Issue 9, 2016
From the journal:

Green Chemistry

Catalyst-free thiolation of indoles with sulfonyl hydrazides for the synthesis of 3-sulfenylindoles in water†

Yu Yang,a   Sheng Zhang,a   Lin Tang,a   Yanbin Hu,a   Zhenggen Zhaa  and  Zhiyong Wang*a  

* Corresponding authors

a Hefei National Laboratory for Physical Sciences at Microscale, CAS Key Laboratory of Soft Matter Chemistry and Department of Chemistry & Collaborative Innovation Center of Suzhou Nano Science and Technology, University of Science and Technology of China, Hefei, P. R. China
E-mail: zwang3@ustc.edu.cn
Fax: (+86) 551-360-3185

Abstract

A catalyst-free thiolation of indoles with sulfonyl hydrazides was efficiently developed in water under mild conditions without any ligand or additive. The reaction provided a variety of 3-sulfenylindoles with good to excellent yields and the only by-products were nitrogen and water.

Graphical abstract: Catalyst-free thiolation of indoles with sulfonyl hydrazides for the synthesis of 3-sulfenylindoles in water

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Article information

DOI
https://doi.org/10.1039/C6GC00313C
Article type
Communication
Submitted
01 Feb 2016
Accepted
22 Feb 2016
First published
22 Feb 2016

Green Chem., 2016,18, 2609-2613

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Catalyst-free thiolation of indoles with sulfonyl hydrazides for the synthesis of 3-sulfenylindoles in water

Y. Yang, S. Zhang, L. Tang, Y. Hu, Z. Zha and Z. Wang, Green Chem., 2016, 18, 2609 DOI: 10.1039/C6GC00313C

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