Abstract
Single-crystalline bulk GdBa2Cu3O7−δ (GdBCO) superconductors were fabricated with top-seeded infiltration-growth technique (TSIG) in air by adding the different amounts of Dy2BaCuO5 (Dy-211) particles (5, 10, 15, 20, 25, 30, 35, and 40 wt%). All the samples show superconducting critical temperature at ∼93 K with sharp transition irrespective of the chemical composition. X-ray diffraction measurements confirmed that all the samples were single domain with high alignment. Microstructural studies through scanning electron microscopy showed that TSIG-processed GdBCO samples contained 211 phase particles of two different sizes, i.e., ∼2–4 and ∼10 μ m. The addition of Dy-211 phase particles led to a significant enhancement of critical current density (J c) at 77 K. GdBCO superconductor with the addition of 20 wt% of Dy-211 showed the highest J c of 45.5 kA/cm 2 at 77 K and self field.
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Murakami, M., Yoo, S.I., Higuchi, T., Sakai, N., Weltz, J., Koshizuka, N., Tanaka, S.: Flux pinning in melt-grown NdBa2Cu3Oy and SmBa2Cu3Oy superconductors. Jpn. J. Appl. Phys. 33, L715–L717 (1994)
Pradhan, A.K., Muralidhar, M., Koblischka, M.R., Murakami, M., Nakao, K., Koshizuka, N.: Evidence of strong flux pinning in melt-processed ternary (Nd–Eu–Gd)Ba2Cu3Oy superconductors. Appl. Phys. Lett. 75, 253–255 (1999)
Muralidhar, M., Sakai, N., Nishiyama, M., Jirsa, M., Machi, T., Murakami, M.: Pinning characteristics in chemically modified (Nd, Eu, Gd)–Ba–Cu–O superconductors. Appl. Phys. Lett. 82, 943–945 (2003)
Awad, R., Abou Aly, A.I., Mohammed, N.H., Isber, S., Motaweh, H.A., El-Said Bakeer, D.: Investigation on superconducting properties of GdBa2Cu3O7−δ added with nano sized ZnFe2O4. J. Alloys Compd. 610, 614–622 (2014)
Sakai, N.: Murakami.: Fabrication of large melt-textured Gd-Ba-Cu-O superconductor with Ag addition. Phys. C 341–348, 2409–2412 (2000)
Izumi, M., Yabe, T., Wada, T., Maeda, A., Uchinokura, K., Tanaka, S., Asano, H.: Structural properties of the superconductor LaBa2Cu3−y O7−z in the solid solution system La1 + x Ba2−x Cu3−y O7−z . Phys. Rev. B 40, 6771–6786 (1989)
Zhang, K., Dabrowski, B., Segre, C.U., Hinks, D.G., Schuller, I.K., Jorgensen, J.D., Slaski, M.: Solubility and superconductivity in RE(Ba2−x REx)Cu3O7 + δ systems (RE = Nd, Sm, Eu, Gd, Dy). J. Phys. C Solid State Phys. 20, L935–L940 (1987)
Kramer, M.J., Yoo, S.I., McCallum, R.W., Yelon, W.B., Xie, H., Allenspach, P.: Hole filling, charge transfer and superconductivity in Nd1 + x Ba2−x Cu3O7 + δ . Phys. C 219, 145–155 (1994)
Murakami, M., Yoo, S.I., Higuchi, T., Sakai, N., Weltz, J., Koshizuka, N., Tanaka, S.: Jpn. J. Appl. Phys. 33, L715–L717 (1994)
Muralidhar, M., Murakami, M.: Effects of Gd BaCuO addition on critical current characteristics in melt-processed Nd, Eu, Gd–Ba–Cu–O. Phys. C 309, 43–48 (1998)
Muralidhar, M., Tomita, M., Suzuki, K., Jirsa, M., Fukumoto, Y., Ishihara, A.: A low-cost batch process for high-performance melt-textured GdBaCuO pellets. Supercond. Sci. Technol. 23, 045033 (2010)
Xu, C., Hu, A., Sakai, N., Izumi, N., Hirabayashi, I.: Effect of BaO2 and fine Gd2BaCuO7−δ addition on the superconducting properties of air-processed GdBa2Cu3O7−δ . Supercond. Sci. Technol. 18, 229–233 (2005)
Li, B., Xu, K., Hara, S., Zhou, D., Zhang, Y., Izumi, M.: Enhanced pinning effect in air-processed Gd-123 bulk superconductors with BaTiO addition. Phys. C 475, 51–56 (2012)
Shi, Y., Hari Babu, N., Iida, K., Yeoh, W.K., Dennis, A.R., Pathak, S.K., Cardwell, D.A.: Batch-processed gdBCO–ag bulk superconductors fabricated using generic seeds with high trapped fields. Phys. C 470, 685–688 (2010)
Murakami, M., Sakai, N., Higuchi, T., Yoo, S.I.: Supercond. Sci. Technol. 9, 1015 (1996)
Yoo, S.I., Sakai, N., Takaichi, H., Murakami, M.: Melt processing for obtaining NdBa2Cu3Oy superconductors with high Tc and large Jc. Appl. Phys. Lett. 65, 633–635 (1994)
Saitoh, T., Segawa, K., Kamada, K., Sakai, N., Segawa, T., Yoo, S.I., Murakami, M.: Microstructures and superconducting properties of melt-processed (RE,RE’)-Ba-Cu-O. Phys. C 288, 141–147 (1997)
Muralidhar, M., Koblischka, M.R., Saitoh, T., Murakami, M.: Microstructure and pinning in high-Tc and large-Jc (Nd, Eu, Gd)-123 superconductors prepared by OCMG process. Supercond. Sci. Technol. 11, 1349–1358 (1998)
Nariki, S., Sakai, N., Murakami, M.: Melt-processed Gd–Ba–Cu–O superconductor with trapped field of 3 T at 77 K. Supercond. Sci. Technol. 18, S126–S130 (2005)
Muralidhar, M., Sakai, N., Chikumoto, N., Jirsa, M., Machi, T., Nishiyama, M., Wu, Y., Murakami, M.: New type of vortex pinning structure effective at very high magnetic fields. Phys. Rev. Lett. 89, 23–25 (2002)
Cloots, R., Koutzarova, T., Mathieu, J.P., Ausloos, M.: Supercond. Sci. Technol. 18, R9 (2005)
Sudhakar Reddy, E., Rajasekharan, T.: Fabrication of textured REBa2Cu3O7/RE2BaCuO5 (RE = Y, Gd) composites by infiltration and growth of RE2BaCuO5 preforms by liquid phases. Supercond. Sci. Technol. 11, 523–534 (1998)
Devendra Kumar, N., Rajasekharan, T., Muraleedharan, K., Banerjee, A., Seshubai, V.: Unprecedented current density to high fields in YBa2Cu3O7−δ superconductor through nano-defects generated by preform optimization in infiltration growth process. Supercond. Sci. Technol. 23, 105020–8 (2010)
Pavan Kumar Naik, S., Devendra Kumar, N., Missak Swarup Raju, P., Rajasekharan, T., Seshubai, V.: Effect of infiltration temperature on the properties of infiltration growth processed YBCO superconductor. Phys. C 487, 72–76 (2013)
Li, G.Z., Yang, W.M., Cheng, X.F., Fan, J., Guo, X.D.: A modified TSIG technique for simplifying the fabrication process of single-domain gdBCO bulks with a new kind of liquid source. J. Mater. Sci. 44, 6423–6426 (2009)
Muralidhar, M., Ide, N., Koblischka, M.R., Diko, P., Inoue, K., Murakami, M.: Microstructure, critical current density and trapped field experiments in IG processed y-123. Supercond. Sci. Technol. 29, 054003–10 (2016)
Li, B., Zhou, D., Xu, K., Hara, S., Tsuzuki, K., Miki, M., Felder, B., Deng, Z., Izumi, M.: Materials process and applications of single grain (RE)–ba–cu–o bulk high-temperature superconductors. Phys. C 482, 50–57 (2012)
Iida, K., Babu, N.H., Shi, Y.H., Cardwell, D.A., Murakami, M.: Gd–ba–cu–o bulk superconductors fabricated by a seeded infiltration growth technique under reduced oxygen partial pressure. Supercond. Sci. Technol. 19, 641–647 (2006)
Wang, M., Yang, P., Yang, W., Li, J.W., Hassan, Q.: The fabrication process of a high performance and pure c-axis grown gdBCO bulk superconductor with the TSMT-IG technique. Supercond. Sci. Technol. 28, 105011–10 (2015)
Pavan Kumar Naik, S., Missak Swarup Raju, P., Rajasekharan, T., Seshubai, V.: Limited infiltration due to reactive sintering of nano-Sm2O3 with preforms - its effect on (Y, Sm)Ba2Cu3 O7−δ superconductors. Supercond. Sci. Technol. 29, 115001–11 (2016)
Pavan Kumar Naik, S., Seshubai, V.: Role of nano and micron sized inclusions on the oxygen controlled POIG processed YBCO superconductors. J. Phys. Chem. Solids 101, 65–73 (2017)
Pavan Kumar Naik, S., Missak Swarup Raju, P., Seshubai, V.: Role of Sm and Nb on the structural, microstructural and magnetic properties of the YBCO superconductors. Mater. Chem. Phys. 182, 503–507 (2016)
Chen, D.X., Goldfarb, R.B.: Kim model for magnetization of type-II superconductors. J. Appl. Phys. 66, 2489–2500 (1989)
Bean, C.P.: Magnetization of hard superconductors. Phys. Rev. Lett. 8, 250–253 (1962)
Gyorgy, E.M., van Dover, R.B., Jackson, K.A., Schneemeyer, L.F., Waszczak, J.V.: Anisotropic critical currents in Ba2YCu3O7 analyzed using an extended Bean model. Appl. Phys. Lett. 55, 283–285 (1989)
Muralidhar, M., Sakai, N., Jirsa, M., Murakami, M., Hirabayashi, I.: Record flux pinning in melt-textured NEG-123 doped by Mo and Nb nanoparticles. Appl. Phys. Lett. 92, 162512–162515 (2008)
Yoo, S.I., Murakami, M., Sakai, N., Ohyama, T., Higuchi, T., Watahiki, M., Takahashi, M.: Melt processing for strong flux pinning in RE-ba-cu-o (RE: Nd, Sm, Eu, Gd) superconductors. J. Electron. Mater. 24, 1923–1930 (1995)
Muralidhar, M., Murakami, M.: Effect of matrix composition on the flux pinning in (Nd,Eu,Gd)Ba2Cu3Oy superconductor. Phys. Rev. B 62, 13911–13914 (2000)
Koblischka, M.R., Muralidhar, M., Murakami, M.: Flux pinning in ternary melt-processed (Nd0.33Eu0.33Gd0.33)Ba2Cu3Oy superconductors. Appl. Phys. Lett. 73, 2351 (1998)
Muralidhar, M., Koblischka, M.R., Murakami, M.: Refinement of secondary phase particles for high critical current densities in Nd,Eu,Gd–Ba–Cu–O superconductors. Phys. C 313, 232–240 (1999)
Kobayashi, S., Kaneko, T., Kato, T., Fujikami, J., Sato, K.: A novel scaling of magnetic field dependencies of critical currents for Ag-sheathed Bi-2223 superconducting tape. Phys. C 258, 336–340 (1996)
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SPKN would like to acknowledge Shibaura Institute of Technology, Tokyo, Japan, gratefully for providing fellowship.
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Pavan Kumar Naik, S., Muralidhar, M. & Murakami, M. Optimization of the Dy Content in Single Crystalline GdBCO Bulk Superconductors Fabricated in Air Via Top-Seeded Infiltration Growth Process. J Supercond Nov Magn 31, 981–987 (2018). https://doi.org/10.1007/s10948-017-4277-0
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DOI: https://doi.org/10.1007/s10948-017-4277-0