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Microwave-assisted one-pot synthesis of Ag NPs/C and its application in H2O2 and glucose detection

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Abstract

The facile preparation of Ag NPs/C via a one-pot strategy was carried out by microwave treatment of a mixed aqueous solution of AgNO3 and glucose at 180 °C for 20 min without the presence of extra reducing agent. The as-synthesized Ag NPs/C showed high catalytic performance toward the reduction of H2O2. The H2O2 sensor constructed with as-synthesized Ag NPs/C exhibited a short amperometric response time of less than 2 s. The linear range was approximately (0.1―50) mmol/L(r=0.997), and the detection limit was approximately 3.3 μmol/L at a signal-to-noise ratio of 3. A glucose biosensor was fabricated by immobilizing glucose oxidase onto Ag NPs/Cmodified glassy carbon electrode to detect glucose. The glucose sensor had a wide linear response range of 2―22 mmol/L(r=0.999) and a detection limit of 190 μmol/L.

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Authors and Affiliations

  1. Clean Energy Technology Laboratory, Changchun University of Science and Technology, Changchun, 130022, P. R. China

    Chenjiao Ge & Jian Tian

  2. State Key Lab of Electroanalytical Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun, 130022, P. R. China

    Chenjiao Ge, Wenbo Lu & Xuping Sun

Authors
  1. Chenjiao Ge
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  2. Wenbo Lu
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  3. Xuping Sun
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  4. Jian Tian
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Corresponding author

Correspondence to Jian Tian.

Additional information

Supported by the National Natural Science Foundation of China(No.21175129), the National Basic Research Program of China(No.2011CB935800) and the Scientific and Technological Development Plan Project of Jilin Province, China(No. 20100534).

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Ge, C., Lu, W., Sun, X. et al. Microwave-assisted one-pot synthesis of Ag NPs/C and its application in H2O2 and glucose detection. Chem. Res. Chin. Univ. 32, 433–436 (2016). https://doi.org/10.1007/s40242-016-5450-x

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  • DOI: https://doi.org/10.1007/s40242-016-5450-x

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