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Shear banding mechanisms in Cu/Ru nano-structured multilayers: effect of phase transformation

  • Metals & corrosion
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Abstract

The shear banding mechanisms of sputter-deposited nanoscale Cu/Ru multilayer with single-layer thickness of 0.8 nm and 1.5 nm, respectively, were investigated by nanoindentation. Shear bands can be observed in Cu/Ru multilayer only when the layer thickness is 1.5 nm. Deformed microstructure analysis showed that the plastic deformation behavior within the shear band of Cu1.5/Ru1.5 multilayer is primarily controlled by the dislocation dominated non-crystallographic rotation through the Cu/Ru interface without changing the crystallographic orientation. By synthetical analyzing of the indentation-induced deformed microstructures, a deformation mode transition from shear banding to opening crack is suggested as decreasing the layer thickness from 1.5 to 0.8 nm, mainly relating to the phase structure of Ru layer. Moreover, the excellent toughness of Cu/Ru multilayers also could be obtained by regulating the influences of phase structure on the shear band formation.

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Acknowledgements

This work was supported by the National Natural Science Foundation of China (No. 52175188), Key Research and Development Program of Shaanxi Province (2023-YBGY-434) and the Open Fund of Liaoning Provincial Key Laboratory of Aero-engine Materials Tribology (LKLAMTF202301). We would also like to thank Dr. Yixue Li and Dr. Qiufeng Wang from the Analytical and Testing Center of Northwestern Polytechnical University for their significant help during the nanoindentation test.

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Authors and Affiliations

  1. School of Mechanical Engineering, Chengdu University, Chengdu, 610106, China

    Xuguang An & Yupeng Zhang

  2. State Key Laboratory of Solidification Processing, Center of Advanced Lubrication and Seal Materials, Northwestern Polytechnical University, Xi’an, 710072, China

    Qikang Li

  3. Science and Technology on Reactor Fuel and Materials Laboratory, Nuclear Power Institute of China, Chengdu, 610041, China

    Hui Wang

  4. Interdisciplinary Materials Research Center, Institute for Advanced Study, Chengdu University, Chengdu, 610106, China

    Hui Wang

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  1. Xuguang An
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  2. Yupeng Zhang
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Contributions

AX contributed to the conceptualization, methodology and writing—original draft. ZY was involved in the investigation, formal analysis and writing—original draft. LQ assisted in the formal analysis, funding acquisition and writing—original draft. WH contributed to the conceptualization and methodology and supervision.

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Correspondence to Hui Wang.

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Handling Editor: :Zhao Shen.

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An, X., Zhang, Y., Li, Q. et al. Shear banding mechanisms in Cu/Ru nano-structured multilayers: effect of phase transformation. J Mater Sci 59, 3652–3661 (2024). https://doi.org/10.1007/s10853-024-09396-9

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  • DOI: https://doi.org/10.1007/s10853-024-09396-9

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