Issue 6, 2012

A facile electrochemical route for fast deposition of featherlike tellurium microstructures

Abstract

In this paper, featherlike t-Te microstructures were synthesized at a large scale via a simple electrochemical deposition route at room temperature, employing Na2TeO3 as a tellurium source in a diluted HNO3 solution without the assistance of any additive. The phase and morphology of the as-prepared product were characterized by means of powder X-ray diffraction (XRD), energy dispersive spectrometry (EDS), (high resolution) transmission electron microscopy (HR/TEM), selected area electron pattern (SAED) and scanning electron microscopy (SEM). Some factors influencing the formation of featherlike t-Te microstructures were systematically investigated, including the deposition current, and the original amounts of Na2TeO3 and HNO3. The time-dependent shape evolution of featherlike t-Te microstructures was investigated. Experiments showed that diluted HNO3 was indispensable in the formation of featherlike t-Te microstructures.

Graphical abstract: A facile electrochemical route for fast deposition of featherlike tellurium microstructures

Article information

Article type
Paper
Submitted
19 Oct 2011
Accepted
09 Dec 2011
First published
27 Jan 2012

RSC Adv., 2012,2, 2340-2345

A facile electrochemical route for fast deposition of featherlike tellurium microstructures

X. Wang and Y. Ni, RSC Adv., 2012, 2, 2340 DOI: 10.1039/C2RA00917J

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