The compound [C6H4(NMe3)2-1,3][O2]2·3NH3 was prepared from [NMe4][O2] via cation-exchange in liquid ammonia; the bond length of the superoxide anion was determined by X-ray crystallographic analysis to be 134(3) pm.
H. Seyeda and M. Jansen, J. Chem. Soc., Dalton Trans., 1998, 875 DOI: 10.1039/A800952J
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