SCHEDULED MAINTENANCE
2-Methoxy-7,8,9,10-tetrahydrobenzo[i]phenanthridine (XI) has been synthesised by a new route. Its N-oxide rearranges on heating with acetic anhydride to give the 7-acetoxy-derivative which is then hydrolysed to afford the title compound.
S. V. Kessar, A. K. Sobti and G. S. Joshi, J. Chem. Soc. C, 1971, 259 DOI: 10.1039/J39710000259
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