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Effect of Ce and Mg doping on LiZn ferrites hollow microspheres prepared by self-reactive quenching technology

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Abstract

Lithium–Zinc ferrite hollow microspheres (LiZn FHMs) doped with Ce and Mg were synthesized with Fe + Zn + Fe2O3 + O2 + Li2CO3 reactive system by using self-reactive quenching technology. Effect of Ce and Mg doping on the surface morphology, phase structure, and microwave absorption properties of LiZn FHMs were investigated in detail. The results indicate that the surface morphology of LiZn FHMs shows little variation after Ce and Mg doping and is still composed of unnoticeable multi-shape crystal. The phases are mainly composed of Fe3O4, Fe2O3, Li0.435Zn0.195Fe2.37O4 and Li0.5Fe2.5O4 without doping. The main phases remain unchanged with Mg doping, but CeO2 appears in the phase components with Ce doping. It can be concluded that the microwave absorption properties are improved by Ce doping due to the variation of the ferromagnetic resonance frequency. But those of Mg doping are reduced due to the introduction of non-magnetic Mg2+.

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Acknowledgments

Authors would like to express their sincere appreciation to National Natural Science Fund of China (No. 51172282) and Hebei Natural Science Fund of China (E2015506011) for financial support. Tremendous thanks are owed to Baochen Li and Aihua Wu, who provide us with great help in the investigation.

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Authors and Affiliations

  1. Advanced Material Institute, Mechanical Engineering College, Heping West Road 97, Shijiazhuang, 050003, People’s Republic of China

    Xudong Cai, Baocai Xu, Jianjiang Wang, Haitao Gao, Liang Yu & Ze Li

  2. Scientific Research Department, Mechanical Engineering College, Shijiazhuang, 050003, People’s Republic of China

    Baochen Li

  3. Hebei Semiconductor Institute, Shijiazhuang, 050051, People’s Republic of China

    Aihua Wu & Bing Wang

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  1. Xudong Cai
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  2. Baocai Xu
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Correspondence to Xudong Cai.

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Cai, X., Xu, B., Wang, J. et al. Effect of Ce and Mg doping on LiZn ferrites hollow microspheres prepared by self-reactive quenching technology. J Mater Sci: Mater Electron 27, 1328–1336 (2016). https://doi.org/10.1007/s10854-015-3893-3

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