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Synthesis and Characterization of Sulfamic-Acid Functionalized Magnetic Fe3O4 Nanoparticles Coated by Poly(amidoamine) Dendrimer

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Abstract

Grafting of chlorosulfuric acid on the amino-functionalized Fe3O4 nanoparticles produced sulfamic acid-functionalized magnetic Fe3O4 nanoparticles as a novel organic–inorganic hybrid material, which was characterized with X-ray diffractometry (XRD), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy, scanning electron spectroscopy, and magnetization measurements (VSM). The as-prepared nanocomposite with a narrow size distribution has the crystallite size from XRD (11 ± 4 nm) and particle size from TEM analysis (12.9 ± 0.4 nm) are consistent with each other. Magnetization measurements proved the superparamagnetic property of the product.

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Acknowledgments

This work was supported by Fatih University under BAP Grant No: P50021301-Y (3146).

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Authors and Affiliations

  1. Department of Chemistry, Fatih University, 34500, B. Cekmece, Istanbul, Turkey

    Umran Kurtan & Abdulhadi Baykal

  2. TUBITAK-UME, National Metrology Institute, PO Box 54, 41470, Gebze, Kocaeli, Turkey

    Hüseyin Sözeri

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  1. Umran Kurtan
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  2. Abdulhadi Baykal
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  3. Hüseyin Sözeri
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Correspondence to Umran Kurtan.

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Kurtan, U., Baykal, A. & Sözeri, H. Synthesis and Characterization of Sulfamic-Acid Functionalized Magnetic Fe3O4 Nanoparticles Coated by Poly(amidoamine) Dendrimer. J Inorg Organomet Polym 24, 948–953 (2014). https://doi.org/10.1007/s10904-014-0066-4

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  • DOI: https://doi.org/10.1007/s10904-014-0066-4

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