Abstract
Herein, clove oil encapsulated-chitosan morphologies have been prepared using the emulsion evaporation method. The prepared microstructures were analyzed for z-average and zeta potential using dynamic light scattering analysis and then applied on cellulosic fabric for antibacterial and textile properties using citric acid as a green cross-linker in the presence of sodium hypophosphite as a catalyst. The treated fabric was characterized for surface morphology, chemical functionalities, crystal properties, conventional textile properties including whiteness index, air permeability, crease recovery, stiffness, tensile strength, antibacterial activity, and finish loading/release profiles. The z-averages of the native chitosan microcapsules were recorded as 250±10 nm, and that of 1 and 2 % (v/v) clove oil containing chitosan microcapsules were observed as 300±10 and 380±15 nm, respectively. The chitosan-based microcapsules-treated cellulosic fabrics exhibited good broad-spectrum antibacterial activity with overall retained tensile properties and a sustained release of essential oil in the phosphate-buffered saline. The results were found validated based on statistical analysis.
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H. Tariq and F. Kishwar appreciate the research facilities provided by the National Textile University (NTU), Faisalabad. The authors acknowledge Tanzeel Sarwar, Ph.D. Scholar, NTU for his help in drawing some chemical structures.
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Tariq, H., Rehman, A., Kishwar, F. et al. Sustainable Development of Chitosan Encapsulated Clove Oil Microstructures and Impregnation Thereof onto Cellulosic Fabric for Multipurpose Textile. Fibers Polym 23, 3068–3078 (2022). https://doi.org/10.1007/s12221-022-4399-2
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DOI: https://doi.org/10.1007/s12221-022-4399-2