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Synthesis and Properties of Iron Oxide Particles Prepared by Hidrothermal Method

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Published under licence by IOP Publishing Ltd
, , Citation T Saragi et al 2017 IOP Conf. Ser.: Mater. Sci. Eng. 196 012025 DOI 10.1088/1757-899X/196/1/012025

1757-899X/196/1/012025

Abstract

Iron oxide of hematite (α-Fe2O3) has been successfully synthesized by hydrothermal method. The starting materials were Fe(NO3)3.9H2O, 2-methoxyethanol, diethanolamine and n-hexane. The optical, morphology and crystal structure were measured by UV-VIS, TEM and XRD, respectively. From UV-VIS measurement, it was found that the band-gap of sample was 4.17 eV. The morphology of particle was plate-like form. The sample which sintered at 1100°C has high quality crystal with hexagonal structure of α-Fe2O3 phase.

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