Issue 4, 1973
From the journal:

Journal of the Chemical Society, Perkin Transactions 2

Crystal and molecular structure of ‘perpendicular’ 9,9-dichloro-trans,trans-bicyclo[6.1.0]non-4-ene oxide

W. A. Szabo,   M. F. Betkouski,   J. A. Deyrup,   M. Mathew  and  G. J. Palenik  

Abstract

The crystal and molecular structure of the title compound has been determined by single-crystal X-ray diffraction techniques. Crystals are monoclinic space group P21/n, with unit cell dimensions a= 8·968(4), b= 8·835(4), c= 12·121(4)Å, β= 93·92(2)°, Z= 4. Diffractometer data were refined by full-matrix least-squares methods to R 0·040 for 1189 observed reflections. The dihedral angle between planes defined by the three-membered rings is 70·3°. The transannular distance between these rings, calculated from the midpoints of the two appropriate bonds, is 2·63 Å.

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Article information

DOI
https://doi.org/10.1039/P29730000339
Article type
Paper

J. Chem. Soc., Perkin Trans. 2, 1973, 339-341

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Crystal and molecular structure of ‘perpendicular’ 9,9-dichloro-trans,trans-bicyclo[6.1.0]non-4-ene oxide

W. A. Szabo, M. F. Betkouski, J. A. Deyrup, M. Mathew and G. J. Palenik, J. Chem. Soc., Perkin Trans. 2, 1973, 339 DOI: 10.1039/P29730000339

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