Reaction of vanadyl sulfate, L-alanine and 2-hydroxynaphthaldehyde with subsequent aeration in D,L-sec-butyl alcohol leads to the Schiff base VV complex [VO{N-(2-oxido-1-naphthylmethylene)-L-ala}OBus(HOBus)] which, in solution, exists in at least three diastereoisomers (51V NMR evidence), and crystallizes with the ASRR and CSSS isomers in the same asymmetric unit.
R. Fulwood, H. Schmidt and D. Rehder, J. Chem. Soc., Chem. Commun., 1995, 1443 DOI: 10.1039/C39950001443
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