Abstract
The aldehyde jasmorange (1) was converted to the oxime (2), acylation of which by alkylcarboxylic acid anhydrides in the presence of HClO4 or by acid chlorides in the presence of pyridine synthesized esters of jasmorange oxime 3–24 in 82–91% yields. Refluxing 3–24 in hexane converted them quantitatively into nitrile 25.
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E. A. Dikusar, N. G. Kozlov, N. A. Zhukovskaya, and K. L. Moiseichuk, Khim. Prir. Soedin., 154 (2002).
N. A. Zhukovskaya, E. A. Dikusar, K. L. Moiseichuk, and O. G. Vyglazov, Zh. Prikl. Khim., 79, 642 (2006).
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Translated from Khimiya Prirodnykh Soedinenii, No. 4, pp. 307–310, July–August, 2007.
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Dikusar, E.A., Zhukovskaya, N.A., Moiseichuk, K.L. et al. Esters of jasmorange oxime. Chem Nat Compd 43, 369–373 (2007). https://doi.org/10.1007/s10600-007-0140-z
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DOI: https://doi.org/10.1007/s10600-007-0140-z