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The Effect of Sintering Temperature in Bi1.7Pb0.2Sb0.1Sr2Ca2Cu3O y Superconductors

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Abstract

In this study, the effects of sintering temperature on the Bi-2223 phase formation and the influence of minor phases on the intergranular properties of Sb substituted Bi-2223 samples were investigated. The samples were prepared by solid-state reaction method with different sintering temperatures ranging from 800 to 855 °C. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and density measurements. We observed the optimal temperature of the Sb + Pb substituted Bi-2223 system as 845 °C.

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Authors and Affiliations

  1. Department of Physics, Dokuz Eylul University, Buca Izmir, Turkey

    Kemal Kocabaş, Özlem Bilgili & Nuray Yaşar

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  1. Kemal Kocabaş
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  2. Özlem Bilgili
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  3. Nuray Yaşar
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Correspondence to Kemal Kocabaş.

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Kocabaş, K., Bilgili, Ö. & Yaşar, N. The Effect of Sintering Temperature in Bi1.7Pb0.2Sb0.1Sr2Ca2Cu3O y Superconductors. J Supercond Nov Magn 22, 643–650 (2009). https://doi.org/10.1007/s10948-009-0455-z

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  • DOI: https://doi.org/10.1007/s10948-009-0455-z

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