Abstract
In this work, we have successfully prepared rod-like lead tungstate (PbWO4) nanostructures via sonochemical route by utilizing lead (II) acetate trihydrate and sodium tungstate dihydrate as starting materials in water as solvent without adding surfactant. The formation of as-produced nanostructures and their structure, shape and elemental composition were analyzed by means of several techniques including X-ray diffraction, energy dispersive X-ray microanalysis, scanning electron microscopy, and ultraviolet–visible spectroscopy. The magnetic properties of as-prepared lead tungstate nanostructures were also investigated with vibrating sample magnetometer. In addition, methyl orange was chosen as a dye water pollution to evaluate its degradation by as-synthesize lead tungstate under ultraviolet light irradiation. The photocatalysis results reveal that the decolorization of 72 % for methyl orange occurred with PbWO4 nanostructures in 70 min under ultraviolet light irradiation.
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Authors are grateful to council of University of Central Tehran for providing financial support to undertake this work.
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Talebi, R. Investigation of the structural, optical and magnetic properties of rod-like lead tungstate nanostructures synthesized via a facile and reliable route. J Mater Sci: Mater Electron 27, 10770–10774 (2016). https://doi.org/10.1007/s10854-016-5181-2
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DOI: https://doi.org/10.1007/s10854-016-5181-2