The novel polyoxothioanion [Mo9S8O12(OH)8(H2O)2]2– was prepared from the acido-basic condensation of four {MoV2S2O2} building units around a central {MoVIO6} octahedron, the anion was characterized by X-ray diffraction as a tetramethylammonium salt.
A. Dolbecq, E. Cadot and F. Sécheresse, Chem. Commun., 1998, 2293 DOI: 10.1039/A805453C
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