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In situ study on dendrite growth of metallic alloy by a synchrotron radiation imaging technology

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Abstract

This study was trying to observe the real-time dendrite growth of Sn-Bi and Sn-Pb binary alloys by a synchrotron radiation imaging technology. The imaging system includes an intense and high brightness synchrotron radiation source, a high-resolution and fast-readout charge coupled device camera, an alloy sample and a Bridgman solidification system. The imaging experiments were done at Beijing Synchrotron Radiation Facility with an updated synchrotron radiation imaging technique, diffraction-enhanced imaging, which was firstly used to study the dendrite growth of metallic alloy. A series of growth behavior and morphology evolution of dendrite have been in situ observed, such as columnar-to-equiaxed transition, dendrite competition, dendrite fragmentation and floating, etc., which can offer the direct proofs to verify or improve the solidification theories of metallic alloy. This research opens a novel window for the study of alloy solidification and enables the unambiguous understanding of solidification processes in optically opaque, metallic alloys.

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References

  1. Daye D M. Solidification of Metals and Alloys. Beijing: Mechanical Industry Press, 1983. 1–2

    Google Scholar 

  2. Young K P, Kirkwood D H. The dendrite arm spacings of alμminμm-copper alloys solidified under steady-state conditions. Metall Trans A, 1975, 6A: 197–205

    Google Scholar 

  3. Peterson P W, Kattamis T Z, Giamei A F. Coarsening kinetics during solidification of Ni-Al-Ta dendrite monocrystals. Metall Trans A, 1980, 11A: 1059–1065

    Google Scholar 

  4. Grugel R N. Secondary and tertiary dendrite arm spacing relationships in directionally solidified Al-Si alloys. J Mater Sci, 1993, 28: 677–683

    Article  Google Scholar 

  5. Flemings M C, Kattamis T Z, Bardes B P. Dendrite arm spacing in aluminum alloys. Trans AFS, 1991, 176: 501–506

    Google Scholar 

  6. Jie W Q, Zhou Y H. A model study on the transition from columnar crystal zone to equiaxed. J Northwest Polytechnical Univ, 1988, 6(1): 29–40

    Google Scholar 

  7. Grange G, Gastaldi J, Jourdan C, et al. Evolution of characteristic pattern parameters in directional solidification of thin sample of a dilute Al-Cu alloy. J Cryst Growth, 1995, 151: 192–199

    Article  Google Scholar 

  8. Zhu M F, Dai T, Li C Y, et al. Modeling of dendritic growth in the presence of convection. Sci China Ser E-Tech Sci, 2005, 35: 673–688

    Google Scholar 

  9. Zhu M F, Yu J, Hong J S. Computer simulation of metal solidification microstructures. Eng Sci, 2004, 6(5): 8–16

    Google Scholar 

  10. Zhu C S, Wang Z P, Jing T, et al. Progress in convection effects on dendritic growth using phase-field method. Mater Rev, 2004, 18: 26–28

    Google Scholar 

  11. Lan C W, Hsu C M, Liu C C, et al. Adaptive phase field simulation of dendritic growth in a forced flow at various supercoolings. Phys Rev E, 2002, 65: 061601

    Article  Google Scholar 

  12. Xu Q Y, Xiong S M, Liu B C. Advances in microstructure simulation of casting alloy. Mater Rev, 2002, 16: 11–14

    Google Scholar 

  13. Tönhardt R, Amberg G. Dendritic growth of randomly oriented nuclei in a shear flow. J Crystal Growth, 2000, 213: 161–187

    Article  Google Scholar 

  14. Thi H N, Jamgotchian H, Gastaldi J, et al. Preliminary in situ and real-time study of directional solidification of metallic alloys by X-ray imaging techniques. J Phys D: App Phys, 2003, 36: A83–A86

    Article  Google Scholar 

  15. Billia B, Bergeon N, Thi H N, et al. Cumulative mechanical moments and microstructure deformation induced by growth shape in columnar solidification. Phys Rev Lett, 2004, 93: 126105

    Article  Google Scholar 

  16. Yasuda H, Ohnaka I, Kawasaki K, et al. Direct observation of stray crystal formation in unidirectional solidification of Sn-Bi alloy by X-ray imaging. J Crystal Growth, 2003, 262: 645–652

    Article  Google Scholar 

  17. Mathiesen R H, Arnberg L. X-ray radiography observations of columnar dendritic growth and constitutional undercooling in an Al-30 wt%Cu alloy. Acta Mater, 2005, 53: 947–956

    Article  Google Scholar 

  18. Mathiesen R H, Arnberg L, Mo F, et al. Time resolved X-ray imaging of dendrite growth in binary alloys. Phys Rev Lett, 1999, 83: 5062–5065

    Article  Google Scholar 

  19. Li B, Brody H D, Kazimirov A. Real-time observation of dendrite coarsening in Sn-13%Bi alloy by synchrotron microradiography. Phys Rev E, 2004, 70: 062602

    Article  Google Scholar 

  20. Zhu P P, Yuan Q X, Huang W X, et al. Principles of X-ray diffraction enhanced imaging. Acta Phys Sin, 2006, 55: 1089–1098

    Google Scholar 

  21. Huang W X, Yuan Q X, Tian Y L, et al. Diffraction-enhanced imaging experiments in BSRF. Acta Phys Sin, 2005, 54: 677–681

    Google Scholar 

  22. LaCombe J C, Koss M B, Glicksman M E. Nonconstant tip velocity in microgravity dendritic growth. Phys Rev Lett, 1999, 83: 2997–3000

    Article  Google Scholar 

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Correspondence to TongMin Wang.

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Wang, T., Xu, J., Li, J. et al. In situ study on dendrite growth of metallic alloy by a synchrotron radiation imaging technology. Sci. China Technol. Sci. 53, 1278–1284 (2010). https://doi.org/10.1007/s11431-010-0087-3

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  • DOI: https://doi.org/10.1007/s11431-010-0087-3

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