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Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations

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Abstract

A green sonochemical method was developed for preparing silver nanoparticles (Ag-NPs) in κ-carrageenan in different concentrations of AgNO3. The κ-carrageenan was used as an eco-friendly stabilizer and ultrasonic irradiation as a green reducing agent. The number of Ag-NPs increased with increasing concentrations of AgNO3. Formation of Ag/κ-carrageenan was determined by UV–visible spectroscopy where the surface plasmon absorption maximum was observed at 410–416 nm. XRD analysis showed the Ag-NPs are of a face-centered cubic structure. TEM images showed the well-dispersed Ag-NPs with an average particle size <5 nm. SEM images showed the spherical shape of the Ag-NPs. The FT-IR spectrum indicated the presence of κ-carrageenan in capping the Ag-NPs. The use of photo irradiation provides a green and economic method features to the synthesis reported in this study.

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Acknowledgments

The authors would like acknowledge technical support from the staff of the Faculty of Engineering, Institute of ITMA and Bioscience at UPM in this work.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science, Universiti Putra Malaysia (UPM), 43400, Serdang, Selangor, Malaysia

    Randa Fawzi Elsupikhe & Mansor B. Ahmad

  2. Malaysia-Japan International Institute of Technology, Universiti Technologi Malaysia, Jalan Sultan Yahya Petra (Jalan Semarak), 54100, Kuala Lumpur, Malaysia

    Kamyar Shameli

Authors
  1. Randa Fawzi Elsupikhe
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  2. Kamyar Shameli
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  3. Mansor B. Ahmad
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Correspondence to Kamyar Shameli or Mansor B. Ahmad.

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Elsupikhe, R.F., Shameli, K. & Ahmad, M.B. Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations. Res Chem Intermed 41, 8515–8525 (2015). https://doi.org/10.1007/s11164-014-1907-z

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  • DOI: https://doi.org/10.1007/s11164-014-1907-z

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