R 1 . . H
    C16 0.0907(5) 0.1521(3) 0.0517(3) 0.0561(9) Uani d . 1 . . C
    H16A 0.1099 0.1744 0.1355 0.084 Uiso calc R 1 . . H
    H16B -0.0428 0.1714 0.0158 0.084 Uiso calc R 1 . . H
    H16C 0.1869 0.1892 0.0088 0.084 Uiso calc R 1 . . H
    Li2 -0.4752(6) 0.4567(4) 0.5990(4) 0.0312(9) Uani d . 1 . . Li
    B2 -0.2459(4) 0.1439(3) 0.3577(3) 0.0298(6) Uani d . 1 . . B
    O21 -0.2642(3) 0.03134(15) 0.39894(16) 0.0334(4) Uani d . 1 . . O
    O22 -0.0291(3) 0.15737(16) 0.34584(17) 0.0355(4) Uani d . 1 . . O
    O23 0.2542(3) 0.06181(18) 0.39764(18) 0.0421(5) Uani d . 1 . . O
    O24 -0.2973(3) 0.22676(16) 0.45056(15) 0.0349(4) Uani d . 1 . . O
    O25 -0.3783(3) 0.17125(15) 0.24773(14) 0.0327(4) Uani d . 1 . . O
    O26 -0.5079(3) 0.36935(19) 0.45402(17) 0.0465(5) Uani d . 1 . . O
    C21 0.0722(4) 0.0708(2) 0.3926(2) 0.0296(6) Uani d . 1 . . C
    C22 -0.0696(4) -0.0112(2) 0.4400(2) 0.0353(6) Uani d . 1 . . C
    H22 -0.0539 -0.0839 0.4030 0.042 Uiso calc R 1 . . H
    C23 -0.0298(5) -0.0215(3) 0.5771(3) 0.0544(9) Uani d . 1 . . C
    H23A -0.0554 0.0484 0.6137 0.082 Uiso calc R 1 . . H
    H23B 0.1079 -0.0423 0.6008 0.082 Uiso calc R 1 . . H
    H23C -0.1165 -0.0770 0.6040 0.082 Uiso calc R 1 . . H
    C24 -0.4384(4) 0.2931(2) 0.4016(2) 0.0318(6) Uani d . 1 . . C
    C25 -0.5032(4) 0.2633(2) 0.2708(2) 0.0348(6) Uani d . 1 . . C
    H25 -0.6437 0.2390 0.2616 0.042 Uiso calc R 1 . . H
    C26 -0.4840(7) 0.3598(3) 0.1873(3) 0.0669(11) Uani d . 1 . . C
    H26A -0.3458 0.3825 0.1938 0.100 Uiso calc R 1 . . H
    H26B -0.5644 0.4204 0.2098 0.100 Uiso calc R 1 . . H
    H26C -0.5295 0.3383 0.1049 0.100 Uiso calc R 1 . . H
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    Li1 O16 . 1.907(5) yes
    Li1 O15 1_455 1.979(5) yes
    Li1 O13 2 1.997(4) yes
    Li1 O25 . 2.050(5) yes
    B1 O11 . 1.430(3) yes
    B1 O15 . 1.443(4) yes
    B1 O12 . 1.495(4) yes
    B1 O14 . 1.507(3) yes
    O11 C12 . 1.431(3) ?
    O11 Li2 2_546 1.960(5) ?
    O12 C11 . 1.292(3) ?
    O13 C11 . 1.220(3) ?
    O13 Li1 2_545 1.997(4) ?
    O14 C14 . 1.311(3) ?
    O15 C15 . 1.436(3) ?
    O15 Li1 1_655 1.979(5) ?
    O16 C14 . 1.209(3) ?
    C11 C12 . 1.514(3) ?
    C12 C13 . 1.500(4) ?
    C14 C15 . 1.514(4) ?
    C15 C16 . 1.498(5) ?
    Li2 O26 . 1.910(5) yes
    Li2 O23 2_556 1.948(5) yes
    Li2 O11 2_556 1.960(5) yes
    Li2 O21 2_456 1.969(5) yes
    B2 O21 . 1.443(4) yes
    B2 O25 . 1.450(3) yes
    B2 O22 . 1.486(3) yes
    B2 O24 . 1.506(3) yes
    O21 C22 . 1.421(3) ?
    O21 Li2 2_446 1.969(5) ?
    O22 C21 . 1.315(3) ?
    O23 C21 . 1.220(3) ?
    O23 Li2 2_546 1.948(5) ?
    O24 C24 . 1.303(3) ?
    O25 C25 . 1.434(3) ?
    O26 C24 . 1.213(3) ?
    C21 C22 . 1.514(4) ?
    C22 C23 . 1.512(4) ?
    C24 C25 . 1.502(3) ?
    C25 C26 . 1.503(4) ?
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    O16 Li1 O15 . 1_455 112.9(2) ?
    O16 Li1 O13 . 2 105.3(2) yes
    O15 Li1 O13 1_455 2 100.4(2) yes
    O16 Li1 O25 . . 105.9(2) yes
    O15 Li1 O25 1_455 . 108.6(2) ?
    O13 Li1 O25 2 . 123.9(2) yes
    O11 B1 O15 . . 115.3(2) ?
    O11 B1 O12 . . 104.7(2) yes
    O15 B1 O12 . . 112.7(2) yes
    O11 B1 O14 . . 113.0(2) yes
    O15 B1 O14 . . 104.0(2) yes
    O12 B1 O14 . . 106.9(2) ?
    B1 O11 C12 . . 108.8(2) ?
    B1 O11 Li2 . 2_546 125.5(2) ?
    C12 O11 Li2 . 2_546 125.5(2) ?
    C11 O12 B1 . . 109.58(19) ?
    C11 O13 Li1 . 2_545 133.5(2) ?
    C14 O14 B1 . . 109.0(2) ?
    C15 O15 B1 . . 107.7(2) ?
    C15 O15 Li1 . 1_655 124.0(2) ?
    B1 O15 Li1 . 1_655 127.8(2) ?
    C14 O16 Li1 . . 151.4(3) ?
    O13 C11 O12 . . 123.9(2) ?
    O13 C11 C12 . . 125.5(2) ?
    O12 C11 C12 . . 110.6(2) ?
    O11 C12 C13 . . 112.8(2) ?
    O11 C12 C11 . . 103.2(2) ?
    C13 C12 C11 . . 113.0(2) ?
    O16 C14 O14 . . 123.0(3) ?
    O16 C14 C15 . . 126.8(3) ?
    O14 C14 C15 . . 110.1(2) ?
    O15 C15 C16 . . 112.9(3) ?
    O15 C15 C14 . . 103.3(2) ?
    C16 C15 C14 . . 114.4(3) ?
    O26 Li2 O23 . 2_556 112.3(2) yes
    O26 Li2 O11 . 2_556 108.5(2) ?
    O23 Li2 O11 2_556 2_556 107.4(2) yes
    O26 Li2 O21 . 2_456 104.9(2) yes
    O23 Li2 O21 2_556 2_456 112.1(2) ?
    O11 Li2 O21 2_556 2_456 111.7(2) yes
    O21 B2 O25 . . 114.4(2) ?
    O21 B2 O22 . . 104.8(2) yes
    O25 B2 O22 . . 113.6(2) yes
    O21 B2 O24 . . 111.9(2) yes
    O25 B2 O24 . . 104.7(2) yes
    O22 B2 O24 . . 107.5(2) ?
    C22 O21 B2 . . 109.2(2) ?
    C22 O21 Li2 . 2_446 127.6(2) ?
    B2 O21 Li2 . 2_446 123.1(2) ?
    C21 O22 B2 . . 109.9(2) ?
    C21 O23 Li2 . 2_546 144.5(2) ?
    C24 O24 B2 . . 110.02(19) ?
    C25 O25 B2 . . 109.57(19) ?
    C25 O25 Li1 . . 122.95(19) ?
    B2 O25 Li1 . . 125.8(2) ?
    C24 O26 Li2 . . 144.3(2) ?
    O23 C21 O22 . . 123.5(2) ?
    O23 C21 C22 . . 126.6(2) ?
    O22 C21 C22 . . 109.9(2) ?
    O21 C22 C23 . . 112.7(2) ?
    O21 C22 C21 . . 104.2(2) ?
    C23 C22 C21 . . 111.4(2) ?
    O26 C24 O24 . . 124.8(2) ?
    O26 C24 C25 . . 124.2(2) ?
    O24 C24 C25 . . 111.0(2) ?
    O25 C25 C24 . . 104.8(2) ?
    O25 C25 C26 . . 113.0(2) ?
    C24 C25 C26 . . 111.8(3) ?
loop_
    _geom_torsion_atom_site_label_1
    _geom_torsion_atom_site_label_2
    _geom_torsion_atom_site_label_3
    _geom_torsion_atom_site_label_4
    _geom_torsion_site_symmetry_1
    _geom_torsion_site_symmetry_2
    _geom_torsion_site_symmetry_3
    _geom_torsion_site_symmetry_4
    _geom_torsion
    _geom_torsion_publ_flag
    O15 B1 O11 C12 . . . . -141.5(2) ?
    O12 B1 O11 C12 . . . . -17.0(3) ?
    O14 B1 O11 C12 . . . . 99.1(2) ?
    O15 B1 O11 Li2 . . . 2_546 43.7(3) ?
    O12 B1 O11 Li2 . . . 2_546 168.2(2) ?
    O14 B1 O11 Li2 . . . 2_546 -75.8(3) ?
    O11 B1 O12 C11 . . . . 9.8(3) ?
    O15 B1 O12 C11 . . . . 135.9(2) ?
    O14 B1 O12 C11 . . . . -110.5(2) ?
    O11 B1 O14 C14 . . . . 140.9(2) ?
    O15 B1 O14 C14 . . . . 15.1(3) ?
    O12 B1 O14 C14 . . . . -104.3(2) ?
    O11 B1 O15 C15 . . . . -148.2(2) ?
    O12 B1 O15 C15 . . . . 91.6(2) ?
    O14 B1 O15 C15 . . . . -23.8(2) ?
    O11 B1 O15 Li1 . . . 1_655 39.3(3) ?
    O12 B1 O15 Li1 . . . 1_655 -80.9(3) ?
    O14 B1 O15 Li1 . . . 1_655 163.6(2) ?
    O15 Li1 O16 C14 1_455 . . . -173.8(4) ?
    O13 Li1 O16 C14 2 . . . 77.7(5) ?
    O25 Li1 O16 C14 . . . . -55.1(6) ?
    Li1 O13 C11 O12 2_545 . . . -1.6(4) ?
    Li1 O13 C11 C12 2_545 . . . 177.9(3) ?
    B1 O12 C11 O13 . . . . -179.5(2) ?
    B1 O12 C11 C12 . . . . 1.0(3) ?
    B1 O11 C12 C13 . . . . 139.6(2) ?
    Li2 O11 C12 C13 2_546 . . . -45.6(3) ?
    B1 O11 C12 C11 . . . . 17.2(2) ?
    Li2 O11 C12 C11 2_546 . . . -167.9(2) ?
    O13 C11 C12 O11 . . . . 169.2(2) ?
    O12 C11 C12 O11 . . . . -11.3(3) ?
    O13 C11 C12 C13 . . . . 47.0(4) ?
    O12 C11 C12 C13 . . . . -133.5(3) ?
    Li1 O16 C14 O14 . . . . 141.6(4) ?
    Li1 O16 C14 C15 . . . . -38.6(6) ?
    B1 O14 C14 O16 . . . . 178.9(3) ?
    B1 O14 C14 C15 . . . . -0.9(3) ?
    B1 O15 C15 C16 . . . . 147.3(3) ?
    Li1 O15 C15 C16 1_655 . . . -39.8(4) ?
    B1 O15 C15 C14 . . . . 23.2(3) ?
    Li1 O15 C15 C14 1_655 . . . -164.0(2) ?
    O16 C14 C15 O15 . . . . 166.4(3) ?
    O14 C14 C15 O15 . . . . -13.8(3) ?
    O16 C14 C15 C16 . . . . 43.2(4) ?
    O14 C14 C15 C16 . . . . -137.0(3) ?
    O25 B2 O21 C22 . . . . 139.4(2) ?
    O22 B2 O21 C22 . . . . 14.3(2) ?
    O24 B2 O21 C22 . . . . -101.9(2) ?
    O25 B2 O21 Li2 . . . 2_446 -42.9(3) ?
    O22 B2 O21 Li2 . . . 2_446 -167.9(2) ?
    O24 B2 O21 Li2 . . . 2_446 75.9(3) ?
    O21 B2 O22 C21 . . . . -9.1(3) ?
    O25 B2 O22 C21 . . . . -134.6(2) ?
    O24 B2 O22 C21 . . . . 110.1(2) ?
    O21 B2 O24 C24 . . . . -124.6(2) ?
    O25 B2 O24 C24 . . . . -0.2(3) ?
    O22 B2 O24 C24 . . . . 120.9(2) ?
    O21 B2 O25 C25 . . . . 122.3(2) ?
    O22 B2 O25 C25 . . . . -117.5(2) ?
    O24 B2 O25 C25 . . . . -0.5(3) ?
    O21 B2 O25 Li1 . . . . -43.3(3) ?
    O22 B2 O25 Li1 . . . . 77.0(3) ?
    O24 B2 O25 Li1 . . . . -166.0(2) ?
    O16 Li1 O25 C25 . . . . 172.9(2) ?
    O15 Li1 O25 C25 1_455 . . . -65.7(3) ?
    O13 Li1 O25 C25 2 . . . 51.5(3) ?
    O16 Li1 O25 B2 . . . . -23.4(3) ?
    O15 Li1 O25 B2 1_455 . . . 98.1(3) ?
    O13 Li1 O25 B2 2 . . . -144.8(2) ?
    O23 Li2 O26 C24 2_556 . . . 74.6(5) ?
    O11 Li2 O26 C24 2_556 . . . -43.9(5) ?
    O21 Li2 O26 C24 2_456 . . . -163.4(3) ?
    Li2 O23 C21 O22 2_546 . . . -152.2(3) ?
    Li2 O23 C21 C22 2_546 . . . 29.3(5) ?
    B2 O22 C21 O23 . . . . -178.1(2) ?
    B2 O22 C21 C22 . . . . 0.6(3) ?
    B2 O21 C22 C23 . . . . 107.1(3) ?
    Li2 O21 C22 C23 2_446 . . . -70.5(3) ?
    B2 O21 C22 C21 . . . . -13.8(3) ?
    Li2 O21 C22 C21 2_446 . . . 168.5(2) ?
    O23 C21 C22 O21 . . . . -173.2(2) ?
    O22 C21 C22 O21 . . . . 8.2(3) ?
    O23 C21 C22 C23 . . . . 65.0(3) ?
    O22 C21 C22 C23 . . . . -113.7(3) ?
    Li2 O26 C24 O24 . . . . 10.0(6) ?
    Li2 O26 C24 C25 . . . . -169.4(3) ?
    B2 O24 C24 O26 . . . . -178.7(3) ?
    B2 O24 C24 C25 . . . . 0.8(3) ?
    B2 O25 C25 C24 . . . . 0.9(3) ?
    Li1 O25 C25 C24 . . . . 166.9(2) ?
    B2 O25 C25 C26 . . . . 122.9(3) ?
    Li1 O25 C25 C26 . . . . -71.1(3) ?
    O26 C24 C25 O25 . . . . 178.4(3) ?
    O24 C24 C25 O25 . . . . -1.1(3) ?
    O26 C24 C25 C26 . . . . 55.6(4) ?
    O24 C24 C25 C26 . . . . -123.9(3) ?
data_global
_journal_date_recd_electronic     2002-03-04
_journal_date_accepted     2002-04-15
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2002
_journal_volume     58
_journal_issue      5
_journal_page_first     m212
_journal_page_last     m214
_journal_paper_category     EM
_publ_contact_author_name     'Dr V. Parthasarathi'
_publ_contact_author_address
;
Department of Physics
Bharathidasan University
Tiruchirappalli 620 024
India
;
_publ_contact_author_email     vpsarati@yahoo.com
_publ_contact_author_fax     '+91 0431 660245'
_publ_contact_author_phone     '(0091) 431 660357'
_publ_section_title
;
Lithium borodilactate
;
loop_
    _publ_author_name
    _publ_author_address
    'Dhanuskodi, S.'
;         Department of Physics
          Bharathidasan University
          Tiruchirappalli 620 024
          India
;
    'Angeli Mary, P. .A'
;         Department of Physics
          Bharathidasan University
          Tiruchirappalli 620 024
          India
;
    'Thamotharan, S.'
;          Department of Physics
           Bharathidasan University
           Tiruchirappalli 620 024
           India
;
    'Parthasarathi, V.'
;          Department of Physics
           Bharathidasan University
           Tiruchirappalli 620 024
           India
;
