Abstract
The compounds MB10H11 (M = Me4N+, Et4N+, Bu4N+, Ph4P+, Ph4As+) are synthesized. A procedure is proposed for boron determination by atomic absorption spectrophotometry, using microwave processing for sample preparation.
Similar content being viewed by others
REFERENCES
Kuznetsov, N.T., Kulikova, L.N., and Kanaeva, O.A., Gravimetric Determination of closo-Dodecaborates, Zh. Anal. Khim., 1976, vol. 31, no. 7, pp. 1382–1383.
Kuznetsov, N.T. and Klimchuk, G.S., Group II Dodecahydrocloso-dodecaborates, Tr. Mosk. Inst. Tonkoi Khim. Tekhnol. im. M. V. Lomonosova, 1972, vol. 2, no. 11, pp. 19–21.
Mustyatsa, V.N., Votinova, N.A., Goeva, L.V., et al., Compounds Containing the Undecahydrodecaborate Anion B10, Koord. Khim., 2001, vol. 27, no. 9, pp. 662–664.
Sedykh, E.M., Petrovskaya, I.N., Matusievich, G., et al., Microwave Decomposition of Biological Entities for Atomic Absorption and ICP Atomic Emission Analyses, Zh. Anal. Khim., 1991, vol. 46, no. 2, pp. 292–298.
Ochertyanova, L.I., Bel'skii, N.K., and Mustyatsa, V.N., Atomic Absorption Determination of Boron in ETA, Vserossiiskaya konferentsiya po aktual'nym problemam analiticheskoi khimii (All-Russia Conf. on Current Topics in Analytical Chemistry), Moscow, 2002, p. 190.
HGA-700 Graphite Furnace, in Analytical Methods for Furnace AAS: Technical Documentation PN B017–4145, Norwalk: Perkin-Elmer.
Lopatto, Yu.S., Ploticher, Yu.S., Bel'skii, N.K., et al., USSR Inventor's Certificate no. 1 358 325, 1985.
Ochertyanova, L.I. and Bel'skii, N.K., Composition and Properties of Superconducting Materials Containing Rare Earths, V, and W, Neorg. Mater., 2004, vol. 40, no. 1, pp. 58–61 [Inorg. Mater. (Engl. Transl.), vol. 40, no. 1, pp. 48–51].
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Ochertyanova, L.I., Mustyatsa, V.N., Zhizhin, K.Y. et al. Synthesis and Composition of Compounds Containing the B10H- 11 Anion. Inorganic Materials 40, 144–146 (2004). https://doi.org/10.1023/B:INMA.0000016088.12295.5b
Issue Date:
DOI: https://doi.org/10.1023/B:INMA.0000016088.12295.5b