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A delicate approach to the determination of duloxetine hydrochloride using electrospun polyvinylidene difluoride nanofibers

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Abstract

A simple and delicate approach was developed for the determination of duloxetine hydrochloride using electrospun polyvinylidene difluoride (PVDF) nanofibers. Synthesis of PVDF-based electrospun nanofibers was monitored by ultraviolet visible (UV) spectrophotometer. The characterization was carried out by atomic force microscopy (AFM) and Fourier transform infrared (FTIR) spectroscopy. AFM images showed that the size of synthesized PVDF electrospun nanofibers ranged in between 20 and 340 nm, while the presence of different functional groups was confirmed by FTIR spectroscopy. The synthesized PVDF electrospun nanofibers were applied for the determination of duloxetine hydrochloride. For the determination of duloxetine hydrochloride, a calibration of the standards of known concentration of duloxetine hydrochloride ranging from 1 to 10 mg/L in PVDF electrospun nanofibers solution against their UV absorbance was developed. Excellent regression coefficient (R2 = 0.994) was achieved from the linear calibration curve with 0.48 and 1.6 mg/L of LOD and LOQ, respectively. Results of the study clearly indicated that electrospun nanofibers obtained through PVDF could be used for an accurate determination of duloxetine hydrochloride.

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Authors and Affiliations

  1. National Centre of Excellence in Analytical Chemistry, University of Sindh, Jamshoro, Pakistan

    Sahrish Khatri, Syed Tufail Hussain Sherazi & Sarfaraz Ahmed Mahesar

  2. Nanomaterial Research Group, Department of Textile Engineering, Mehran University of Engineering and Technology, Jamshoro, Pakistan

    Zeeshan Khatri & Farooq Ahmed

  3. International Center for Chemical and Biological Sciences, HEJ Research Institute of Chemistry, University of Karachi, Karachi, 75270, Pakistan

    Sirajuddin

Authors
  1. Sahrish Khatri
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  2. Syed Tufail Hussain Sherazi
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  3. Zeeshan Khatri
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  4. Sarfaraz Ahmed Mahesar
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  5. Sirajuddin
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Correspondence to Syed Tufail Hussain Sherazi.

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Khatri, S., Sherazi, S.T.H., Khatri, Z. et al. A delicate approach to the determination of duloxetine hydrochloride using electrospun polyvinylidene difluoride nanofibers. J IRAN CHEM SOC 19, 2067–2074 (2022). https://doi.org/10.1007/s13738-021-02429-z

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  • DOI: https://doi.org/10.1007/s13738-021-02429-z

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