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Microstructure Evolution and Constitutive Analysis of Al-Mg-Si-Ce-B Alloy during Hot Deformation

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Abstract

In the present work, hot compression tests of Al-Mg-Si-Ce-B alloy were carried out with temperature of 623-823 K and strain rates of 0.01-50 s−1, using a Gleeble 3500 thermal simulation tester. The microstructure evolution of the alloy was investigated by transmission electron microscopy and electron backscattered diffraction. From the true stress–strain curves, work hardening is evident at the beginning of hot compression. Dynamic recovery (DRV) and continuous dynamic recrystallization occurred, and DRV is confirmed to be the main softening mechanism. It is revealed that both the peak and steady values of the true stress decrease with increasing temperature and decreasing strain rate, which implies an increase in the degree of dynamic softening. Physical-based diffusion models and a bio-functional artificial neural network (ANN) model were constructed to predict the hot deformation behavior, of which the accuracy was evaluated based on the average relative error and the correlation coefficient (R). The ANN model was found to have the highest accuracy.

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References

  1. J.K. Sunde, C.D. Marioara, S. Wenner, and R. Holmestad, On the Microstructural Origins of Improvements in Conductivity by Heavy Deformation and Ageing of Al-Mg-Si Alloy 6101, Mater. Charact., 2021, 176, p 111073.

    Article  CAS  Google Scholar 

  2. K.X. Chen, L.Z. Yan, Y.A. Zhang, X.W. Li, Z.H. Li, H.W. Yan, K. Wen, H.W. Liu, Y.N. Li, and B.Q. Xiong, Effect of Solution Heat Treatment on Microstructure and Mechanical Properties of Al-Mg-Si Alloy, Mater. Sci. Forum, 2020, 1003, p 26–30.

    Article  Google Scholar 

  3. G. Liu, Q. Wang, T. Liu, B. Ye, H. Jiang, and W. Ding, Effect of T6 Heat Treatment on Microstructure and Mechanical Property of 6101/A356 Bimetal Fabricated by Squeeze Casting, Mater. Sci. Eng. A, 2017, 696, p 208–215.

    Article  CAS  Google Scholar 

  4. K. Majchrowicz, Z. Pakieła, W. Chrominski, and M. Kulczyk, Enhanced Strength and Electrical Conductivity of Ultrafine-Grained Al-Mg-Si Alloy Processed by Hydrostatic Extrusion, Mater. Charact., 2018, 135, p 104–114.

    Article  CAS  Google Scholar 

  5. Q. Li, Y. Zhu, S. Zhao, Y. Lan, D. Liu, G. Jian, Q. Zhang, and H. Zhou, Influences of Fe, Mn and Y Additions on Microstructure and Mechanical Properties of Hypoeutectic Al–7%Si Alloy, Intermetallics, 2020, 120, p 106768.

    Article  CAS  Google Scholar 

  6. W. Wang, Q. Pan, G. Lin, X. Wang, Y. Sun, X. Wang, J. Ye, Y. Sun, Y. Yu, F. Jiang, J. Li, and Y. Liu, Microstructure and Properties of Novel Al-Ce-Sc, Al-Ce-Y, Al-Ce-Zr and Al-Ce-Sc-Y Alloy Conductors Processed by Die Casting, Hot Extrusion and Cold Drawing, J. Mater. Sci. Technol., 2020, 58, p 155–170.

    Article  Google Scholar 

  7. A. Güzel, A. Jäger, F. Parvizian, H.G. Lambers, A.E. Tekkaya, B. Svendsen, and H.J. Maier, A New Method for Determining Dynamic Grain Structure Evolution During Hot Aluminum Extrusion, J. Mater. Process. Technol., 2012, 212, p 323–330.

    Article  Google Scholar 

  8. S. Liu, Q. Pan, M. Li, X. Wang, X. He, X. Li, Z. Peng, and J. Lai, Microstructure Evolution and Physical-Based Diffusion Constitutive Analysis of Al–Mg–Si Alloy During Hot Deformation, Mater. Des., 2019, 184, p 108181.

    Article  CAS  Google Scholar 

  9. S. Liu, Q. Pan, H. Li, Z. Huang, K. Li, X. He, and X. Li, Characterization of Hot Deformation Behavior and Constitutive Modeling of Al–Mg–Si–Mn–Cr Alloy, J. Mater. Sci., 2018, 54, p 4366–4383.

    Article  Google Scholar 

  10. X.-M. Chen, Y.C. Lin, D.-X. Wen, J.-L. Zhang, and M. He, Dynamic Recrystallization Behavior of a Typical Nickel-Based Superalloy During Hot Deformation, Mater. Des., 2014, 57, p 568–577.

    Article  CAS  Google Scholar 

  11. Y.C. Lin, X.-Y. Wu, X.-M. Chen, J. Chen, D.-X. Wen, J.-L. Zhang, and L.-T. Li, EBSD Study of a Hot Deformed Nickel-Based Superalloy, J. Alloy. Compd., 2015, 640, p 101–113.

    Article  CAS  Google Scholar 

  12. Y.C. Lin, J. Huang, D.-G. He, X.-Y. Zhang, Q. Wu, L.-H. Wang, C. Chen, and K.-C. Zhou, Phase Transformation and Dynamic Recrystallization Behaviors in a Ti55511 Titanium Alloy During Hot Compression, J. Alloys Compd., 2019, 795, p 471–482.

    Article  CAS  Google Scholar 

  13. H. Mirzadeh, Constitutive Description of 7075 Aluminum Alloy During Hot Deformation by Apparent and Physically-Based Approaches, J. Mater. Eng. Perform., 2015, 24, p 1095–1099.

    Article  CAS  Google Scholar 

  14. H. Mirzadeh, A Simplified Approach for Developing Constitutive Equations for Modeling and Prediction of Hot Deformation Flow Stress, Metall. Mater. Trans. A, 2015, 46, p 4027–4037.

    Article  CAS  Google Scholar 

  15. A. Saboori, A. Abdi, S.A. Fatemi, G. Marchese, S. Biamino, and H. Mirzadeh, Hot Deformation Behavior and Flow Stress Modeling of Ti–6Al–4V Alloy Produced Via Electron Beam Melting Additive Manufacturing Technology in Single β-Phase Field, Mater. Sci. Eng. A, 2020, 792, p 139822.

    Article  CAS  Google Scholar 

  16. C. Zener and J.H. Hollomon, Effect of Strain Rate Upon Plastic Flow of Steel, J. Appl. Phys., 1944, 15, p 22–32.

    Article  Google Scholar 

  17. G.R. Johnson and W.H. Cook, Fracture Characteristics of Three Metals Subjected to Various Strains, Strain Rates, Temperatures and Pressures, Eng. Fract. Mech., 1985, 21, p 31–48.

    Article  Google Scholar 

  18. Y. Jia, F. Cao, S. Guo, P. Ma, J. Liu, and J. Sun, Hot Deformation Behavior of Spray-Deposited Al–Zn–Mg–Cu alloy, Mater. Des., 2014, 53, p 79–85.

    Article  CAS  Google Scholar 

  19. S. Wang, J.R. Luo, L.G. Hou, J.S. Zhang, and L.Z. Zhuang, Physically Based Constitutive Analysis and Microstructural Evolution of AA7050 Aluminum Alloy During Hot Compression, Mater. Des., 2016, 107, p 277–289.

    Article  CAS  Google Scholar 

  20. X. Wang, Q. Pan, S. Xiong, and L. Liu, Prediction on Hot Deformation Behavior of Spray Formed Ultra-High Strength Aluminum Alloy—A Comparative Study Using Constitutive Models, J. Alloys Compd., 2018, 735, p 1931–1942.

    Article  CAS  Google Scholar 

  21. J.M. Cabrera, A. Al Omar, J.M. Prado, and J.J. Jonas, Modeling the Flow Behavior of a Medium Carbon Microalloyed Steel Under Hot Working Conditions, Metall. Mater. Trans. A, 1997, 28, p 2233–2244.

    Article  Google Scholar 

  22. K. Singh, S.K. Rajput, and Y. Mehta, Modeling of the Hot Deformation Behavior of a High Phosphorus Steel Using Artificial Neural Networks, Mater. Discov., 2016, 6, p 1–8.

    Article  Google Scholar 

  23. Y. Sun, W.D. Zeng, Y.Q. Zhao, X.M. Zhang, Y. Shu, and Y.G. Zhou, Modeling Constitutive Relationship of Ti40 Alloy Using Artificial Neural Network, Mater. Des., 2011, 32, p 1537–1541.

    Article  CAS  Google Scholar 

  24. Y. Sun, Q. Pan, W. Wang, A. Li, and W. Song, Microstructural Evolution and Constitutive Analysis Combined with Weight Optimization Method of Al–7.82Zn–1.96Mg–2.35Cu–0.11Zr Alloy During Hot Deformation, J. Alloys Compd., 2018, 732, p 902–914.

    Article  CAS  Google Scholar 

  25. D. Odoh, Y. Mahmoodkhani, and M. Wells, Effect of Alloy Composition on Hot Deformation Behavior of Some Al-Mg-Si Alloys, Vacuum, 2018, 149, p 248–255.

    Article  CAS  Google Scholar 

  26. Y. Cao, Y. Liu, B. Liu, and W. Zhang, Precipitation Behavior During Hot Deformation Of Powder Metallurgy Ti-Nb-Ta-Zr-Al High Entropy Alloys, Intermetallics, 2018, 100, p 95–103.

    Article  CAS  Google Scholar 

  27. A.G. Atkins, Deformation-Mechanism Maps (the Plasticity and Creep of Metals and Ceramics): by H.J. Frost and M.F. Ashby, Pergamon, Oxford 1982. ISBN 0-08-029338-7, ix + 166 pages, illustrated, flexicover, US $25. J. Mech. Work. Technol. (1984).

  28. H. Mirzadeh, J.M. Cabrera, and A. Najafizadeh, Constitutive Relationships for Hot Deformation of Austenite, Acta Mater., 2011, 59, p 6441–6448.

    Article  CAS  Google Scholar 

  29. A. Thomas, M. El-Wahabi, J.M. Cabrera, and J.M. Prado, High Temperature Deformation of Inconel 718, J. Mater. Process. Technol., 2006, 177, p 469–472.

    Article  CAS  Google Scholar 

  30. H.J. McQueen and N.D. Ryan, Constitutive Analysis in Hot Working, Mater. Sci. Eng. A, 2002, 322, p 43–63.

    Article  Google Scholar 

  31. F. Reyes-Calderón, I. Mejía, and J.M. Cabrera, Hot Deformation Activation Energy (QHW) of Austenitic Fe–22Mn–1.5Al–1.5Si–0.4C TWIP Steels Microalloyed with Nb, V, and Ti, Mater. Sci. Eng. A, 2013, 562, p 46–52.

    Article  Google Scholar 

  32. Y.J. Qin, Q.L. Pan, Y.B. He, W.B. Li, X.Y. Liu, and X. Fan, Artificial Neural Network Modeling to Evaluate and Predict the Deformation Behavior of ZK60 Magnesium Alloy During Hot Compression, Mater. Manuf. Process., 2010, 25, p 539–545.

    Article  CAS  Google Scholar 

  33. Y. Han, G. Qiao, J. Sun, and D. Zou, A Comparative Study on Constitutive Relationship of as-cast 904L Austenitic Stainless Steel During Hot Deformation Based on Arrhenius-Type and Artificial Neural Network Models, Comput. Mater. Sci., 2013, 67, p 93–103.

    Article  CAS  Google Scholar 

  34. K. Li, Q. Pan, R. Li, S. Liu, Z. Huang, and X. He, Constitutive Modeling of the Hot Deformation Behavior in 6082 Aluminum Alloy, J. Mater. Eng. Perform., 2019, 28, p 981–994.

    Article  CAS  Google Scholar 

Download references

Acknowledgments

This work was supported by the Key Research and Development Program of Guangdong Province (No. 2020B010186002).

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Correspondence to Bing Liu.

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Yu, Y., Pan, Q., Wang, W. et al. Microstructure Evolution and Constitutive Analysis of Al-Mg-Si-Ce-B Alloy during Hot Deformation. J. of Materi Eng and Perform 31, 4707–4720 (2022). https://doi.org/10.1007/s11665-021-06561-y

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  • DOI: https://doi.org/10.1007/s11665-021-06561-y

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