SCHEDULED MAINTENANCE
Reaction of nitroalkanes with Grignard reagents, in the presence of anhydrous CeCl3 in tetrahydrofuran at –78 °C, affords N,N-disubstituted hydroxylamines in fair to good yields, depending on the nature of the reagent used.
G. Bartoli, E. Marcantoni and M. Petrini, J. Chem. Soc., Chem. Commun., 1993, 1373 DOI: 10.1039/C39930001373
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