High-pressure powder x-ray diffraction experiments on Zn at low temperature

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Published 25 October 2002 Published under licence by IOP Publishing Ltd
, , Citation K Takemura et al 2002 J. Phys.: Condens. Matter 14 10563 DOI 10.1088/0953-8984/14/44/333

0953-8984/14/44/10563

Abstract

High-pressure powder x-ray diffraction experiments have been performed on Zn with a He-pressure medium at low temperature. When the sample was compressed in the He medium at low temperature, large nonhydrostaticity developed, yielding erroneous lattice parameters. On the other hand, when the pressure was changed at high temperatures, good hydrostaticity was maintained. No anomaly in the volume dependence of the c/a axial ratio has been found.

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10.1088/0953-8984/14/44/333