Reaction of methanol with CrCl3,6H2O dehydrated in situ with 2,2-dimethoxypropane gave trans-dichlorotetramethanolchromium(III) chloride; the cation, [Cr(MeOH)4Cl2]+, has C4 symmetry with slightly different Cr–Cl distances but otherwise normal atom-atom distances.
K. I. Hardcastle, D. O. Skovlin and A. Eidawad, J. Chem. Soc., Chem. Commun., 1975, 190a DOI: 10.1039/C3975000190A
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