Issue 9, 1995
From the journal:

Analyst

Perspective. Analytical validation of a general protocol for the preparation of dose-controlled solutions in aluminium toxicology

Andrea Tapparo,   Lidia Soldà,   G. Giorgio Bombi,   Pamela Zambenedetti,   Paolo F. Zatta,   Roberta Bertani  and  Benedetto Corain  

Abstract

Aluminium(III) solutions suitable for careful toxicological investigation both in vivo and in vitro, are prepared from AlCl3·6H2O and from neutral metal complexes, Al(lactate)3, Al2(citrate)2(H2O)6, Al(acetylacetonate)3 and Al(maltolate)3, by dissolving the pure compounds in TRIS-HCl buffer solutions. The metal concentrations in the supernatant liquids are determined spectrophotometrically under reproducible conditions. Al(acetylacetonate)3 and Al(maltolate)3 are detected as molecular entities by using 1H NMR spectroscopy down to concentrations of 200 and 100 µmol l–1, respectively.

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Article information

DOI
https://doi.org/10.1039/AN9952002425
Article type
Paper

Analyst, 1995,120, 2425-2429

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Perspective. Analytical validation of a general protocol for the preparation of dose-controlled solutions in aluminium toxicology

A. Tapparo, L. Soldà, G. G. Bombi, P. Zambenedetti, P. F. Zatta, R. Bertani and B. Corain, Analyst, 1995, 120, 2425 DOI: 10.1039/AN9952002425

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