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Mechanical and performance-related properties of bitumen-beneficiated indurated shale aggregates for use in road construction in southeastern Nigeria

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Abstract

In most developing countries, the use of marginal quality aggregates had resulted in premature distress on the road pavements not visible until years after construction. Abakaliki region is endowed with low-grade indurated shales that have tremendous potentials for use in road construction but require beneficiation in order to improve their quality and durability before use. It is, therefore, necessary to develop process of improving the aggregate properties to achieve satisfactory results. This study presents results of laboratory testing of the physico-mechanical properties of shales and when treated with bitumen. The concept was based on the principle of using coating process on the aggregates with a bituminous film. The aggregates can be rendered water-proofed so that their strength in dry condition could be retained even after wetting. The results of mineralogical and chemical analyses revealed that the shales have no remarkable differences in their mineralogy with predominance of quartz, clay minerals, and feldspar and high silica, aluminum, and alkali content, respectively. The strength and resistance to abrasion attrition of the aggregates were critical factors that determined the quality of the aggregates. The aggregates when tested in dry condition performed marginally when compared with standard criteria as the presence of moisture further downgrade the aggregate properties. When beneficiated, bituminous materials reduced the aggregate absorption capacity by blocking the capillaries within the aggregates with hydrophobic film, and increased the aggregate resistance against weathering. The treated aggregates showed potential for appreciable gain in strength which qualifies the aggregates for use as road construction.

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References

  • Ademeso OA, Olaleye BM (2014) Physicomechanical characteristics of charnockitic rock of Akure. Southwest Nigeria, Gen Scie Res 2(1):31–37

    Google Scholar 

  • Adom-Asamoah M, Afrifa RO (2010) A study of concrete properties using phyllite as coarse aggregates. J Mater Design 31(9):4561–4566

    Article  Google Scholar 

  • Aghamelu OP, Okogbue CO (2015) Usability of pyroclastic rocks as construction materials, example from Nigeria. Eng Geol Soc Territory 5:1259–1266

    Article  Google Scholar 

  • Agyeman S, Assiamah S, Twumas G (2019) Correlations of physicomechanical properties of quarry aggregates - the case of two quarries in Ghana. Global J Eng Sci 2(1):1–11

    Google Scholar 

  • ASTM (2005) Standard Test Method for Laboratory Determination of Pulse Velocities and Ultrasonics Elastic Constants of Rock: D. 2845-05, Annual Book of A.S.T.M. Standards: 4.08. American Society for Testing and Materials, West Conshocken

  • ASTM (American Society for Testing and Materials) C 127 (1990a) Standard test for specific gravity and absorption of coarse aggregate. ASTM International, West Conshohocken

  • ASTM (American Society for Testing and Materials) C 88 (1990b) Standard test for soundness of aggregate by use of sodium or magnesium sulphate. ASTM International, West Conshohocken

  • ASTM (American Society for Testing and Materials) C 128 (1990c) Standard tests for specific gravity and absorption of fine aggregate. ASTM International, West Conshohocken

  • ASTM (American Society for Testing and Materials) Standards (2006a) Standard test method for the resistance to degradation of small-size coarse aggregates by abrasion and impact in the Los Angeles Machine, C131–03, v. 04.02, USA

  • ASTM (American Society for Testing and Materials) Standards (2006b) Standard test method for the resistance to degradation of small-size coarse aggregates by abrasion and impact in the Los Angeles Machine, C127–04, v. 04.02, USA

  • ASTM (American Society for Testing and Materials) D75/D75M-09 (2009) Standard practice for sampling aggregates. West Conshohocken, Pennsylvania, PA 19428, USA

  • Benkhelil J (1989) The origin and evolution of the Cretaceous Benue Trough, Nigeria. J Africa Earth Sci 8:251–282

    Article  Google Scholar 

  • BS (British Standard Institution) 812, 1990 Testing aggregates, Part 121—method of determination of aggregate soundness British Standard Institution London

  • BS (British Standard Institute) (1990b) Methods for determination of aggregate impact value, BS 812.112, London

  • BS (British Standard Institution) 812 100 (1990c) Testing aggregates, Part 100—methods for determination of ten percent fines value (TFV) British Standard Institution London

  • British Standards Institution (1963) Sampling and testing of lightweight aggregate for concrete. BS 3681

  • British Standard Institute (1985) Methods for determination of Flakiness Index. BS 812.105.1, London

  • Bryson SL, Gomez-Gutierrez IC, Hopkins TC (2012) Development of a new durability index for compacted shale. Eng Geol 139–140:66–75

    Article  Google Scholar 

  • Bureau of Indian Standards (1978) “Methods for testing tar and bituminous materials, determination of penetration,” IS 1203:1978, Bureau of Indian Standards, New Delhi, India, 1978

  • Bureau of Indian Standards (1992) “Indian standard paving bitumen-specification, 2nd Revision,” IS 73:1992, Bureau of Indian Standards

  • Burke K, Dessauvagie TFJ, Whiteman AJ (1971) Opening of the gulf of Guinea and geological history of the Benue Depression and Niger Delta. Nat Phys Sci 233(38):51–55

    Article  Google Scholar 

  • Chang C (1980) “Evaluation of selected marginal aggregates stabilized with cement”, Transportation Research Report 80–8. Oregon State University, June, Department of Civil Engineering, p 1980

    Google Scholar 

  • Cratchley C, Jones GP (1965) An interpretation of the geology and gravity anomalies of the Benue Valley, Nigeria. Overseas Geol Surv Geophys Pap 1 Geol Mag 118:59–67

  • Deere DU, Gamble JC (1971) Durability-plasticity classification of shales and indurated clay. Proceedings of the 22nd Annual Highway Geology Symposium, Univ. of Oklahoma, Norman, OK, 37–52

  • Ehinola OA (2010) Biostratigraphy and depositional environment of the oil shale deposit In the Abakaliki fold belt, southeastern Nigeria. Oil Shale 27(2):99–125

    Article  Google Scholar 

  • Evans GL (1980) “Properties of marginal aggregates treated with asphalt emulsion”, Transportation Engineering Report 80–5. Oregon State University, June, Department of Civil Engineering, p 1980

    Google Scholar 

  • Eze EO (1997) Geotechnical assessment of some charnockites from Nigeria as construction materials. Q J Eng Geol 30:231–236

    Article  Google Scholar 

  • Franklin JA, Chandra A (1972) The slake durability test. Intern J Rock Mech 9:325–341

    Article  Google Scholar 

  • Freedonia (2009) World construction aggregates: industry study with forecasts for 2013 & 2018. The Freedonia Group Inc, Cleveland. Study No. (2564):322

  • Fournari R, Ioannou I (2019) Correlations between the properties of crushed fine aggregates, Minerals 2019, 9, 86. https://doi.org/10.3390/min9020086

  • Huddleston IJ, Vinson TS, Hicks RG (1980) “Cement stabilization of degrading aggregates,” paper presented at 59th Annual Meeting of Transportation Research Board, Washington, D.C.

  • Ioannou I, Petrou MF, Fournari R, Andreou A, Hadjigeorgiou C, Tsikouras B, Hatzipanagiotou K (2010) Crushed limestone as an aggregate in concrete production: the Cyprus case. Geol Soc Spec Publ 331:127–135

    Article  Google Scholar 

  • Irfan TY (1994) Aggregate properties and resources of granitic rocks for use in concrete in Hong Kong. Q J Eng Geol 27:25–38

    Article  Google Scholar 

  • Koncagul EC, Santi PM (1999) Predicting the unconfined compressive strength of the Breathitt shale using slake durability, shore hardness and rock structural properties. Int J Rock Mech Min Sci 36(2):139–153

    Article  Google Scholar 

  • Krynine DP, Judd WR (1957) Principles of engineering geology and geotechnics. McGraw-Hill, New York, p 699

    Google Scholar 

  • Marques EAG, Vargas EDA, Antunes FS (2005) A study of the durability of some shales, mudrocks and siltstones from Brazil. Geotech Geol Eng 23(3):321–348

    Article  Google Scholar 

  • Naeem M, Khalid P, Sanaullah M, Din Z (2014) Physio-mechanical and aggregate properties of limestones from Pakistan, A Quarterly of the Hungarian Academy of Sci., Acta Geod Geophys 49(3):369–380

  • Ndukauba E, Tse T (2012) Engineering-geological evaluation of rock materials from Bansara, Bamenda Massif Southeastern Nigeria as aggregates for pavement construction. Geosciences 2(5):107–111

    Google Scholar 

  • Nwajide CS (2013) Geology of Nigeria’s sedimentary basins. CSS Bookshops Ltd, Lagos, p 565

    Google Scholar 

  • Nweke OM, Okogbue CO (2017) The potential of cement stabilized shale quarry dust for possible use as road foundation material. Inter J Geo-Eng 8(29):1- 14

  • Obiora SC, Umeji AC (2004) Petrographic evidence for regional burial metamorphism of sedimentary rocks in the lower Benue Rift. Jour Afr Earth Sci 38(3):269–277

    Article  Google Scholar 

  • Obiora SC, Charan SN (2011) Geochemistry of regionally metamorphosed sedimentary rocks from the lower Benue Rift: implications for provenance and tectonic setting of the Benue rift sedimentary suite. South Africa J Geo 1(1):25–40

  • Ofonime A, Aniekan E (2005) Relationship between road pavement failures, Engineering indices and underlying Geology in a tropical environment. Global J Geol Sci 4(2):99–108

    Google Scholar 

  • Oyediran IA, Fadamoro OF (2015) Suitability of Ugbo-Odogu and Gariki Shale, Southeastern Nigeria as Construction Materials. Int J Pure Appl Sci Technol 26(1):1–13

    Google Scholar 

  • Paige-Green P (2007) Durability of basic crystalline rocks and specification for use as road base aggregate. Bull Eng Geol Environ 66:431–440

    Article  Google Scholar 

  • Petrounias P, Giannakopoulou PP, Rogkala A, Lampropoulou P, Koutsopoulou E, Papoulis D, Tsikouras B, Hatzipanagiotou K (2018) The impact of secondary phyllosilicate minerals on the engineering properties of various igneous aggregates from Greece. Minerals 8:329

    Article  Google Scholar 

  • Pinard MI, Jackalas P (1988) Durability aspects of chemically stabilized weathered basaltic materials for low volume road base construction. Transportation Research Record N1106. Fourth Intern Con Low-Vol Roads, USA 1:89–102

    Google Scholar 

  • Reidenour DR (1970) Shale suitability- Phase II, Pennsylvania department of transportation, Bureau of materials, testing and research, Interim Report No. 1

  • Reidenour DR, Geiger EG, Howe RH (1976) "Suitability of shale as a construction material," Living with marginal aggregates, STP 597. American Society for Testing and Materials, Philadelphia, Pennsylvania

  • Reyment RA (1965) Aspects of the geology of Nigeria. University Press, Ibadan, Nigeria, p 154

    Google Scholar 

  • Rigopoulos I, Tsikouras B, Pomonis P, Hatzipanagiotou K (2010) The influence of alteration on the engineering properties of dolerites: the example from the Pindos and Vourinos ophiolites (northern Greece). Int J Rock Mech Min Sci 47:69–80

    Article  Google Scholar 

  • Robnett QL, Thompson MR (1970) “Recommendations for stabilization of Illinois soils”, Bulletin 502. University of Illinois, Engineering Experiment Station

    Google Scholar 

  • Shakoor A, West TR, Scholer CF (1982) Physical characteristics of some Indiana argillaceous carbonates regarding their freeze–thaw resistance in concrete. Bull Assoc Eng Geol 19(4):371–384

    Google Scholar 

  • Shakoor A, Brock D (1987) Relationship between fissility, composition and engineering properties of selected shales from northeast Ohio. Bull. A.E.G., 14(3):363–379

  • Stålheim, J. (2014). Comparative study of established test methods for aggregate strength and durability of Archean rocks from Botswana UPTEC W13044, Examensarbete 30 hp, 44

  • Waltham AC (1994) Foundations of engineering geology, 2nd edn. Spon Press, London

    Google Scholar 

  • Williams, S.G. and Cunningham, J.B. (2012). Evaluation of aggregate durability performance test procedures. Available online: http://arkansastrc.com/TRC%20REPORTS/TRC%200905.pdf

  • Wu Y, Parker F, Kandhal K (1998) Aggregate toughness/abrasion resistance and durability/soundness tests related to asphalt concrete performance in pavements; Technical Report for NCAT: Auburn, AL, USA, March 1998

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Acknowledgements

We appreciate the laboratory attendants that assisted during the analyses and Dr. Ezekiel Igwe of Ebonyi State University who assisted in proofreading the manuscript as well as all the anonymous reviewers for their valuable and useful comments which assisted in improving the quality of the paper.

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Correspondence to Obisi Matthias Nweke.

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Nweke, O.M., Okogbue, C.O. Mechanical and performance-related properties of bitumen-beneficiated indurated shale aggregates for use in road construction in southeastern Nigeria. Bull Eng Geol Environ 80, 9141–9156 (2021). https://doi.org/10.1007/s10064-021-02379-z

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