Abstract
In this work, microstructural changes during creep of 9Cr-1Mo steel were characterized using ultrasonic and hardness measurements. The creep testing of this steel was firstly performed at 873 K under the initial stresses of 160 and 175 MPa, respectively. Then, eight specimens under each stress level were prepared by the interrupted tests to simulate various creep states. Subsequently, two parameters of ultrasonic attenuation and velocity were introduced by the ultrasonic testing. Experiment results showed that regardless of the stresses, the ultrasonic attenuation experiences a peak at about 20% of the creep rupture time and a minimum value at about 50%, showing a strong correlation between ultrasonic attenuation and the creep life fraction. In addition to a slight increase during the primary creep, the ultrasonic velocity exhibits a significant change during the tertiary creep. Based on the analysis of microstructure changes, it indicated that the ultrasonic attenuation is significantly sensitive to the dynamic changes of the dislocation. In contrast, the velocity is mainly related to the evolution of precipitates. The Vickers hardness decreases monotonously during the creep process and presents a linear relation with the inverse of average diameter of M23C6 carbides during the secondary and tertiary creep. Accordingly, it suggested that the present ultrasonic and hardness measurements provided a convenient tool to evaluate the microstructure evolution during creep degradation of heat-resistant steels.
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R. Viswanathan and W. Bakker, Materials for Ultrasupercritical Coal Power Plants—Boiler Materials: Part 1, J. Mater. Eng. Perform., 2001, 10(1), p 81–95
M. Sireesha, S. Sundaresan, and S.K. Albert, Microstructure and Mechanical Properties of Weld Fusion Zones in Modified 9Cr-1Mo Steel, J. Mater. Eng. Perform., 2001, 10(3), p 320–330
B.A. Badidi, A. Benchaala, and K. Alem, Ultrasonic Characterization of Materials Hardness, Ultrasonics, 2000, 38(1–8), p 224–227
Z. Keran, M. Mihaljević, B. Runje, and D. Markučič, Ultrasonic Testing of Grain Distortion Direction in Cold Formed Aluminium Profile, Arch. Civ. Mech. Eng., 2017, 17(2), p 375–381
S. Sahoo, B.B. Jha, and T.K. Sahoo, Microstructural Characterisation of Thermally Degraded 2·25Cr-1Mo Steel Using Ultrasonic Measurement and Its Correlation with Mechanical Properties, Mater. Sci. Technol., 2014, 30(10), p 1197–1204
M. Vasudevan and P. Palanichamy, Characterization of Microstructural Changes During Annealing of Cold Worked Austenitic Stainless Steel Using Ultrasonic Velocity Measurements and Correlation with Mechanical Properties, J. Mater. Eng. Perform., 2002, 11(2), p 169–179
F. Uzun and A.N. Bilge, Ultrasonic Investigation of the Effect of Carbon Content in Carbon Steels on Bulk Residual Stress, J. Nondestr. Eval., 2015, 34(2), p 1–10
H. Suzuki, T. Maruyama, and S. Mukohara, Effects of Heat-Treatment and Neutron-Irradiation on Ultrasonic Attenuation and Young’s Modulus of Carbon, J. Nucl. Mater., 1978, 78(2), p 374–379
M. Toozandehjani, K.A. Matori, F. Ostovan, F. Mustapha, N.I. Zahari, and A. Oskoueian, On the Correlation Between Microstructural Evolution and Ultrasonic Properties: A Review, J. Mater. Sci., 2015, 50(7), p 2643–2665
A.B. Bouda, S. Lebaili, and A. Benchaala, Grain Size Influence on Ultrasonic Velocities and Attenuation, Ndt E Int., 2003, 36(1), p 1–5
K. Vijayalakshmi, V. Muthupandi, and R. Jayachitra, Influence of Heat Treatment on the Microstructure, Ultrasonic Attenuation and Hardness of SAF 2205 Duplex Stainless Steel, Mater. Sci. Eng., A, 2011, 529(1), p 447–451
M.M.E. Rayes, E.A. El-Danaf, and A.A. Almajid, Characterization and Correlation of Mechanical, Microstructural and Ultrasonic Properties of Power Plant Steel, Mater. Charact., 2015, 100, p 120–134
X. Liu, S. Takamori, and Y. Osawa, Effect of Matrix Structure on Ultrasonic Attenuation of Ductile Cast Iron, J. Mater. Sci., 2007, 42(1), p 179–184
X. Liu, S. Takamori, Y. Osawa, and F. Yin, Diffraction Correction in the Measurement of Ultrasonic Attenuation, Mater. Sci. Eng., A, 2006, 442(1), p 527–531
F. Abe, Precipitate Design for Creep Strengthening of 9% Cr Tempered Martensitic Steel for Ultra-Supercritical Power Plants, Sci. Technol. Adv. Mater., 2008, 9(1), p 013002
K. Guguloth and N. Roy, Creep Deformation Behavior of 9Cr1MoVNb (ASME Grade 91) Steel, Mater. Sci. Eng., A, 2017, 680(5), p 388–404
B. Xiao, L. Xu, L. Zhao, H. Jing, Y. Han, and Z. Tang, Microstructure Evolution and Fracture Mechanism of a Novel 9Cr Tempered Martensite Ferritic Steel During Short-Term Creep, Mater. Sci. Eng., A, 2017, 707(7), p 466–477
M. Taneike, F. Abe, and K. Sawada, Creep-Strengthening of Steel At High Temperatures Using Nano-Sized Carbonitride Dispersions, Nature, 2003, 424(6946), p 294–296
C.S. Kim, Mechanical Softening of Tempered Martensitic Steel Resulting From Long-Term Aging and Creep, Mater. Res. Innov., 2016, 19(sup5), p S5–1016-S1015-1019
C.S. Kim, S.I. Kwun, B.Y. Ahn, S.H. Nahm, and S.S. Lee, Microstructural Characterization of Creep Damaged 11Cr-3.5W-3Co Steel, Solid State Phenom., 2006, 118, p 475–478
R. Truell, C. Elbaum, B.B. Chick, and C. Garland, Ultrasonic Methods in Solid State Physics, Phys. Today, 1971, 24(1), p 77–79
A. Kumar, B.K. Choudhary, K. Laha, T. Jayakumar, K.B.S. Rao, and B. Raj, Characterisation of Microstructure in 9% Chromium Ferritic Steels Using Ultrasonic Measurements, Trans. Indian Inst. Met., 2003, 56(5), p 483–497
T. Ohtani, Acoustic Damping Characterization and Microstructure Evolution during Creep of a Martensitic Stainless Steel, J. Soc. Mater. Sci. Jpn., 2007, 56(2), p 114–120
A. Granato and K. Lücke, Theory of Mechanical Damping Due to Dislocations, J. Appl. Phys., 2004, 27(6), p 583–593
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This work was supported by the National Natural Science Foundation of China (Grant No. 51371142).
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Zhu, L., Liu, X., Fan, P. et al. A Study of Microstructure Evolution During Creep of 9Cr-1Mo Steel Using Ultrasonic and Hardness Measurements. J. of Materi Eng and Perform 28, 2348–2355 (2019). https://doi.org/10.1007/s11665-019-03987-3
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DOI: https://doi.org/10.1007/s11665-019-03987-3