SCHEDULED MAINTENANCE
14 N N.m.r. spectroscopy reveals that liquid ammonia solutions of [S4N3]Cl or [S3N2Cl]Cl contain S3N3– whilst solutions of S4N4 contain S3N3– and S4N5– and traces of other species such as S2N22–; the usefulness of these liquid ammonia solutions in synthesis has been established in several cases with two new complexes being characterised by X-ray crystallography.
P. S. Belton, I. P. Parkin, D. J. Williams and J. D. Woollins, J. Chem. Soc., Chem. Commun., 1988, 1479 DOI: 10.1039/C39880001479
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