SCHEDULED MAINTENANCE
Deoxygenation of phosphole oxide dimers with HSiCl3–C5H5N, but not HSiCl3 alone, gives stable diphosphines whose phosphorus atoms in the syn-7-phosphanorbornene position have the most deshielded 31P n.m.r. shifts ever reported for tertiary phosphines.
L. D. Quin and K. A. Mesch, J. Chem. Soc., Chem. Commun., 1980, 959 DOI: 10.1039/C39800000959
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