Issue 9, 1983
From the journal:

Journal of the Chemical Society, Perkin Transactions 2

X-Ray determination of the molecular structure of the novel antibiotic DC-52-d, 6-hydroxymethyl-3,12-imino-7-methoxy-13-methyl-1,2,3,4-tetrahydroazepino[1,2-b]isoquinoline-1-carboxylic acid

Noriaki Hirayama  and  Kunikatsu Shirahata  

Abstract

The molecular geometry of the title compound has been determined by X-ray diffraction. The molecule has a novel tetracyclic skeleton. Crystallographic data are a= 11.185(2), b= 15.878(2), c= 11.1184(9)Å, Z= 4, space group P212121. Diffractometer intensity measurements were made with Mo-Kα radiation and least-squares adjustment of the atomic parameters converged at Rw 0.069 for 1 793 |F0| values.

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Article information

DOI
https://doi.org/10.1039/P29830001705
Article type
Paper

J. Chem. Soc., Perkin Trans. 2, 1983, 1705-1708

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X-Ray determination of the molecular structure of the novel antibiotic DC-52-d, 6-hydroxymethyl-3,12-imino-7-methoxy-13-methyl-1,2,3,4-tetrahydroazepino[1,2-b]isoquinoline-1-carboxylic acid

N. Hirayama and K. Shirahata, J. Chem. Soc., Perkin Trans. 2, 1983, 1705 DOI: 10.1039/P29830001705

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