Captodative substituent effects XXI. 1: Synthesis of selenenylated captodative olefins via selenenyl halide addition to olefins bearing electron-withdrawing substituents
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2008, TetrahedronCitation Excerpt :For example (Scheme 4), in cyclopropanes 15 and 16, protons cis to the acetyl group have a chemical shift of 2.0–2.2 ppm whereas when they are trans, their chemical shift is lower (1.2–1.5 ppm). These results are consistent with non-selenylated cyclopropanes values.20 Furthermore, 77Se NMR analysis of cyclopropanes allowed us to correlate the chemical shift to the cis or trans configuration.
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Captodative Substitution Effect Part XX : S. Mignani, Z. Janousek, R. Merényi et H.G. Viehe, Bull. Soc. Chim. France, submitted.
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