Abstract
Chromatographic instrumentation has been really influential in shaping the modern chemical practice, and yet it has been largely overlooked by history of science.Gas chromatography in the 1960s was considered the analytical technique closer to becoming dominant, and being the first automated chromatography set the standards that all the subsequent chromatographic instrumentation had to fulfill. Networks of specialists, groups of actors, corporate strategies and the analytical practice itself, were all affected and in many ways because of the entrance of gas chromatography in the chemical laboratory and in the instrumentation market. This paper gives a view of the early history of the gas chromatography instrumentation, relates it to the broader research-technology phenomenon and discusses issues of education and group reproduction in the case of the groups of technologists of the era. The chaotic elements of knowledge transfer during the instrumentation revolution in chemistry are being highlighted and they are being connected to the observable radical innovation of the period.
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Notes
Interestingly, in the important for the epistemology of instrumentation book of Baird, Thing Knowledge (University of California Press 2004), three different types of instrumentation are distinguished (p. 5): (a) models, (b) devices that create a phenomenon, and (c) measuring instruments. In order for the chromatography apparatuses to fit the third category, the meaning of the word “measurement” must be broadened. Similarly, it is unclear where should computers as scientific instruments be placed in this categorization.
The term here is employed with the meaning given to it by Suzan Leigh Star and James R. Griesemer in 1989. Research instruments being tools are subjects of contextual alterations of meaning due to different uses as Heidegger would have it—that is, their meaning changes according to different uses (Heidegger in Ihde 2009). However, it could be the case that the more complicated a tool is the least the alterations of meaning from context to context.
The journal L’Année Sociologique was founded by Durkheim in 1898, after he had published a manifesto (Les Règles de la Méthode Sociologique) and had founded the first sociology department at the University of Bordeaux in 1895.
For Richard Kuhn, see his Nobel Prize biography online at: http://www.nobelprize.org/nobel_prizes/chemistry/laureates/1938/kuhn-bio.html (retrieval July 11th 2012); for Edgar Lederer (1983).
http://shop.perkinelmer.com/Content/RelatedMaterials/nlt_lcgc50yearsofgc.pdf (retrieval September 16, 2011).
For example the case of the first HPLC apparatus (see Gerontas et al. in preparation).
The first HPLC was constructed by Horváth and Lipsky at the Yale University in 1965. See in detail: Ibid. Gerontas et al. (in preparation).
See Kenndler (2001); Kirkland (2004) and Unger (2004). For Glueckauf, see the Biographical Memoirs of the Fellows of the Royal Society (available online: http://www.jstor.org/stable/10.2307/769825).
Reinhardt is making a strong case for the importance of the middleman minorities in the migration of technological knowledge in chemistry. See op. cit. Reinhardt, p. 21.
The term “trading zone” is here used with the meaning that Galison gives to it. Scientists and engineers of different paradigms and functioning in different environments can agree on a given set of rules and meanings, which will allow the transfer of knowledge between their milieus despite the differences.
Laboratory Instrumentation: Laboratory Automation, Separation Techniques, Chemicals, Laboratory Equipment: Contributions from American Laboratory and International Laboratory; Series II, Volumes II and IV respectively, 1977.
http://www.isa.org/Content/NavigationMenu/General_Information/About_ISA1/ISAs_History/ISAs_History.htm (retrieval May 2011). The history of the early ISA is intimately connected to the history of the PITTCON.
For the role of the workshops and the training centres, see: op.cit. Gerontas et al. (in preparation).
The material contains slides (PE-B, B:10, FF:2, FF: 3, FF: 4), notes and brochures scattered throughout (for example PE-B, B: 10, B:11) and a whole side-collection with seminar material.
More about that, and its effects in op.cit (Gerontas et al. in preparation).
For the effects of advertisement (see Gerontas and Lykknes in preparation).
GC Laboratory Instrumentation; Contributions from American Laboratory and International Laboratory, pp. 179–180.
For the first steps of HPLC, see details in op.cit. Gerontas et al. (in preparation).
See Horváth (1992). For his role in the construction of the first HPLC see: op. cit. Gerontas et al. (in preparation).
Indeed, for the majority of the seminars and workshops that were offered, either in the course centres or in other sites, there were no prerequisites concerning the educational background of the participants. Since the knowledge offered was praxical, there was something there for both the academic and the technician. When suggestions of books were given, those were more often than not manuals, corporate published handbooks and brochures (see Gerontas et al. in preparation).
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Acknowledgments
The completion of this work would not be possible without the generous support of the Chemical Heritage Foundation, Philadelphia, USA. I am grateful for the financial support of my research, the access offered to most valuable archive material relating to my subject, and the license to use this material. Special thanks to Andrew Mangravite, Amanda Shields and Ashley Augustyniak of the Chemical Heritage Foundation. Thanks are also due to historians and philosophers of science who heard parts of my work in conferences and assisted to its improvement through questions, observations and comments. I also want to thank my supervisor, friends and colleagues at the Department of Chemistry of the Norwegian University of Science and Technology for their general support, comments and advice.
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Gerontas, A. Creating New Technologists of Research in the 1960s: The Case of the Reproduction of Automated Chromatography Specialists and Practitioners. Sci & Educ 23, 1681–1700 (2014). https://doi.org/10.1007/s11191-013-9654-x
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DOI: https://doi.org/10.1007/s11191-013-9654-x