SCHEDULED MAINTENANCE
[Au9L8]3+(L = PPh3) reacts with L to give [Au9L10]3+ and with X–(X = Cl, Br, I, CN, or SCN) to give Au9L8X3 which converts into [Au11L8X2]+ in solution (investigated for X = Cl and SCN); from 31P [1H] n.m.r., i.r., and Mössbauer spectra it is concluded that these new Au9 and Au11 clusters are structurally related to the known complexes [Au9L8]3+ and Au11L7X3, respectively.
F. A. Vollenbroek, J. J. Bour, J. M. Trooster and J. W. A. van der Velden, J. Chem. Soc., Chem. Commun., 1978, 907 DOI: 10.1039/C39780000907
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