Laminate thickness and resin pressure evolution during axisymmetric liquid composite moulding with flexible tooling
Introduction
Liquid Composite Moulding (LCM) describes a range of composites manufacturing processes where dry fibrous reinforcements are compacted in a mould before being impregnated with a liquid thermosetting matrix. Although all LCM processes use closed moulds, they vary in stiffness from fully rigid to fully flexible, with the heavy tooling of Resin Transfer Moulding (RTM) and Compression RTM (CRTM) processes at one end of the spectrum, and the thin films used in Resin Infusion (a.k.a. VARTM) at the other.
This paper focuses on LCM processes with flexible tooling, in particular RTM Light and Resin Infusion (Fig. 1). RTM Light differs from RTM by replacing one rigid mould half with a lighter, less rigid component, often manufactured from an isotropic glass fibre composite. Clamping is usually provided by application of vacuum to a region at the periphery of the mould cavity, and resin flow is driven by a cavity vacuum, an external injection system, or a combination of the two. RTM Light can provide significant reductions in tooling costs when compared to RTM, while at the same time allowing for higher injection pressures, higher volume fractions, and reduced cycle times when compared to flexible film processes. RTM Light has been employed in the manufacture of a variety of composites products, including boat hulls, bath tubs and automobile chassis components, where part size or volume of production makes rigid tool processes economically or technically unfeasible, and lack of process control or slow cycle times rule out Resin Infusion.
Numerical simulations of rigid tool LCM processes have been in development for over 20 years, with several academic and commercial packages now available [1], [2], [3], [4]. In the last decade a number of Resin Infusion simulations have also been developed [5], [6], [7], [8], [9], [10], along with numerous advances in the areas of computational efficiency, process control and optimisation, and part quality prediction [11], [12], [13], [14], [15], [16], [17]. These simulations are predominantly based on the Finite Element/Control Volume (FE/CV) method because of its efficiency and the ease with which it can model complex part geometries [1], [4], [6].
Extending a rigid tool simulation to flexible tooling processes such as Resin Infusion and RTM Light introduces a number of complexities attributable to the deforming mould and the resulting coupling between laminate thickness and the fluid pressure field in the saturated portion of the part. In particular, a simulation requires a constitutive model for the fibrous reinforcement to link applied stresses to deformations in the fluid–fibre system. Given that reinforcements typically exhibit non-linear load–deformation behaviour with rate and path dependencies [18], [19], [20], [21], [22], either a non-linear solution technique or some form of linearisation is necessary to solve the resulting problem within a FE/CV framework. Even under linear compaction behaviour, the coupling between deformation and flow creates a separate level of non-linearity [23]. Further complication arises in the form of a consolidation process that occurs subsequent to the saturation of the part (Fig. 1). At the completion of filling, mould deflection and part thickness vary spatially, even between regions with the same initial thickness. This post-filling stage, which is not present in RTM, involves the equilibration of fluid pressure and part thickness through bleeding of excess resin. Because the speed at which this process occurs dictates the final part thickness at gelation, it is an important phenomenon for parts where consistency or control of final part thickness is necessary.
Clearly, the interactions between fluid pressure, flow evolution, reinforcement deformation behaviour, and the structural response of the tooling present challenges to the modelling and simulation of flexible tool LCM processes. Despite this, there are still a number of benefits to be had from developing a good simulation of flexible tooling processes, including accurate predictions of filling and post-filling time, guidance over mould design, and laminate thickness predictions throughout the process. It must be recognised that the utility of a flexible tooling simulation extends well beyond fill time prediction, where the improvements over RTM based predictions may be small, by providing estimates of part thickness variation during and at the completion of processing. RTM simulations are unable to account for these effects, and as a consequence will not indicate when they can, and cannot, be discounted.
An important and necessary step in the simulation development process is performing experimental studies to guide model design and to validate simulation results. Such studies help identify the effects of mould compliance and the point at which they necessitate inclusion in a simulation. While a number of experimental studies on Resin Infusion have been presented in the literature [24], [25], [26], [27], there is a paucity of experimental work regarding RTM Light [28], [29]. This paper presents the results of a comprehensive experimental study on the Resin Infusion and RTM Light manufacturing processes, investigating the effect of mould stiffness and injection scheme on variables relevant to industrial process design and numerical simulation development, such as fill time, post-filling time, and cycle-to-cycle variability.
Section snippets
Experimental approach
The experimental study in this paper adopts the common scientific approach of simplifying a problem that includes a large number of variables by selecting and varying those which the authors consider important and controlling for the rest. While typical industrial RTM Light processes may involve complex geometries, preform construction, heat transfer, and resin cure kinetics, they are controlled for or simplified here. The key variables in this study are mould stiffness and injection scheme,
RTM Light mould
Fig. 2 shows a schematic of the experimental facility developed for this study, which is capable of performing and monitoring 1D axisymmetric infusions with partially and fully flexible upper mould components. This has been achieved using a circular mould with a rigid aluminium lower half and upper mould halves of either nylon vacuum film or polycarbonate plates, depending on whether a Resin Infusion or RTM Light process is under consideration (Fig. 3). Two polycarbonate plates with 6 mm and 10
Materials
The fibre reinforcement used in this study is an emulsion-bound E-glass chopped strand mat (CSM) with a nominal areal weight of 450 g/m2 (Owens Corning, product code M705). Actual areal weight measurements were conducted before each test, giving an average value of 454 g/m2 and maximum and minimum values of 469 g/m2 and 433 g/m2. The CSM has random fibre orientation, providing the in-plane isotropic permeability that is necessary for 1D axisymmetric flow. Preforms for all experiments comprised 10
Process time
Fig. 6 shows the fill time and post-filling time for each experiment, along with the ambient temperature. Fill time is defined as the time between the injection gate being opened and the preform being fully saturated, and post-filling time is defined as the time between the end of the filling stage and the time at which the thickness variation across the part is less than 2% of nominal part thickness (0.08 mm). Fig. 6 reveals a strong correlation between process times and ambient temperature,
Repeatability
Although the aggregate property of fill time showed good repeatability, pressure and thickness measurements exhibited significant variability between repeats for the peripheral fill mode, particularly for the Resin Infusion experiments. Fig. 11 compares the pressure traces for all repeats, mould types and fill modes. Once again, time is normalised with respect to fill time. The general trend seen in Fig. 11 is that increasing the mould stiffness or switching to radial filling gives more
Conclusions
An experimental facility has been developed to monitor LCM processes under flexible and semi-rigid tooling. Pressure and laminate thickness data was presented from a series of experiments in which the influence of mould stiffness and fill mode was investigated, revealing key issues in performing and modelling LCM processes with flexible tooling. Investigating the effect of fill mode showed peripheral filling to result in shorter fill times but longer post-filling times when compared to radial
Acknowledgements
The authors acknowledge the support of the Ministry for Science and Innovation, New Zealand and the University of Auckland Doctoral Scholarship programme.
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