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SrSnO3:Nd obtained by the polymeric precursor method

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Abstract

In this work, the synthesis of Nd-doped SrSnO3 by the polymeric precursor method, with calcination between 250 and 700 °C is reported. The powder precursors were characterized by TG/DTA and high temperature X-ray diffraction (HTXRD). After heat treatment, the material was characterized by XRD and infrared spectroscopy. Ester and carbonate amounts were strictly related to Nd-doping. According to XRD patterns, the orthorhombic perovskite was obtained at 700 °C for SrSnO3 and SrSn0.99Nd0.01O3. For Sr0.99Nd0.01SnO3, the kinetics displayed an important hole in the crystallization process, as no peak was observed in HTXRD up to 700 °C, while a XRD patterns showed a crystalline material after calcination at 250 °C.

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Acknowledgements

The authors acknowledge CNPq/MCT, FINEP and CAPES for the financial support.

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Authors and Affiliations

  1. LACOM, Departamento de Química/CCEN, Universidade Federal da Paraíba, Campus I, João Pessoa, PB, Brazil

    Soraia Carvalho de Souza, Mary Cristina Ferreira Alves, A. Luiz M. de Oliveira, F. Ticiano Gomes Vieira, L. E. B. Soledade, A. G. de Souza & Iêda M. Garcia dos Santos

  2. CMDMC—LIEC, Instituto de Química, UNESP, Araraquara, SP, Brazil

    E. Longo

  3. LSR, Departamento de Engenharia Mecânica/CT, UFPB, Campus I, João Pessoa, PB, CEP 58059-900, Brazil

    Rodinei Medeiros Gomes

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  1. Soraia Carvalho de Souza
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  2. Mary Cristina Ferreira Alves
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  3. A. Luiz M. de Oliveira
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  4. E. Longo
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  5. F. Ticiano Gomes Vieira
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  6. Rodinei Medeiros Gomes
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  7. L. E. B. Soledade
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  8. A. G. de Souza
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  9. Iêda M. Garcia dos Santos
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Correspondence to Soraia Carvalho de Souza.

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de Souza, S.C., Alves, M.C.F., de Oliveira, A.L.M. et al. SrSnO3:Nd obtained by the polymeric precursor method. J Therm Anal Calorim 97, 185–190 (2009). https://doi.org/10.1007/s10973-009-0239-5

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  • DOI: https://doi.org/10.1007/s10973-009-0239-5

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