Issue 70, 2015
From the journal:

Chemical Communications

Sealed rotors for in situ high temperature high pressure MAS NMR†

Jian Zhi Hu,*a   Mary Y. Hu,a   Zhenchao Zhao,a   Suochang Xu,a   Aleksei Vjunov,a   Hui Shi,a   Donald M. Camaioni,a   Charles H. F. Pedena  and  Johannes A. Lerchera  

* Corresponding authors

a Pacific Northwest National Laboratory, Richland, WA 99352, USA
E-mail: Jianzhi.Hu@pnnl.gov

Abstract

Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.

Graphical abstract: Sealed rotors for in situ high temperature high pressure MAS NMR

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Article information

DOI
https://doi.org/10.1039/C5CC03910J
Article type
Communication
Submitted
11 May 2015
Accepted
06 Jul 2015
First published
06 Jul 2015

Chem. Commun., 2015,51, 13458-13461

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Sealed rotors for in situ high temperature high pressure MAS NMR

J. Z. Hu, M. Y. Hu, Z. Zhao, S. Xu, A. Vjunov, H. Shi, D. M. Camaioni, C. H. F. Peden and J. A. Lercher, Chem. Commun., 2015, 51, 13458 DOI: 10.1039/C5CC03910J

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