Issue 3, 1980
From the journal:

Journal of the Chemical Society, Dalton Transactions

Crystal structure of (IOF3·IO2F3)2

Ronald J. Gillespie,   John P. Krasznai  and  David R. Slim  

Abstract

The crystal structure of (IOF3·IO2F3)2 has been determined from three-dimensional X-ray counter data at -45 °C. Crystals are monoclinic with a= 9.832(4), b= 8.307(5), c= 10.187(7)Å, β= 125.46(7)°, U= 677.7 Å3, Z= 4, and Dc= 4.08 g cm–3. The structure has been refined in the space group P21/n to a final conventional R′ index of 0.061 for 1 289 independent reflections. It consists of two IOF2 and two IO2F4 units linked by asymmetric oxygen bridges to give a cyclic molecule. These molecules are weakly bounded together in sheets by additional weak oxygen bridges.

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Article information

DOI
https://doi.org/10.1039/DT9800000481
Article type
Paper

J. Chem. Soc., Dalton Trans., 1980, 481-483

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Crystal structure of (IOF3·IO2F3)2

R. J. Gillespie, J. P. Krasznai and D. R. Slim, J. Chem. Soc., Dalton Trans., 1980, 481 DOI: 10.1039/DT9800000481

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