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Mullite-bonded porous SiC-based Mn3O4–Ni system: control of electrical resistivity, flexural strength, and extrusion

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Abstract

An electrically conductive mullite-bonded porous SiC-based Mn3O4–Ni system was designed, which provided low-temperature sintering and excellent extrudability into complex shapes. Each designed composition contained kaolin (30 wt%) and Mn3O4 (10 wt%) as sintering aids. The combination of Ni (0–20 wt%) and sintering temperature (1100–1300 °C) regulated the electrical resistivity (5.5 × 107–3.4 × 10–1 Ω cm) and flexural strength (33 ± 2–59 ± 3 MPa) of the sintered samples. Interface reactions formed secondary phases [e.g. nickel silicide (Ni2Si) and manganese silicate (MnSiO3)], which decreased the electrical resistivity. The in situ formation of mullite and an increased amount of Ni collectively improved the flexural strength. The sample with 15 wt% Ni sintered at 1200 °C in argon flow had a low electrical resistivity of 5.6 × 10–1 Ω cm and a good flexural strength of 51 ± 4 MPa. The same composition was extruded to form a square honeycomb structure to verify the large-scale viability of the developed composition.

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Acknowledgements

This work was supported by (1) National R&D Program through the National Research Foundation of Korea (NRF) funded by Ministry of Science and ICT [Grant number 2020M3H4A3106359] and (2) the Research Program of the Korea Institute of Materials Science (Republic of Korea) [Grant number PNK 8120].

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  1. Muhammad Shoaib Anwar, Syed Zaighum Abbas Bukhari have equally contributed.

Authors and Affiliations

  1. Ceramic Materials Division, Korea Institute of Materials Science (KIMS), 797 Changwon-daero, Seongsan-gu, Changwon-si, Gyeongsangnam-do, 51508, Republic of Korea

    Muhammad Shoaib Anwar, Syed Zaighum Abbas Bukhari, Jang-Hoon Ha, Jongman Lee & In-Hyuck Song

  2. Department of Advanced Materials Engineering, University of Science and Technology (UST), 217 Gajeong-ro, Yuseong-gu, Daejeon, 34113, Republic of Korea

    Muhammad Shoaib Anwar, Jongman Lee & In-Hyuck Song

Authors
  1. Muhammad Shoaib Anwar
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  2. Syed Zaighum Abbas Bukhari
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  3. Jang-Hoon Ha
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  4. Jongman Lee
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  5. In-Hyuck Song
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Corresponding author

Correspondence to In-Hyuck Song.

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Anwar, M.S., Bukhari, S.Z.A., Ha, JH. et al. Mullite-bonded porous SiC-based Mn3O4–Ni system: control of electrical resistivity, flexural strength, and extrusion. J. Korean Ceram. Soc. 59, 835–845 (2022). https://doi.org/10.1007/s43207-022-00238-5

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