Abstract
The plastic cold rolling deformation is one method to enhance the microstructure and mechanical characteristics of austenitic steel. The role of effective strain \(\left( \varepsilon \right)\) during cold rolling deformation of the AISI 304 austenitic stainless steel has been studied. The results of the research were collected based on the means of optical, field emission-scanning electron microscopy, X-ray diffraction, microhardness, and tensile stress–strain tests. After 80% of ε, the size of coarse grains of the austenitic phase \((\gamma_{FCC} )\) was diminished as well as larger domains were generated from the martensitic phase \(\left( {\alpha^{\prime}_{BCC} } \right)\). Also, the large carbide particles (M23C6) have been fragmented and they were sprinkled in both phases during the cold rolling process. Therefore, the dislocation density (ρ) has augmented for the deformed alloys. Consequently, the hardness and the ultimate strength (UTS) values are improved to ≈ 150% and ≈ 200%, respectively with increasing the effective strain to 80%. Generally, the increase of the effective strain leads to diminished grain size and increased the values of hardness, yield stress (YS) and UTS of the samples, meanwhile it causes the decrease of their ductility. Moreover, the values of YS have been calculated based on Hall–Petch, Orowan equations and dislocation strengthening formula. Finally, the calculated and the measured results were compared, where both of them are very matching especially at lower values of effective strain.
Graphic Abstract
SEM micrographs of AISI 304 steel samples (a) So, (b) S2, (c) S4 and (d) S5 that were subjected to different percent of plastic deformation during the cold rolling process.
Similar content being viewed by others
References
K.H. Lo, C.H. Shek, J.K.L. Lai, Recent developments in stainless steels. Mater. Sci. Eng. R 65, 39–104 (2009). https://doi.org/10.1016/j.mser.2009.03.001
M.F. McGuire, Stainless Steels for Design Engineers (ASM International, 2008). https://www.asminternational.org/search/-/journal_content/56/10192/05231G/PUBLICATION
G.M. de Bellefon, J.C. van Duysen, Tailoring plasticity of austenitic stainless steels for nuclear applications: review of mechanisms controlling plasticity of austenitic steels below 400 °C. J. Nucl. Mater. 475, 168–191 (2016). https://doi.org/10.1016/j.jnucmat.2016.04.015
C. Zheng, C. Liu, M. Ren, H. Jiang, L. Li, Microstructure and mechanical behavior of an AISI 304 austenitic stainless steel prepared by cold- or cryogenic-rolling and annealing. Mater. Sci. Eng. A 724, 260–268 (2018). https://doi.org/10.1016/j.msea.2018.03.105
J. Lia, Y. Wang, X. Chen, X. Yan, L. Xiang, Microstructure evolution in stress relaxation behavior of austenite AISI 304 stainless steel spring. Mater. Charact. 148, 266–271 (2019). https://doi.org/10.1016/j.matchar.2018.12.026
M. Shaban Ghazani, B. Eghbali, Characterization of the hot deformation microstructure of AISI 321 austenitic stainless steel. Mater. Sci. Eng. A 730, 380–390 (2018). https://doi.org/10.1016/j.msea.2018.06.025
K.-L. Agnieszka, O. Wojciech, R. Wiktoria, K. Joanna, Analysis of deformation texture in AISI 304 steel sheets. Solid State Phenom. 203–204, 105–110 (2013). https://doi.org/10.4028/www.scientific.net/SSP.203-204.105
Y. Lu, B. Hutchinson, D.A. Molodov, G. Gottstein, Effect of deformation and annealing on the formation and reversion of ε-martensite in Fe–Mn–C alloy. Acta Mater. 58, 3079–3090 (2010). https://doi.org/10.1016/j.actamat.2010.01.045
A. Hedayati, A. Najafizadeh, A. Kermanpur, F. Forouzan, The effect of cold rolling regime on microstructure and mechanical properties of AISI 304L stainless steel. J. Mater. Process. Technol. 210, 1017–1022 (2010). https://doi.org/10.1016/j.jmatprotec.2010.02.010
D.G. Rodrigues, G.G.B. Maria, N.A.L. Viana, D.B. Santos, Effect of low cold-rolling strain on microstructure, texture, phase transformation, and mechanical properties of 2304 lean duplex stainless steel. Mater. Charact. 150, 138–149 (2019). https://doi.org/10.1016/j.matchar.2019.02.011
J.T. Benzing, W.A. Poling, D.T. Pierce, J. Bentley, K.O. Findley, D. Raabe et al., Effects of strain rate on mechanical properties and deformation behavior of an austenitic Fe–25Mn–3Al–3Si TWIP-TRIP steel. Mater. Sci. Eng. A 711, 78–92 (2018). https://doi.org/10.1016/j.msea.2017.11.017
B.C. De Cooman, Y. Estrin, S.K. Kim, Twinning-induced plasticity (TWIP) steels. Acta Mater. 142, 283–362 (2018). https://doi.org/10.1016/j.actamat.2017.06.046
G. Sun, L. Du, J. Hu, B. Zhang, R.D.K. Misra, On the influence of deformation mechanism during cold and warm rolling on annealing behavior of a 304 stainless steel. Mater. Sci. Eng. A 746, 341–355 (2019). https://doi.org/10.1016/j.msea.2019.01.020
L.F. Francis, B.J.H. Stadler, C.C. Roberts, Materials Processing, A Unified Approach to Processing of Metals, Ceramics, and Polymers (Academic Press is an imprint of Elsevier 125, London Wall, EC2Y 5AS., Contract No. DE-AC04-94AL85000). ISBN: 978-0-12-385132-1
T. Angel, Formation of martensite in austenitic stainless steels. J. Iron Steel Inst. 177, 165–174 (1954)
R.E. Schramm, R.P. Reed, Stacking fault energies of seven commercial austenitic stainless steels. Metall. Trans. 6A, 1345–1351 (1975)
K. Mao, H. Wang, W. Yaqiao, V. Tomar, J.P. Wharry, Microstructure property relationship for AISI 304/308L stainless steel laser weldment. Mater. Sci. Eng. A 721, 234–243 (2018). https://doi.org/10.1016/j.msea.2018.02.092
H. Wen, T.D. Topping, D. Isheim, D.N. Seidman, E.J. Lavernia, Strengthening mechanisms in a high-strength bulk nanostructured Cu–Zn–Al alloy processed via cryomilling and spark plasma sintering. Acta Mater. 61, 2769–2782 (2013). https://doi.org/10.1016/j.actamat.2012.09.036
R. Chen, P. Guo, Z. Zheng, J. Li, F. Feng, Dislocation based flow stress model of 300M steel in isothermal compression process. Materials 11, 972 (2018). https://doi.org/10.3390/ma11060972
H. Essoussi, S. Elmouhri, S. Ettaqi, E. Essadiqi, Heat treatment effect on mechanical properties of AISI 304 austenitic stainless steel. Procedia Manuf. 32, 883–888 (2019). The 12th international conference interdisciplinarity in engineering
E.A. Eid, A.M. Deghady, A.N. Fouda, Enhanced microstructural, thermal and tensile characteristics of heat-treated Sn–5.0Sb–0.3Cu (SSC-503) Pb-free solder alloy under high pressure. Mater. Sci. Eng. A 743, 726–732 (2019). https://doi.org/10.1016/j.msea.2018.11.137
E.A. Eid, A.B. El-Basaty, A.M. Deghady, S. Kaytbay, A. Nassar, Influence of nano-metric Al2O3 particles addition on thermal behavior, microstructural and tensile characteristics of hypoeutectic Sn–5.0Zn–0.3Cu Pb-free solder alloy. J. Mater. Sci. Mater. Electron. (2019). https://doi.org/10.1007/s10854-019-00726-1
G.E. Dieter, Mechanical Metallurgy, SI Metric Edition (McGraw-Hill Company, New York, 1988), p. 288
B. Ravi Kumar, D. Raabe, Tensile deformation characteristics of bulk ultrafine-grained austenitic stainless steel produced by thermal cycling. Scr. Mater. 66, 634–637 (2012). https://doi.org/10.1016/j.scriptamat.2012.01.052
Q. Duan, H. Pan, F. Bin, J. Yan, An investigation on the strengthening mechanism based on grain-boundary misorientation of high-strength pipeline steel. Steel Res. Int. 2019, 1900317 (2019). https://doi.org/10.1002/srin.201900317
Funding
This study is not funded.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of interest
The authors declare that they have no conflict of interest.
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Eid, E.A., Sadawy, M.M. Role of Effective Strain During Cold Rolling Deformation on Mechanical Characteristics of AISI 304 Steel. Met. Mater. Int. 27, 4536–4549 (2021). https://doi.org/10.1007/s12540-020-00722-9
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s12540-020-00722-9