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The Effect of Sulphur and Water Treatments on the Performance of Pd/β-Zeolite Diesel Oxidation Catalysts

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Abstract

Sulphur, sulphur-water, and water pretreatments were done to find out the effect of these compounds on a diesel oxidation Pd/β-zeolite catalyst and β-zeolite washcoat. After pretreatments, the samples were analysed by BET, XRF, TEM-SEM, and XPS. In addition, the activity of fresh and pretreated Pd/β-zeolite catalysts was studied utilizing the by Gasmet FT-IR in production gas analysis. Sulphur compounds (SO2 or −SO4) were found to have a deactivating effect on the activity of the studied Pd/β-zeolite catalyst.

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Acknowledgments

Authors acknowledge financial support from the 100th Anniversary Foundation of the Federation of Finnish Technology Industries. The authors are grateful to Ecocat Oy for supplying the catalysts. A. Hallikainen is acknowledged for carrying out the experiments.

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Authors and Affiliations

  1. Department of Process and Environmental Engineering, University of Oulu, P.O. Box 4300, 90014, University of Oulu, Finland

    Tanja Kolli, Mika Huuhtanen & Riitta L. Keiski

  2. Department of Materials Science, Tampere University of Technology, P.O. Box 589, 33101, Tampere, Finland

    Tomi Kanerva, Minnamari Vippola & Toivo Lepistö

  3. Ecocat Oy, Typpitie 1, 90650, Oulu, Finland

    Kauko Kallinen & Toni Kinnunen

  4. Department of Applied Physics, Aalto University School of Science and Technology, Aalto University, P.O. Box 11100, 00076, Aalto, Finland

    Jouko Lahtinen

Authors
  1. Tanja Kolli
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  2. Mika Huuhtanen
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  3. Tomi Kanerva
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  4. Minnamari Vippola
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  5. Kauko Kallinen
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  7. Toivo Lepistö
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  8. Jouko Lahtinen
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  9. Riitta L. Keiski
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Correspondence to Tanja Kolli.

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Kolli, T., Huuhtanen, M., Kanerva, T. et al. The Effect of Sulphur and Water Treatments on the Performance of Pd/β-Zeolite Diesel Oxidation Catalysts. Top Catal 54, 1185 (2011). https://doi.org/10.1007/s11244-011-9740-8

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  • DOI: https://doi.org/10.1007/s11244-011-9740-8

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