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Hydrolysis of Bis[5,5-dimethyl-3-(4-oxa-1-azoniacyclohexylidene)-1-cyclohexenyl] Sulfide Diperchlorate

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Abstract

Hydrolysis of bis[5,5-dimethyl-3-(4-oxa-1-azoniacyclohexylidene)-1-cyclohexenyl] sulfide diperchlorate, as well as of bis(5,5-dimethyl-3-thioxo-1-cyclohexenyl) sulfide, in the system MeCN-Et3N yields a mixture of bis(5,5-dimethyl-3-oxo-1-cyclohexenyl) sulfide and isomeric 5,5-dimethyl-3-oxo-1-cyclohexenyl 3,3-dimethyl-5-oxo-1-cyclohexenyl sulfide. The structure of the products and their ratio were established by 1H and 13C NMR and IR spectroscopy.

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REFERENCES

  1. Timokhina, L.V., Panova, G.M., Toryashinova, D.-S.D., Albanov, A.I., Sokol'nikova, O.V., and Voronkov, M.G., Russ. J. Org. Chem., 1999, vol. 35, no. 9, pp. 1408-1409.

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Authors and Affiliations

  1. Siberian Division, Russian Academy of Sciences, Favorskii Irkutsk Institute of Chemistry, ul. Favorskogo 1, Irkutsk, 664033, Russia

    L. V. Timokhina, G. M. Panova, L. V. Kanitskaya, D. -S. D. Toryashinova, O. V. Sokol'nikova, S. V. Fedorov & M. G. Voronkov

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  1. L. V. Timokhina
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  2. G. M. Panova
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  3. L. V. Kanitskaya
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  4. D. -S. D. Toryashinova
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  5. O. V. Sokol'nikova
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  6. S. V. Fedorov
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  7. M. G. Voronkov
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Timokhina, L.V., Panova, G.M., Kanitskaya, L.V. et al. Hydrolysis of Bis[5,5-dimethyl-3-(4-oxa-1-azoniacyclohexylidene)-1-cyclohexenyl] Sulfide Diperchlorate. Russian Journal of Organic Chemistry 37, 1335–1337 (2001). https://doi.org/10.1023/A:1013100209089

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  • DOI: https://doi.org/10.1023/A:1013100209089

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