Atomic configurations of dislocation core and twin boundaries in 3CSiC studied by high-resolution electron microscopy

C. Y. Tang, F. H. Li, R. Wang, J. Zou, X. H. Zheng, and J. W. Liang
Phys. Rev. B 75, 184103 – Published 10 May 2007

Abstract

The defects in 3CSiC film grown on (001) plane of Si substrate were studied using a 200kV high-resolution electron microscope with point resolution of 0.2nm. A posterior image processing technique, the image deconvolution, was utilized in combination with the image contrast analysis to distinguish atoms of Si from C distant from each other by 0.109nm in the [110] projected image. The principle of the image processing technique utilized and the related image contrast theory is briefly presented. The procedures of transforming an experimental image that does not reflect the crystal structure intuitively into the structure map and of identifying Si and C atoms from the map are described. The atomic configurations for a 30° partial dislocation and a microtwin have been derived at atomic level. It has been determined that the 30° partial dislocation terminates in C atom and the segment of microtwin is sandwiched between two 180° rotation twins. The corresponding stacking sequences are derived and atomic models are constructed according to the restored structure maps for both the 30° partial dislocation and microtwin. Images were simulated based on the two models to affirm the above-mentioned results.

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  • Received 20 November 2006

DOI:https://doi.org/10.1103/PhysRevB.75.184103

©2007 American Physical Society

Authors & Affiliations

C. Y. Tang1, F. H. Li1,*, R. Wang2, J. Zou3, X. H. Zheng4, and J. W. Liang4

  • 1Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, Beijing 100080, China
  • 2Department of Materials Physics and Chemistry, University of Science and Technology Beijing, Beijing 100083, China
  • 3School of Engineering and Centre for Microscopy and Microanalysis, The University of Queensland, Brisbane QLD 4072, Australia
  • 4R&D Center for Optoelectronic Technology, Institute of Semiconductors, Chinese Academy of Sciences, P.O. Box 912, Beijing 100083, China

  • *Author to whom correspondence should be addressed. FAX: 86-10-8264-9531. Electronic address: lifh@aphy.iphy.ac.cn

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Issue

Vol. 75, Iss. 18 — 1 May 2007

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