O-Cholesteryl thiobenzoate (I; Ar = Ph) is smoothly photolysed to give cholesta-3,5-diene (II) and thiobenzoic acid in high yield.
S. Achmatowicz, D. H. R. Barton, P. D. Magnus, G. A. Poulton and P. J. West, J. Chem. Soc., Perkin Trans. 1, 1973, 1567 DOI: 10.1039/P19730001567
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