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The molecular structure of gaseous trisilylarsine has been determined by the sector-microphotometer method of electron diffraction. The heavy-atom skeleton is found to be pyramidal; the As–Si distance is 2·355 ± 0·001 Å and the Si–As–Si angle 93·79 ± 0·17°. The Si–H distance is 1·488 ± 0·011 Å.
B. Beagley, A. G. Robiette and G. M. Sheldrick, J. Chem. Soc. A, 1968, 3006 DOI: 10.1039/J19680003006
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